IP Library Granted Patent US 7,993,620
Granted Patent B2
US 7,993,620 · App. 11/488,387 · Granted Aug 9, 2011

Systems and methods for formation and harvesting of nanofibrous materials

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Quick Facts
Patent No.
US 7,993,620
App. No.
11/488,387
Granted
Aug 9, 2011
Kind
B2
Abstract

A system that receives nanomaterials, forms nanofibrous materials therefrom, and collects these nanofibrous materials for subsequent applications. The system is coupled to a chamber that generates nanomaterials, typically carbon nanotubes produced from chemical vapor deposition, and includes a mechanism for spinning the nanotubes into yarns or tows. Alternatively, the system includes a mechanism for forming non-woven sheets from the nanotubes. The system also includes components for collecting the formed nanofibrous materials. Methods for forming and collecting the nanofibrous materials are also provided.

Claims (37)

1. A method for forming a nanofibrous non-woven sheet, the method comprising:

synthesizing a volume of free-flowing nanotubes from a carbon source and a plurality of catalyst particles;

depositing the volume of free-flowing nanotubes continually onto a moving surface;

transporting the volume of nanotubes continually deposited onto the moving surface away from a point of deposition;

applying pressure onto the plurality of nanotubes against the surface, so as to compact the nanotubes into a non-woven sheet of intermingled nanotubes;

directing the non-woven sheet toward an area independent of the moving surface for collection;

putting a material onto one side of the non-woven sheet to prevent the non-woven sheet from bonding to itself; and

collecting the non-woven sheet from the moving surface by winding the sheet about an axis substantially transverse to a direction of movement of the sheet.

2. A method as set forth in claim 1 , wherein the step of depositing includes continuously depositing the nanotubes onto the surface within an airtight environment.

3. A method as set forth in claim 1 , wherein the step of transporting includes moving the nanotubes away in a direction substantially transverse to a direction of deposition.

4. A method as set forth in claim 1 , wherein the step of applying includes forcing the nanotubes to move between the surface and a rolling mechanism.

5. A method as set forth in claim 1 , wherein the step of directing includes lifting the non-woven sheet from the surface so that it is substantially disengaged for subsequent harvesting.

6. A method as set forth in claim 1 , wherein, in the step of putting, the material is a non-magnetic material so as to prevent the non-woven sheet from sticking strongly to the material.

7. A method as set forth in claim 1 , wherein the step of collecting includes controlling a rate of winding, so as to avoid compromising the integrity of the non-woven sheet.

8. A method as set forth in claim 1 , further including, prior to the step of depositing, generating an electrostatic field through which the nanotubes can be directed to permit substantial alignment of the nanotubes.

9. A method for forming a nanofibrous non-woven sheet, the method comprising:

synthesizing a volume of free-flowing nanotubes from a carbon source and a plurality of catalyst particles;

depositing the volume of free-flowing nanotubes continually onto a moving surface;

transporting the volume of nanotubes continually deposited onto the moving surface away from a point of deposition;

directing the non-woven sheet toward an area independent of the moving surface for collection; and

collecting the non-woven sheet from the moving surface.

10. A method as set forth in claim 9 , wherein the step of removing includes lifting the non-woven sheet from the surface so that it is substantially disengaged for subsequent harvesting.

11. A method as set forth in claim 9 , further including, prior to the step of depositing, generating an electrostatic field through which the nanotubes can be directed to permit substantial alignment of the nanotubes.

12. A method for forming a nanofibrous sheet, the method comprising:

synthesizing, from a carbon source and a plurality of catalyst particles, a volume of free-flowing nanotubes;

continually depositing the volume of free-flowing nanotubes onto a moving surface;

transporting the volume of nanotubes continually deposited onto the moving surface away from a point of deposition;

allowing the plurality of nanotubes deposited onto the surface to compact into a non-woven sheet of intermingled nanotubes; and

collecting the non-woven sheet.

13. A method as set forth in claim 12 , further including, prior to the step of depositing, generating an electrostatic field through which the nanotubes can be directed to permit substantial alignment of the nanotubes.

14. A method for forming a nanofibrous sheet, the method comprising:

synthesizing, from a carbon source and a plurality of catalyst particles, a volume of free-flowing nanotubes;

continually depositing the volume of free-flowing nanotubes onto a moving surface;

transporting the volume of nanotubes continually deposited onto the moving surface away from a point of deposition;

removing the non-woven sheet from the moving surface; and

collecting the non-woven sheet from the moving surface.

15. A method as set forth in claim 14 , further including, prior to the step of depositing, generating an electrostatic field through which the nanotubes can be directed to permit substantial alignment of the nanotubes.

Assignments (9)
RELEASE OF SECURITY INTEREST Recorded Jul 28, 2026
From: SECTOR CAPITAL GROUP, LLC
To: HUNTSMAN NANOCOMP LLC
Reel/Frame 075425/0284 →
RELEASE OF SECURITY INTEREST Recorded Jul 28, 2026
From: PIVOTAL CAPITAL FUND, LP
To: HUNTSMAN NANOCOMP LLC
Reel/Frame 075425/0272 →
SECURITY INTEREST Recorded May 4, 2026
From: HUNTSMAN INTERNATIONAL LLC; HUNTSMAN ADVANCED MATERIALS AMERICAS LLC; HUNTSMAN NANOCOMP LLC; HUNTSMAN PETROCHEMICAL LLC
To: CITIBANK N.A.
Reel/Frame 075498/0663 →
PATENT SECURITY AGREEMENT Recorded Mar 10, 2026
From: HUNTSMAN INTERNATIONAL LLC; HUNTSMAN ADVANCED MATERIALS AMERICAS LLC; HUNTSMAN NANOCAMP LLC; HUNTSMAN PETROCHEMICAL LLC
To: CITIBANK, N.A.
Reel/Frame 075106/0238 →
SECURITY INTEREST Recorded Jan 21, 2018
From: NANOCOMP TECHNOLOGIES, INC.
To: SECTOR CAPITAL GROUP, LLC
Reel/Frame 044683/0242 →
RELEASE OF SECURITY INTEREST Recorded May 12, 2017
From: HORIZON TECHNOLOGY FINANCE CORPORATION
To: NANOCOMP TECHNOLOGIES, INC.
Reel/Frame 042364/0414 →
SECURITY INTEREST Recorded May 12, 2017
From: NANOCOMP TECHNOLOGIES, INC.
To: PIVOTAL CAPITAL FUND, LP
Reel/Frame 042364/0279 →
SECURITY INTEREST Recorded Apr 8, 2016
From: NANOCOMP TECHNOLGIES, INC.
To: HORIZON TECHNOLOGY FINANCE CORPORATION
Reel/Frame 038231/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 9, 2006
From: LASHMORE, DAVID S.; BROWN, JOSEPH J.; CHAFFEE, JARED K.; RESNICOFF, BRUCE; ANTOINETTE, PETER
To: NANOCOMP TECHNOLOGIES, INC.
Reel/Frame 018136/0927 →