Cellulose acylate resin film and method for producing the same
View Patent ↗The present invention provides a method for producing a cellulose acylate resin film, comprising the step of, melting a cellulose acylate resin in an extruder and extruding the molten cellulose acylate resin to a die, wherein the step of melting is carried out using a tandem extruder having a first-stage extruder and a second-stage extruder connected in tandem, in order to prevent discoloration and thickness non-uniformity make the film seriously defective for use as an optical film. Because the resin in the form of a powder or flakes is once pelletized in a pelletizing extruder, and then the pellets are melt-extruded in an extruder. This promotes discoloration of the resin, disadvantageously.
1. A method for producing a cellulose acylate resin film, comprising the step of,
melting a cellulose acylate resin in an extruder and extruding the molten cellulose acylate resin to a die, wherein
the step of melting is carried out using a tandem extruder having a first-stage extruder and a second-stage extruder connected in tandem,
the cellulose acylate resin has an acylate group satisfying the following substitution degree:
2.0 ≦X+Y≦ 3.0 (1)
0 ≦X≦ 2.0 (2)
1.2 ≦Y≦ 2.9 (3)
wherein X is a substitution degree of an acetyl group, and Y is a total substitution degree of a propionyl group, butyryl group, pentanoyl group, and hexanoyl group,
wherein a reservoir tank having a heating device is provided between the first-stage extruder and the second-stage extruder to absorb the fluctuation in pressure between the first-stage extruder and the second-stage extruder, and
wherein the reservoir tank has a head space part filled with an inert gas.
2. The method for producing a cellulose acylate resin film according to claim 1 , wherein
the cellulose acylate resin before melting is in the form of a powder or flakes.
3. The method for producing a cellulose acylate resin film according to claim 2 , wherein
a twin-screw extruder is used as the first-stage extruder, and a single-screw extruder is used as the second-stage extruder.
4. The method for producing a cellulose acylate resin film according to claim 3 , wherein
the first-stage extruder is a vent extruder.
5. The method for producing a cellulose acylate resin film according to claim 1 , wherein
an additive is added to the first-stage extruder.
6. The method for producing a cellulose acylate resin film according to claim 1 , wherein
the amount and/or the pressure of the molten cellulose acylate resin in the reservoir tank are controlled to be constant.