Process for preparing methylhydroxyalkylcellulose having a small number of coloured particles
View Patent ↗The present invention describes a process for preparing methylhydroxyalkylcellulose having a small number of colored particles by separation of methylhydroxyalkylcellulose from aqueous suspension with subsequent washing of the methylhydroxyalkylcellulose using a specially equipped rotary pressure filter.
1. A process for preparing methyl hydroxyalkylcellulose comprising the steps of:
providing a rotary pressure filter including at least one drying zone, said filter comprising:
at least one heat-resistant, abrasion-resistant plastic separation plate sealing the drying zone(s), said separation plate being made of polyether ether ketone; and
at least one additional separation plate which seals off zones other than the drying zone(s) is made of polyvinylidene fluoride;
introducing an aqueous suspension containing methylhydroxyalkylcellulose into said rotary pressure filter; and
separating said methylhydroxyalkylcellulose from said aqueous suspension using said rotary pressure filter to obtain a concentrated methylhydroxyalkylcellulose stream.
2. The process according to claim 1 , wherein the methylhydroxyalkylcellulose is a methylhydroxyethylcellulose (MHEC) or a methylhydroxypropylcellulose (MHPC).
3. The process according to claim 1 , wherein the methylhydroxyalkylcellulose is a methylhydroxypropylcellulose (MHPC) which has a proportion by mass of hydroxypropoxy groups of from 3.0 to 35.0% and a proportion by mass of methoxyl groups of from 15.0 to 35.0.
4. The process according to claim 1 , wherein the methylhydroxyalkylcellulose is a methylhydroxypropylcellulose (MHPC) which has a proportion by mass of hydroxypropoxy groups of from 4.0 to 32.0% and a proportion by mass of methoxyl groups of from 16.5 to 30.0%.
5. The process according to claim 1 , wherein the methylhydroxyalkylcellulose is a methylhydroxyethylcellulose (MHEC) which has a degree of substitution MS (HE) of from 0.10 to 1.00 and a degree of substitution DS (M) of from 1.25 to 2.20.
6. The process according to claim 1 , wherein the methylhydroxyalkylcellulose is a methylhydroxyethylcellulose (MHEC) which has a degree of substitution MS (HE) of from 0.15 to 0.80, and a degree of substitution DS (M) of from 1.40 to 2.00.