IP Library Granted Patent US 8,076,518
Granted Patent B2
US 8,076,518 · App. 11/534,980 · Granted Dec 13, 2011

Chain extenders

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Quick Facts
Patent No.
US 8,076,518
App. No.
11/534,980
Granted
Dec 13, 2011
Kind
B2
Abstract

This invention provides chain extender compositions. These compositions comprise (i) an aliphatic secondary diamine, and (ii) a component selected from the group consisting of: (a) a cycloaliphatic primary diamine; (b) an aliphatic secondary diamine; (c) an aliphatic secondary diamine and an aliphatic primary diamine; (d) an aliphatic diimine; and (e) a combination of any two or more of (a) through (d), with the proviso that when (ii) is (a), (i) is a noncyclic aliphatic secondary diamine. Processes for producing polyurethanes, polyureas, and polyurea-urethanes are also provided.

Claims (33)

1. A chain extender composition which comprises

(i) N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane, and

(ii) a cycloaliphatic primary diamine,

wherein the relative proportions of N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane to cycloaliphatic primary diamine in the chain extender composition are in the range of about 5.7:1 to about 3:1 on a weight basis.

2. A composition as in claim 1 wherein (ii) is a cycloaliphatic primary diamine which has at least one of the following features:

the cycloaliphatic group has a single ring;

at least one of the amino groups is bound directly to a ring.

3. A composition as in claim 2 wherein said cycloaliphatic primary diamine is isophorone diamine.

4. A process for producing a polymer, which process comprises mixing together (A) at least one aliphatic polyisocyanate, (B) at least one polyol and/or at least one polyetheramine, and (C) a chain extender comprised of

(i) N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane, and

(ii) a cycloaliphatic primary diamine,

wherein the relative proportions of N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane to cycloaliphatic primary diamine in the chain extender composition are in the range of about 5.7:1 to about 3:1 on a weight basis.

5. A process as in claim 4 wherein said polyisocyanate is isophorone diisocyanate.

6. A process as in claim 4 wherein (B) is at least one polyetheramine.

7. A process as in claim 4 wherein said polyisocyanate is isophorone diisocyanate, and wherein (B) is at least one polyetheramine.

8. A process as in claim 4 wherein (ii) is isophorone diamine.

9. A process as in claim 4 wherein (ii) is a cycloaliphatic primary diamine which has at least one of the following features:

the cycloaliphatic group has a single ring;

one of the amino groups is bound directly to a ring.

10. A process as in claim 9 wherein said polyisocyanate is isophorone diisocyanate, and wherein (B) is at least one polyetheramine.

11. A process as in claim 4 wherein a quasiprepolymer is formed during the process.

12. A process as in claim 4 wherein a prepolymer is formed during the process.

13. A polymer formed from ingredients comprising (A) at least one aliphatic polyisocyanate, (B) at least one polyol and/or at least one polyetheramine, and (C) a chain extender comprised of

(i) N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane, and

(ii) a cycloaliphatic primary diamine,

wherein the relative proportions of N,N′-di-(3,3-dimethyl-2-butyl)-1,6-diaminohexane to cycloaliphatic primary diamine in the chain extender composition are in the range of about 5.7:1 to about 3:1 on a weight basis.

14. A polymer as in claim 13 wherein said polyisocyanate is isophorone diisocyanate.

15. A polymer as in claim 13 wherein (B) is at least one polyetheramine.

16. A polymer as in claim 13 wherein said polyisocyanate is isophorone diisocyanate, and wherein (B) is at least one polyetheramine.

17. A polymer as in claim 13 wherein (ii) is a cycloaliphatic primary diamine which has at least one of the following features:

the cycloaliphatic group has a single ring;

one of the amino groups is bound directly to a ring.

18. A polymer as in claim 13 wherein (ii) is isophorone diamine.

Assignments (6)
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 044473/0872 Recorded Mar 6, 2020
From: JEFFERIES FINANCE LLC
To: LINE-X LLC
Reel/Frame 052114/0407 →
SECURITY INTEREST Recorded Mar 5, 2020
From: LINE-X LLC; GROUND EFFECTS LTD.
To: UBS AG, STAMFORD BRANCH, AS GRANTEE
Reel/Frame 052029/0361 →
SECURITY INTEREST Recorded Mar 5, 2020
From: LINE-X LLC; GROUND EFFECTS LTD.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 052033/0439 →
SECURITY INTEREST Recorded Dec 22, 2017
From: LINE-X LLC
To: JEFFERIES FINANCE LLC
Reel/Frame 044473/0872 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2017
From: ALBEMARLE CORPORATION
To: LINE-X LLC
Reel/Frame 043756/0587 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 12, 2007
From: WIGGINS, PAUL L.; LEE, JOHN Y.; ORGAD, JUDIT O.; OWENS, DAVID W.
To: ALBEMARLE CORPORATION
Reel/Frame 019150/0756 →