IP Library Patent Application 11541526
Patent Application
App. No. 11/541,526

Method for producing particles, particles, and adsorption apparatus

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Quick Facts
Patent No.
US None
App. No.
11/541,526
Abstract

Disclosed herein are a method for producing particles whereby dense particles (especially, spherical particles) composed of a calcium phosphate-based compound can be efficiently produced at low cost, particles which are produced by the method, and an adsorption apparatus which is produced by using the particles as an adsorbent. The method for producing particles comprises preparing a liquid containing primary particles composed of a calcium phosphate-based compound and a dispersion medium; feeding the liquid into a heated atmosphere in the form of droplets to obtain aggregates of the primary particles by removing the dispersion medium from each of the droplets and then bring the aggregates into a molten state so that each of the aggregates is formed into a spherical shape; and solidifying the aggregates in the molten state to obtain dense secondary particles. The heated atmosphere preferably contains plasma produced by ionization of an ambient gas. Further, the plasma forms a plasma flame in the heated atmosphere; and the droplets are preferably fed into the circumferential portion of the plasma flame

Claims (22)

1 . A method for producing particles, comprising:

preparing a liquid containing primary particles composed of a calcium phosphate-based compound and a dispersion medium;

feeding the liquid into a heated atmosphere in the form of droplets to obtain aggregates of the primary particles by removing the dispersion medium from each of the droplets and then bring the aggregates into a molten state so that the respective aggregates are formed into a spherical shape; and

solidifying the aggregates in the molten state to obtain dense secondary particles.

2 . The method for producing particles as claimed in claim 1 , wherein the heated atmosphere contains plasma produced by ionization of an ambient gas.

3 . The method for producing particles as claimed in claim 2 , wherein the plasma forms a plasma flame in the heated atmosphere; and

wherein the droplets are fed into the circumferential portion of the plasma flame.

4 . The method for producing particles as claimed in claim 3 , wherein the temperature at the circumferential portion of the plasma flame is in the range of 1,000 to 3,000° C.

5 . The method for producing particles as claimed in claim 1 , wherein the aggregates in the molten state each having the spherical shape are solidified by forcibly cooling them.

6 . The method for producing particles as claimed in claim 1 , wherein each of the obtained secondary particles has a surface with irregularities, and the surface of each secondary particle is subjected to a smoothing process to decrease or remove the irregularities.

7 . The method for producing particles as claimed in claim 6 , wherein the smoothing process includes a thermal treatment.

8 . The method for producing particles as claimed in claim 7 , wherein the temperature of the thermal treatment is in the range of 400 to 900° C.

9 . The method for producing particles as claimed in claim 1 , wherein the porosity of the obtained secondary particles is 5% or less.

10 . The method for producing particles as claimed in claim 1 , wherein an average particle diameter of the obtained secondary particles is in the range of 0.5 to 20 μm.

11 . The method for producing particles as claimed in claim 1 , wherein an average roundness coefficient C of the obtained secondary particles represented by the following formula (I) is in the range of 0.8 to 0.99:

C= 4 πS/L 2   ( I )

wherein S (μm 2 ) represents an area of a projection image of a particle as a measuring object, and L (μm) represents a circumferential length of the projection image of the particle.

12 . The method for producing particles as claimed in claim 1 , wherein the calcium phosphate-based compound includes hydroxyapatite or tricalcium phosphate.

13 . Particles produced by the method for producing particles defined by claim 1 .

14 . An adsorption apparatus, comprising:

a column having a filling space, and

an adsorbent filled in the filling space, the adsorbent including the particles defined by claim 13.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2006
From: KOBAYASHI, SHINTARO; YUBUTA, KAZUHIRO
To: PENTAX CORPORATION; NISSHIN ENGINEERING INC.
Reel/Frame 018632/0659 →