IP Library Granted Patent US 7,750,151
Granted Patent B2
US 7,750,151 · App. 11/547,113 · Granted Jul 6, 2010

Inhibitors of Akt activity

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Quick Facts
Patent No.
US 7,750,151
App. No.
11/547,113
Granted
Jul 6, 2010
Kind
B2
Abstract

The present invention is directed to compounds which contain substituted napthyridines which inhibit the activity of Akt, a serine/threonine protein kinase. The invention is further directed to chemotherapeutic compositions containing the compounds of this invention and methods for treating cancer comprising administration of the compounds of the invention.

Claims (93)

1. A compound which is selected from:

3-[(3-hydroxyphenyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)phenyl]-N-{[5-(1H-pyrazol-1-yl)pyridin-2-yl]methyl}methane;

(6-chloropyridin-3-yl)-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]methane;

[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)phenyl]-N-(pyridin-3-ylmethyl)methane;

(6-methoxypyridin-3-yl)-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]methane;

(6-oxo-1,6-dihydropyridin-3-yl)-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]methane;

3-[(2-hydroxyphenyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-[(3-hydroxyphenyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-[(4-hydroxyphenyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-[(2-methoxyphenyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-[(2-methoxyphenyl)(methyl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-[(3-hydroxypyridin-2-yl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-phenyl-2-[4-({[4-(1H-pyrazol-1-yl)benzyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2,2,2-trifluoro-N—[4-(6-methyl-5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]ethanesulfonamide;

2-[4-({[3-(2-aminophenyl)-3-oxopropyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[3-(5-oxo-4,5-dihydro-1H-pyrazol-4-yl)propyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(1,3-benzodioxol-5-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

4-(2-{[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]amino}ethyl)benzenesulfonamide;

2-{4-[({2-[(5-nitropyridin-2-yl)amino]ethyl}amino)methyl]phenyl}-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[4-(1,2,3-thiadiazol-4-yl)benzyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[1-(1H-benzimidazol-2-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-(4-{[(2-pyridin-3-ylethyl)amino]methyl}phenyl)-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3,4-dimethoxybenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(5-methyl-4H-1,2,4-triazol-3-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(1H-1,2,4-triazol-5-yl)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[(5-oxo-4,5-dihydro-1H-1,2,4-triazol-3-yl)methyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(3-pyridin-4-yl-1H-1,2,4-triazol-5-yl)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(1H-benzimidazol-2-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-(4-{[(2-pyridin-2-ylethyl)amino]methyl}phenyl)-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-(4-{[(2-pyridin-4-ylethyl)amino]methyl}phenyl)-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(2-oxoimidazolidin-1-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(2-morpholin-4-ylethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(2-anilinoethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(pyridin-2-ylamino)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[3-(2-oxopyrrolidin-1-yl)propyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(dimethylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(1,3-benzodioxol-5-ylmethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

N-(2-{[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]amino}ethyl)-1H-1,2,4-triazole-3-carboxamide;

2-[4-({[2-(1H-benzimidazol-1-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3,5-dimethoxybenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[4-(1H-pyrrol-1-yl)benzyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(3,4-dimethoxyphenyl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(6-methoxy-1H-indol-3-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(4-morpholin-4-ylbenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[3-(1H-1,2,3-triazol-1-yl)propyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-(4-{[(4-hydroxybenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-(4-{[(2-{[5-(trifluoromethyl)pyridin-2-yl]amino}ethyl)amino]methyl}phenyl)-1,6-naphthyridin-5(6H)-one;

2-(4-{[(imidazo[1,2-a]pyridin-2-ylmethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

4-({[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]amino}methyl)benzenesulfonamide;

2-[4-({[2-(2-amino-4-methyl-1,3-thiazol-5-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(1H-imidazol-4-yl)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(3,5-dimethyl-1H-pyrazol-4-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(1,3-benzothiazol-2-ylmethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-(4-{[(2-pyrazin-2-ylethyl)amino]methyl}phenyl)-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(1H-1,2,4-triazol-1-yl)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3H-imidazo[4,5-b]pyridin-2-ylmethyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-{4-[({1-[4-(1H-1,2,4-triazol-1-yl)phenyl]ethyl}amino)methyl]phenyl}-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(5-phenyl-2,5-diazabicyclo[2.2.1]hept-2-yl)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(1-methyl-1H-benzimidazol-2-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-phenyl-2-[4-({[2-(4-pyrimidin-2-ylpiperazin-1-yl)ethyl]amino}methyl)phenyl]-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3-morpholin-4-ylpropyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(4-hydroxyphenyl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(5-methyl-1H-imidazol-4-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(1H-imidazol-4-yl)ethyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(4-hydroxyphenyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[3-(dimethylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(dimethylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[2-(dimethylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(methylthio)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(methylsulfonyl)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(methylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3,4-dihydroxybenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[(1-methyl-1,2,3,4-tetrahydroquinolin-6-yl)methyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(4-chlorobenzyl)amino]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[(1-methyl-2,3-dihydro-1H-indol-5-yl)methyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

1,6-naphthyridin-5(6H)-one, 2-[4-[[[(6-methoxy-1H-benzimidazol-2-yl)methyl]amino]methyl]phenyl]-3-phenyl;

3-phenyl-2-{4-[({[6-(trifluoromethyl)pyridin-3-yl]methyl}amino)methyl]phenyl}-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3-hydroxybenzyl)oxy]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-(4-{[(3-hydroxybenzyl)oxy]methyl}phenyl)-3-phenyl-1,6-naphthyridin-5(6H)-one;

2-[4-({[4-(diethylamino)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

3-[(6-methoxypyridin-3-yl)amino]-3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]propane;

3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]-3-(pyridine-2-ylamino)propane;

2-[(2-hydroxybenzoyl)amino]-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]ethane;

3-oxo-N—[4-(5-oxo-3-phenyl-5,6-dihydro-1,6-naphthyridin-2-yl)benzyl]-3-(pyridine-4-ylamino)propane; and

2-[4-({methyl[4-(1H-pyrazol-1-yl)benzyl]amino}methyl)phenyl]-3-phenyl-1,6-naphthyridin-5(6H)-one;

or a pharmaceutically acceptable salt, tautomer or a stereoisomer thereof.

2. A compound of Formula C, wherein:

R 2 is H;

R 3 is selected from: phenyl, heterocyclyl, N(H)heterocyclyl and (C═O)R 6 , said phenyl and heterocyclyl optionally substituted with 1-3 sub substituents selected from R z′ ;

R 6 is independently selected from: H, NH 2 , phenyl and heterocyclyl, said phenyl and heterocyclyl optionally substituted with 1-3 substituents selected from R z′ ; and

R z′ is selected from: NH 2 , NO 2 , oxo, (C 1 -C 6 )alkyl, OH and S(O) 2 NH 2 ;

or a pharmaceutically acceptable salt, tautomer or a stereoisomer thereof.

Assignments (3)
CHANGE OF NAME Recorded Aug 29, 2012
From: SCHERING CORPORATION
To: MERCK SHARP & DOHME CORP.
Reel/Frame 028866/0511 →
MERGER Recorded Aug 27, 2012
From: MERCK SHARP & DOHME CORP.
To: SCHERING CORPORATION
Reel/Frame 028850/0515 →
CHANGE OF NAME Recorded Jan 25, 2010
From: MERCK & CO., INC.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 023837/0668 →