IP Library Granted Patent US 7,625,880
Granted Patent B2
US 7,625,880 · App. 11/617,651 · Granted Dec 1, 2009

Inhibitors of tyrosine kinases and uses thereof

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,625,880
App. No.
11/617,651
Granted
Dec 1, 2009
Kind
B2
Abstract

Disclosed herein are compounds that inhibit the activity of particular tyrosine kinases. Methods for the preparation of such compounds are disclosed. Also disclosed are pharmaceutical compositions that include the compounds. Methods of using the compounds disclosed, alone or in combination with other therapeutic agents, for the treatment of tyrosine kinase-mediated diseases or conditions or tyrosine kinase-dependent diseases or conditions are provided.

Claims (61)

1. A compound of Formula (III):

wherein:

R a and R b are each independently selected from among H, halogen, CN, NO 2 , C 1 -C 4 alkyl, C 1 -C 4 haloalkyl, and C 1 -C 4 alkoxy;

T is 1 ,6-dimethyl-9-oxo-8,9-dihydro- 1H-imidazo[4,5-h]isoquinolin-2,7-ylene, or 1,7-dimethyl-9-oxo-8,9-dihydro-1H-imidazo[4,5-h]isoquinolin-2,6-ylene;

L is —X 250a —Y 250 — or —Y 250 —X 250a —, wherein,

X 250a is a substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 1 -C 6 haloalkyl, substituted or unsubstituted C 3 -C 8 cycloalkyl, substituted or unsubstituted C 5 -C 8 cycloalkenyl, substituted or unsubstituted C 2 -C 6 alkenyl, substituted or unsubstituted C 2 -C 6 haloalkenyl, substituted or unsubstituted C 2 -C 6 alkynyl, or substituted or unsubstituted C 2 -C 6 haloalkynyl;

Y 250 is a bond, —O—, —S(═O)—, —S(═O) 2 —, —C(═O)—, —NR 45 —, —NH—, —NHC(═O)—, —NR 45 C(═O)—, —NR 45 C(═O)NR 45 —, —C(═O)NH—, —C(═O)NR 45 —, —OC(═O)—, —C(═O)O—, —NHSO 2 —, —NR 45 SO 2 —, —SO 2 NH—, —SO 2 NR 45 —, —C(R 45 )═NO—, —CH═NO—, —ON═CH—, aryl, —NHC(═O)O—, —OC(═O)NH—, —NR 45 C(═O)O—, or —OC(═O)NR 45 —;

where each R 45 is independently selected from among hydrogen, substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 3 -C 8 cycloalkyl, substituted or unsubstituted C 2 -C 6 alkenyl, substituted or unsubstituted C 2 -C 6 alkynyl;

M is N or CH;

W is

E is oxygen or sulfur;

R 100 is halogen, —OH, or an optionally substituted group selected from among C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, phenyl, C 1 -C 4 alkyl(phenyl), C 3 -Cycloalkyl, C 1 -C 4 alkyl(C 3 -C 8 cycloalkyl), C 2 -C 8 heterocycloalkyl, C 1 -C 4 alkyl(C 2 -C 8 heterocycloalkyl), C 1 -C 6 alkoxy, C 1 -C 6 alkenyloxy, C 1 -C 6 alkynyloxy, or —NR 102a R 102b ;

R 102a and R 102b are independently hydrogen, or an optionally substituted group selected from among C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, aryl, aralkyl, C 3 -C 8 cycloalkyl, C 1 -C 4 alkyl(C 3 -C 8 cycloalkyl), C 2 -C 8 heterocycloalkyl, and C 1 -C 4 alkyl(C 2 -C 8 heterocycloalkyl);

R 200 is an optionally substituted group selected from among C 2 -C 10 acyl, C 1 -C 6 alkylsulfonyl, C 2 -C 6 alkenylsulfonyl, arylsulfonyl, C 1 -C 10 alkoxycarbonyl, aminosulfonyl, C 1 -C 6 alkylaminosulfonyl,

R 350a is hydrogen, a substituted or unsubstituted C 1 -C 6 alkyl, a substituted or unsubstituted C 2 -C 6 alkenyl, a substituted or unsubstituted C 2 -C 6 alkynyl, a substituted or unsubstituted C 1 -C 6 haloalkyl, a substituted or unsubstituted C 2 -C 6 haloalkenyl, or a substituted or unsubstituted C 2 -C 6 haloalkynyl;

n is 1; or a

pharmaceutically acceptable salt or a pharmaceutically acceptable prodrug thereof.

2. The compound of claim 1 , wherein:

T is 1,6-dimethyl-9-oxo-8,9-dihydro-1H-imidazo[4,5-h]isoquinolin-2,7-ylene substituted at the 2 position with

and substituted at the 7 position with

3. The compound of claim 2 , wherein

Y 250 is a bond, —O—, —S(═O)—, —S(═O) 2 —, —C(═)—, —NH—, —NHC(═O)—, —NHC(═O)NH—, —C(═O)NH—, —OC(═O)—, —C(═O)O—, —NHSO 2 —, —SO 2 NH—, —NHC(═O)O—, or —OC(═O)NH—;

E is O; and

R 350a is hydrogen, a substituted or unsubstituted C 1 -C 6 alkyl, or a substituted or unsubstituted C 1 -C 6 haloalkyl.

4. The compound of claim 3 , wherein

X 250a is a substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 1 -C 6 haloalkyl, substituted or unsubstituted C 2 -C 6 alkenyl, substituted or unsubstituted C 2 -C 6 haloalkenyl, substituted or unsubstituted C 2 -C 6 alkynyl, or substituted or unsubstituted C 2 -C 6 haloalkynyl; and

n is 1.

5. The compound of claim 4 , wherein compound has a structure selected from among:

6. The compound of claim 5 , wherein:

R 100 is halogen, or an optionally substituted group selected from among C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, phenyl, C 1 -C 4 alkyl(phenyl), C 3 -C 8 cycloalkyl, C 1 -C 4 alkyl(C 3 -Cycloalkyl), C 2 -C 8 heterocycloalkyl, and C 1 -C 4 alkyl(C 2 -C 8 heterocycloalky);

R 200 is an optionally substituted group selected from among C 2 -C 10 acyl, C 1 -C 6 alkylsulfonyl, C 2 -C 6 alkenylsulfonyl, arylsulfonyl, C 1 -C 10 alkoxycarbonyl, aminosulfonyl, C 1 -C 6 alkylaminosulfonyl, and di(C 1 -C 6 alkyl)aminosulfonyl.

7. The compound of claim 6 , wherein:

R 350a is hydrogen;

Y 250 is a bond, —C(═O)—, —NHC(═O)—, —C(═O)NH—.

8. The compound of claim 7 , wherein L is selected from among:

9. The compound of claim 8 , wherein the compound has a structure of Formula (IIIc).

10. The compound of claim 9 , wherein:

L is C 1 -C 4 alkyl or

and

R 200 is an optionally substituted group selected from among C 2 -C 10 acyl, aryl, C 1 -C 6 alkylsulfonyl, C 2 -C 6 alkenylsulfonyl, arylsulfonyl, C 1 -C 10 alkoxycarbonyl, aminosulfonyl, C 1 -C 6 alkylaminosulfonyl, and di(C 1 -C 6 alkyl)aminosulfonyl.

11. The compound of claim 1 , wherein: T is 1,7-dimethyl-9-oxo-8,9-dihydro-1H-imidazo[4,5-h]isoquinolin-2,6-ylene substituted at the 2 position with

and substituted at the 6 position with

12. The compound of claim 11 , wherein

Y 250 is a bond, —O—, —S(═O)—, —S(═O) 2 —, —C(═O)—, —NH—, —NHC(═O)—, —NHC(═O)NH—, —C(═O)NH—, —OC(═O)—, —C(═O)O—, —NHSO 2 —, —SO 2 NH—, —NHC(═O)O—, or —OC(═O)NH—;

E is O; and

R 350a is hydrogen, or a substituted or unsubstituted C 1 -C 6 alkyl.

13. The compound of claim 12 , wherein

X 250a is a substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 1 -C 6 haloalkyl, substituted or unsubstituted C 2 -C 6 alkenyl, substituted or unsubstituted C 2 -C 6 haloalkenyl, substituted or unsubstituted C 2 -C 6 alkynyl, or substituted or unsubstituted C 2 -C 6 haloalkynyl; and

n is 1.

14. The compound of claim 13 , wherein compound has a structure selected from among:

15. The compound of claim 14 , wherein:

R 100 is halogen, or an optionally substituted group selected from among C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, phenyl, C 1 -C 4 alkyl(phenyl), C 3 -C 8 cycloalkyl, C 1 -C 4 alkyl(C 3 -C 8 cycloalkyl), C 2 -C 8 heterocycloalkyl, and C 1 -C 4 alkyl(C 2 -C 8 heterocycloalkyl);

R 200 is an optionally substituted group selected from among C 2 -C 10 acyl, C 1 -C 6 alkylsulfonyl, C 2 -C 6 alkenylsulfonyl, arylsulfonyl, C 1 -C 10 alkoxycarbonyl, aminosulfonyl, C 1 -C 6 alkylaminosulfonyl, and di(C 1 -C 6 alkyl)aminosulfonyl.

16. The compound of claim 15 , wherein:

R 350a is hydrogen;

Y 250 is —C(═O)—; and

X 250a is a substituted or unsubstituted C 1 -C 6 alkyl.

17. The compound of claim 16 , wherein L is

18. The compound of claim 17 , wherein the compound has a structure of Formula (IIIb).

19. A pharmaceutical composition comprising a therapeutically effective amount of a compound of claim 1 and a pharmaceutically acceptable excipient.

20. The pharmaceutical composition of claim 19 , wherein the composition is formulated for oral administration.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE CONVEYING PARTY DATA PREVIOUSLY RECORDED ON REEL 036130 FRAME 0254. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded May 18, 2016
From: OXFORD AMHERST CORPORATION; PHARMACYCLICS, INC.
To: PHARMACYCLICS, INC.
Reel/Frame 038742/0624 →
CORRECTIVE ASSIGNMENT TO CORRECT THE CONVEYING PARTY DATA PREVIOUSLY RECORDED ON REEL 036130 FRAME 0285. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER AND CHANGE OF NAME. Recorded May 18, 2016
From: PHARMACYCLICS, INC.; OXFORD AMHERST LLC
To: PHARMACYCLICS LLC
Reel/Frame 038742/0673 →
MERGER Recorded Jul 18, 2015
From: OXFORD AMHERST CORPORATION
To: PHARMACYCLICS, INC.
Reel/Frame 036130/0254 →
MERGER AND CHANGE OF NAME Recorded Jul 18, 2015
From: PHARMACYCLICS, INC.; OXFORD AMHERST LLC
To: PHARMACYCLICS LLC
Reel/Frame 036130/0285 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 22, 2007
From: JANKOWSKI, ORION D.; PALMER, JAMES T.; HONIGBERG, LEE
To: PHARMACYCLICS, INC.
Reel/Frame 019734/0535 →