Titanium alkoxide compound
View Patent ↗A titanium alkoxide composition is provided, as represented by the chemical formula (OC 6 H 5 N) 2 Ti(OC 6 H 5 NH 2 ) 2 . As prepared, the compound is a crystalline substance with a hexavalent titanium atom bonded to two OC 6 H 5 NH 2 groups and two OC 6 H 5 N groups with a theoretical molecular weight of 480.38, comprising 60.01% C, 5.04% H and 11.66% N.
1. A compound of the formula
2. The compound of claim 1 having a theoretical molecular weight of 480.38, comprising 60.01% C, 5.04% H and 11.66% N.
3. A crystalline compound comprising (OC 6 H 5 N) 2 Ti(OC 6 H 5 NH 2 ) 2 . (solvent), wherein (solvent) is a solvent adduct in the crystalline compound.
4. The crystalline compound of claim 3 wherein said solvent adduct is a Lewis base capable of supporting the solubilization of (OC 6 H 5 N) 2 Ti(OC 6 H 5 NH 2 ) 2 .
5. The crystalline compound of claim 4 wherein said solvent adduct results from an amine-based solvent.
6. The crystalline compound of claim 5 wherein said amine-based solvent is selected from the group consisting of pyridine, substituted pyridine compounds, aniline, substituted aniline compounds, alkyl amines and substituted alkyl amines.
7. The crystalline compound of claim 5 wherein said amine-based solvent is pyridine and the crystalline compound comprises (OC 6 H 5 N) 2 Ti(OC 6 H 5 NH 2 ) 2 . (C 5 H 5 N).
8. The crystalline compound of claim 7 wherein said crystalline compound has a molecular weight of 559.5.
9. The crystalline compound of claim 7 wherein the crystalline compound has an ortho-rhombic structure with unit cell dimensions of a=12.5716 Å, b=12.8307 Å and c=16.406 Å.