IP Library Granted Patent US 7,592,415
Granted Patent B2
US 7,592,415 · App. 11/640,625 · Granted Sep 22, 2009

Infrared solvent stripping process

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Quick Facts
Patent No.
US 7,592,415
App. No.
11/640,625
Granted
Sep 22, 2009
Kind
B2
Abstract

A process for stripping chemically bonded spinning solvent from a solution-spun nonwoven web comprising the steps of providing a nonwoven web comprising solvent-laden polymeric fibers having average fiber diameters of less than about 1 micrometer, and transporting the nonwoven web through a solvent stripping zone wherein infrared radiation irradiates the nonwoven web and a solvent stripping fluid impinges on the nonwoven web in order to reduce the solvent concentration of the fibers to less than about 10,000 ppmw.

Claims (17)

1. A process for stripping chemically bonded spinning solvent from a solution-spun nonwoven web comprising the steps of:

providing a nonwoven web comprising solvent-laden polymeric fibers having average fiber diameters of less than about 1 micrometer,

transporting the nonwoven web through a first zone in which a solvent stripping fluid impinges on the nonwoven web in order to reduce the solvent concentration of the fibers to less than about 10,000 ppmw, and

transporting the nonwoven web through a second zone wherein infrared radiation irradiates the nonwoven web and the bound solvent concentration is reduced to less than about 1000 ppmw.

2. The process according to claim 1 wherein the average fiber diameter is less than 0.8 micrometer.

3. The process according to claim 2 , wherein the average fiber diameter is less than 0.5 micrometer.

4. The process according to claim 1 , wherein the solvent stripping fluid is heated.

5. The process according to claim 4 , wherein the solvent stripping fluid is heated to between about 70° C. and the melting point of the fiber polymer.

6. The process according to claim 4 , wherein the solvent stripping fluid is heated to between about 70° C. and the decomposition point of the fiber polymer.

7. The process according to claim 1 , wherein the solvent stripping fluid is selected from the group of air, nitrogen, argon, helium, carbon dioxide, hydrocarbons, halocarbons, halohydrocarbons, and mixtures thereof.

8. The process according to claim 7 , wherein the solvent stripping fluid is air.

9. The process according to claim 1 , wherein the bound solvent concentration is reduced to less than 300 ppmw.

10. The process according to claim 1 , further comprising transporting the web through the solvent stripping zone by pinning the nonwoven web to a moving porous belt with a vacuum source located on the side of the porous belt opposite the nonwoven web, and passing fresh solvent stripping fluid through the web.

11. The process according to claim 1 , wherein the nonwoven web is transported through the solvent stripping zone on top of a scrim.

12. The process according to claim 1 , further comprising transporting the nonwoven web through at least one additional solvent stripping zone.

13. The process according to claim 12 , wherein the at least one additional solvent stripping zone wherein a solvent stripping fluid heated to at least about 70° C. impinges on the nonwoven web.

14. The process according to claim 13 , wherein the nonwoven web is transported through the at least one additional solvent stripping zone prior to the solvent stripping zone which includes the infrared radiation.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 25, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT SAFETY & CONSTRUCTION, INC.
Reel/Frame 049586/0001 →