IP Library Granted Patent US 8,206,627
Granted Patent B2
US 8,206,627 · App. 11/690,047 · Granted Jun 26, 2012

Systems and methods of making molded composite blocks

Assignee: 3M Innovative Properties Company
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Quick Facts
Patent No.
US 8,206,627
App. No.
11/690,047
Granted
Jun 26, 2012
Kind
B2
Abstract

Provided are filtration matrixes formed from adsorptive media, such as activated carbon, and polymeric binder for use in water filtration systems. A first aspect of the invention provides methods of making a filtration matrix comprising: mixing an adsorptive media with a polymeric binder to form a mixture; impulse filling a mold with the mixture; and processing the mixture to form the filtration matrix. Filtration matrixes formed from this method are also provided. Another aspect includes methods of making a filtration matrix comprising: mixing adsorptive media with a polymeric binder to form a mixture; filling a mold with the mixture; and applying heat and pressure the mixture to form the filtration matrix, wherein the step of applying pressure to the mixture comprises compressing the mixture until a desired final shape of the filtration matrix is obtained.

Claims (27)

1. A method of making a filtration matrix comprising:

mixing an adsorptive media with a polymeric binder to form a mixture, the adsorptive media comprising activated carbon suitable for the removal of contaminants from water;

impulse filling a mold with the mixture to an uncompressed density, impulse filling comprises administering impulses at a rate in the range of 6 to 120 impulses per minute; and

following impulse filling, heating and compressing the mixture to form the filtration matrix with a VOC capacity according to NSF-53 of 20 gal/in 3 or greater.

2. The method of claim 1 , wherein the rate is about 20 impulses per minute.

3. The method of claim 1 , wherein the mixture has a maximum uncompressed density, and the mixture after the mold is filled is at least 90% of the maximum uncompressed density.

4. The method of claim 3 , wherein the mixture after the mold is filled is at least 95% of the maximum uncompressed density.

5. The method of claim 1 , wherein heating comprises heating the mold to a temperature in the range of 160° C. to 250° C.

6. The method of claim 1 , further comprising providing a mold that is tapered to facilitate removal of the filtration matrix from the mold.

7. The method of claim 1 , wherein the adsorptive media further comprises a lead-removal media.

8. The method of claim 1 , wherein the binder comprises ultra high molecular weight polyethylene.

9. The method of claim 1 , wherein the impulse filling is used to fill a plurality of molds, and wherein a plurality of filtration matrixes is formed.

10. The method of claim 9 , wherein a standard deviation of the average weight of the plurality of filtration matrixes is no greater than 10% of the average weight.

11. The method of claim 10 , wherein the standard deviation is no greater than 5% of the average weight.

12. The method of claim 1 , wherein heating and compressing are done substantially simultaneously.

13. The method of claim 1 , wherein heating occurs before compressing.

14. The method of claim 1 , wherein compressing occurs before heating.

15. The method of claim 1 , wherein compressing comprises applying compressive force axially to the mixture.

16. The method of claim 1 , wherein the impulse filling comprises an indirect force on the mold such that the table to which the mold is secured receives a force directly.

17. A method of making a filtration matrix comprising:

mixing an adsorptive media with ultra high molecular weight polyethylene to form a mixture comprising the adsorptive media in an amount in the range of 65 to 90% by weight and ultra high molecular weight polyethylene in an amount in the range of 35 to 10% by weight, the adsorptive media comprising an activated carbon suitable for the removal of contaminants from water;

impulse filling a mold with the mixture to an uncompressed density, impulse filling comprises administering impulses at a rate in the range of 6 to 120 impulses per minute;

following impulse filling, heating the mold to a temperature in the range of 160° C. to 200° C.;

compressing the mixture until a fixed length of the filtration matrix is obtained; and

cooling the mold;

wherein the filtration matrix has a VOC capacity according to NSF-53 of 20 gal/in 3 or greater.

18. The method of claim 17 , wherein the impulse filling comprises an indirect force on the mold such that the table to which the mold is secured receives a force directly.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2024
From: 3M INNOVATIVE PROPERTIES COMPANY
To: SOLVENTUM INTELLECTUAL PROPERTIES COMPANY
Reel/Frame 066444/0535 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2007
From: STOUFFER, MARK R.; PRINCE, RICHARD A.; ASTLE, ROBERT E.
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 019163/0428 →
Continuity (2)
Provisional Application 60785397 · Mar 22, 2006
Related Publication 20070222101A1 · Sep 27, 2007