Purification of ionic liquids
The invention relates to a process for purifying an ionic liquid, which comprises the steps (a) partial crystallization of the ionic liquid from its melt and (b) separation of the crystals from the residual melt.
1. A process for purifying an ionic liquid, which comprises (a) partially crystallizing the ionic liquid from a melt of the ionic liquid until at least 5% by weight and not more than 90% by weight of the ionic liquid has crystallized out, and (b) separating the crystals crystallized out from a residual melt, wherein the crystals comprise at least 85% by weight of a purified ionic liquid.
2. The process according to claim 1 , wherein the partial crystallization is carried out discontinuously.
3. The process according to claim 1 , wherein the partial crystallization is carried out continuously.
4. The process according to claim 1 , wherein the partial crystallization is carried out statically or dynamically.
5. The process according to claim 4 , wherein the partial crystallization is carried out as a layer or suspension crystallization.
6. The process according to claim 1 , wherein the partial crystallization is carried out in a plurality of stages.
7. The process according to claim 6 , wherein the partial crystallization is carried out as a countercurrent crystallization.
8. The process according to claim 1 , wherein the partial crystallization is carried out as a zone melting process.