IP Library Granted Patent US 7,709,690
Granted Patent B2
US 7,709,690 · App. 11/721,742 · Granted May 4, 2010

Method for producing tertiary butyl alcohol

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Quick Facts
Patent No.
US 7,709,690
App. No.
11/721,742
Granted
May 4, 2010
Kind
B2
Abstract

Disclosed is a method for producing tertiary butyl alcohol through hydration reaction of isobutylene and water in the presence of a cation exchange resin by using a reactor having at least two reactor vessels provided in series. The method is characterized in that a fluid in a reactor vessel at the most downstream side forms a two-liquid phase and the reaction temperature of the reactor vessel is kept at 70° C. or lower, and a fluid in at least one reactor vessel other than the one at the most downstream side forms a homogeneous phase.

Claims (5)

1. A method for producing tertiary butyl alcohol through hydration reaction of isobutylene and water in the presence of a cation exchange resin by using a reactor having at least two reactor vessels provided in series, comprising:

making a fluid in a reactor vessel at the most downstream side form a two-liquid phase while keeping a reaction temperature of the reactor vessel at 70° C. or lower; and

making a fluid in at least one reactor vessel other than the reactor vessel at the most downstream side form a homogeneous phase.

2. The method for producing tertiary butyl alcohol of claim 1 , wherein fluids in all the reactor vessels other than the reactor vessel at the most downstream side are homogeneous phases.

3. The method for producing tertiary butyl alcohol of claim 1 or 2 , wherein a part of the tertiary butyl alcohol is removed from a reaction liquid taken out from an outlet of a reactor vessel located upstream by one from the reactor vessel at the most downstream side and the resultant reaction liquid in which a part of the tertiary butyl alcohol has been removed is supplied to the reactor vessel at the most downstream side.

Assignments (2)
CHANGE OF NAME Recorded Sep 5, 2017
From: MITSUBISHI RAYON CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 043750/0834 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 18, 2007
From: ENDOH, TOHRU; TANAKA, SHIGEHO; SATO, HARUKI
To: MITSUBISHI RAYON CO., LTD.
Reel/Frame 019980/0489 →