IP Library Granted Patent US 7,897,624
Granted Patent B2
US 7,897,624 · App. 11/737,109 · Granted Mar 1, 2011

Pyridone sulfonamides and pyridone sulfamides as MEK inhibitors

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Quick Facts
Patent No.
US 7,897,624
App. No.
11/737,109
Granted
Mar 1, 2011
Kind
B2
Abstract

This invention concerns N-(ortho phenylamino dihydropyridyl)sulfonamides and N-(ortho phenylamino dihydropyridyl), N′-alkyl sulfamides which are inhibitors of MEK and are useful in the treatment of cancer and other hyperproliferative diseases.

Claims (40)

1. A compound of formula I, or a pharmaceutically acceptable salt or tautomer thereof:

wherein

B is H, C 1 -C 6 alkyl or C 2 -C 6 alkenyl;

wherein said C 1 -C 6 alkyl is optionally substituted with one or two groups independently selected from the group consisting of hydroxy, alkoxy, and oxy;

A and A′ are each independently H, C 1 -C 6 alkyl, or C 2 -C 6 alkenyl;

wherein each C 1 -C 6 alkyl is optionally substituted with one or two groups independently selected from the group consisting of hydroxy, alkoxy, and oxy; or

A and A′ together with the carbon atom to which they are attached, form a cyclopropyl, cyclobutyl, or cyclopentyl group,

wherein each cyclopropyl, cyclobutyl, or cyclopentyl group is optionally substituted with one or two groups independently selected from the group consisting of methyl, hydroxy, and halogen;

X and Y are each independently halogen, methyl, SCH 3 or trifluoromethyl;

R 1 is H, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl;

wherein each alkyl, cycloalkyl, alkenyl, cycloalkenyl or alkynyl group is optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alky, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl difluoromethoxy and phenyl; and

R 2 is H, halogen, hydroxy, azido, cyano, cyanomethy, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl, wherein each alkyl, cycloalkyl, alkenyl cycloalkenyl or alkynyl group is optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl and phenyl.

2. The compound of claim 1 , where X and Y are both halogen.

3. The compound of claim 2 , where X is F and Y is Br or I.

4. The compound of claim 1 , where one or both of X and Y are methyl, SCH 3 or trifluoromethyl.

5. The compound of claim 1 , where A and A′ together with the carbon atom to which they are attached, form a cyclopropyl, cyclobutyl, or cyclopentyl group, wherein each cyclopropyl, cyclobutyl, or cyclopentyl group is optionally substituted with one or two groups independently selected from the group consisting of methyl, hydroxy, and halogen.

6. The compound of claim 5 , where R 1 is H, C 1 -C 6 alkyl, or C 3 -C 6 cycloalkyl.

7. The compound of claim 6 , where R 2 is H, halogen, or C 1 -C 3 alkyl.

8. The compound of claim 1 , where R 1 is C 2 -C 6 alkenyl or C 2 -C 6 alkynyl, optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alky, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl difluoromethoxy and phenyl.

9. The compound of claim 5 , where R 1 is C 2 -C 6 alkenyl or C 2 -C 6 alkynyl, optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alky, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl difluoromethoxy and phenyl.

10. The compound of claim 1 , where B is C 1 -C 6 alkyl, unsubstituted or substituted with one or two hydroxy groups.

11. The compound of claim 5 , where B is C 1 -C 6 alkyl, unsubstituted or substituted with one or two hydroxy groups.

12. A compound selected from the group consisting of:

13. A pharmaceutical composition comprising a compound of formula I of claim 1 and a pharmaceutically acceptable carrier.

14. The composition of claim 13 wherein said compound of formula I is selected from the group consisting of:

15. A pharmaceutically acceptable salt of a compound of formula I of claim 1 .

16. A compound of formula I, or a pharmaceutically acceptable salt or tautomer thereof:

wherein

B is H, C 1 -C 6 alkyl or C 2 -C 6 alkenyl;

wherein said C 1 -C 6 alkyl is optionally substituted with one or two groups independently selected from the group consisting of hydroxy, alkoxy, oxy, ethylamine, diethylamine, ethylenediamine, ethanolamine, diethanolamine and piperazine;

A and A′ are each independently H, C 1 -C 6 alkyl, or C 2 -C 6 alkenyl;

wherein each C 1 -C 6 alkyl is optionally substituted with one or two groups independently selected from the group consisting of hydroxy, alkoxy, and oxy, ethylamine, diethylamine, ethylenediamine, ethanolamine, diethanolamine and piperazine; or

A and A′ together with the carbon atom to which they are attached, form a cyclopropyl, cyclobutyl, or cyclopentyl group,

wherein each cyclopropyl, cyclobutyl, or cyclopentyl group is optionally substituted with one or two groups independently selected from the group consisting of methyl, hydroxy, and halogen;

X and Y are each independently halogen, methyl, SCH 3 or trifluoromethyl;

R 1 is H, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl;

wherein each alkyl, cycloalkyl, alkenyl, cycloalkenyl or alkynyl group is optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alky, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl difluoromethoxy and phenyl; and

R 2 is H, halogen, hydroxy, azido, cyano, cyanomethy, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl, wherein each alkyl, cycloalkyl, alkenyl cycloalkenyl or alkynyl group is optionally substituted with 1-3 substituents independently selected from the group consisting of halogen, hydroxy, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl and phenyl.

17. A pharmaceutically acceptable salt of a compound of formula I of claim 16 .

18. A pharmaceutical composition comprising a compound of formula I of claim 16 and a pharmaceutically acceptable carrier.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Apr 8, 2025
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: SOLTA MEDICAL, INC.; PRECISION DERMATOLOGY, INC.; BAUSCH HEALTH IRELAND LIMITED (F/K/A/ VALEANT PHARMACEUTICALS IRELAND LIMITED); SALIX PHARMACEUTICALS, INC.; SALIX PHARMACEUTICALS, LTD; SANTARUS, INC.; MEDICIS PHARMACEUTICAL CORPORATION; HUMAX PHARMACEUTICAL S.A.; SOLTA MEDICAL IRELAND LIMITED; BAUSCH & LOMB MEXICO, S.A. DE C.V.; BAUSCH+LOMB OPS B.V.; BAUSCH HEALTH AMERICAS, INC.; BAUSCH HEALTH COMPANIES INC.; BAUSCH HEALTH HOLDCO LIMITED; BAUSCH HEALTH MAGYARORSZAG KFT (A/K/A BAUSCH HEALTH HUNGARY LLC); BAUSCH HEALTH POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA (F/K/A VALEANT PHARMA POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA); BAUSCH HEALTH US, LLC; BAUSCH HEALTH, CANADA INC. / SANTE BAUSCH, CANADA INC.; ICN POLFA RZESZOW SPOLKA AKCYJNA (A/K/A ICN POLFA RZESZOW S.A.); ORAPHARMA, INC.; PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA SPOLKA AKCYJNA (A/K/A PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA S.A.); SOLTA MEDICAL DUTCH HOLDINGS B.V.; V-BAC HOLDING CORP.; VRX HOLDCO LLC; 1261229 B.C. LTD.; 1530065 B.C. LTD.
Reel/Frame 070778/0199 →
NOTICE OF SUCCESSION OF AGENCY Recorded Jan 9, 2015
From: GOLDMAN SACHS LENDING PARTNERS, LLC
To: BARCLAYS BANK PLC, AS SUCCESSOR AGENT
Reel/Frame 034749/0689 →
CORRECTIVE PARTIAL RELEASE OF SECURITY INTEREST IN PATENTS Recorded Oct 12, 2011
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: VALEANT PHARMACEUTICALS INTERNATIONAL; ATON PHARMA, INC.; CORIA LABORATORIES, LTD.; DOW PHARMACEUTICAL SCIENCES; VALEANT PHARMACEUTICALS NORTH AMERICA LLC,; PRESTWICK PHARMACEUTICALS, INC.; VALEANT BIOMEDICALS, INC.
Reel/Frame 027052/0883 →
SECURITY AGREEMENT Recorded Jul 18, 2011
From: VALEANT PHARMACEUTICALS INTERNATIONAL, A DELAWARE CORPORATION; ATON PHARMA, INC., A DELAWARE CORPORATION; CORIA LABORATORIES, LTD., A DELAWARE CORPORATION; DOW PHARMACEUTICAL SCIENCES, INC., A DELAWARE CORPORATION; VALEANT PHARMACEUTICALS NORTH AMERICA LLC, A DELAWARE LLC; PRESTWICK PHARMACEUTICALS, INC., A DELAWARE CORPORATION; VALEANT BIOMEDICALS, INC., A DELAWARE CORPORATION
To: GOLDMAN SACHS LENDING PARTNERS LLC, AS COLLATERAL AGENT
Reel/Frame 026606/0061 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2007
From: YAN, SHUNQI; VERNIER, JEAN-MICHEL; HONG, ZHI; CHOW, SUETYING; KOH, YUNG-HYO
To: ARDEA BIOSCIENCES
Reel/Frame 019340/0781 →