IP Library Granted Patent US 8,470,981
Granted Patent B2
US 8,470,981 · App. 11/770,973 · Granted Jun 25, 2013

Additives for the improved dewatering of corn gluten

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Quick Facts
Patent No.
US 8,470,981
App. No.
11/770,973
Granted
Jun 25, 2013
Kind
B2
Abstract

The invention relates to a method of dewatering corn gluten stream wherein coagulant is add to the corn gluten stream of the corn wet milling process. The method of dewatering corn gluten uses an effective amount of a coagulant of one or more anionic polymers, the anionic polymers comprising one or more anionic monomers. The method further includes a process for separating the water from the gluten using a solids/liquids filtration device.

Claims (24)

1. A method of dewatering a corn gluten stream, the method comprising:

(i) Adding to the corn gluten stream comprised of water and corn gluten of a corn wet milling process an effective amount of a coagulant comprising at least one anionic polymer of sodium acrylate; and

(ii) Separating the water from the corn gluten using a solids/liquids filtration device.

2. The method of claim 1 wherein the anionic polymer is a homopolymer of sodium acrylate.

3. The method of claim 1 wherein the anionic polymer is a copolymer with at least one monomer selected from sodium (Meth)acrylate, acrylamido-propylsulfonic acid sodium salt, acrylamide, methacrylamide, N-methylacrylamide, N,N-dimethyl acrylamide, vinylpyrolidone, N-vinylformamide, and hydroxyethylacrylate.

4. The method of claim 1 wherein the anionic polymer comprises at least one monomer selected from the group consisting of acrylic acid and acrylamide.

5. The method of claim 1 wherein the anionic polymer has an anionic charge of about 70 to 100 mole percent.

6. The method of claim 1 wherein the anionic polymer has an anionic charge of about 95 to 100 mole percent.

7. The method of claim 1 wherein the anionic polymer has an intrinsic viscosity of about 0.2 dL/g to 5.0 dL/g.

8. The method of claim 1 wherein the coagulant further comprises one or more cross linking agents.

9. The method of claim 8 wherein the cross linking agents are selected from any combination of methylene-bis acrylamide, diglycidal ethers and diacrylate esters.

10. The method of claim 1 wherein the anionic polymer has a reduced specific viscosity of about 0.2 dL/g to 6.0 dL/g.

11. The method of claim 1 wherein about 50 to 1000 ppm of the coagulant is added to the corn gluten stream of the corn wet milling process.

12. The method of claim 1 comprising adding the coagulant in the corn gluten stream of the corn wet milling process simultaneously as the corn gluten stream is being sent to the solids/liquids filtration device.

13. The method of claim 12 wherein the coagulant is added before the addition of the corn gluten stream of the corn wet milling process to the solids/liquids filtration device.

14. The method of claim 1 wherein the solids/liquids filtration device uses pneumatic pressure.

15. The method of claim 1 wherein the solids/liquids filtration device uses hydraulic pressure in the system.

16. The method of claim 1 wherein the solids/liquids filtration device is used to treat a heavy gluten component of the corn gluten stream of the corn wet milling process.

17. The method of claim 1 wherein the solids/liquids filtration device is a rotary drum vacuum filter.

18. The method of claim 1 wherein the solids/liquids filtration device is a vacuum table filter.

19. The method of claim 1 wherein the solids/liquids filtration device is a pressure filtration system.

20. The method of claim 19 wherein the pressure filtration system is a recess chamber press.

21. The method of claim 19 wherein the pressure filtration system is a plate and frame press.

22. The method of claim 1 wherein the anionic polymer is a copolymer.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 4, 2017
From: NALCO COMPANY
To: ECOLAB USA INC.
Reel/Frame 042147/0420 →
CHANGE OF NAME Recorded Feb 28, 2017
From: NALCO COMPANY
To: NALCO COMPANY LLC
Reel/Frame 041835/0903 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2017
From: NALCO COMPANY LLC; CALGON CORPORATION; CALGON LLC; ONDEO NALCO ENERGY SERVICES, L.P.
To: ECOLAB USA INC.
Reel/Frame 041836/0437 →
RELEASE OF SECURITY INTEREST Recorded Feb 24, 2017
From: BANK OF AMERICA, N.A.
To: NALCO COMPANY
Reel/Frame 041808/0713 →