Smokeless tobacco composition
View Patent ↗The invention provides a process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, the process including: providing a slurry comprising water and a tobacco material, the slurry comprising at least about 75% by weight water, based on the total weight of the slurry; heating the slurry to a temperature of at least about 60° C. for a time sufficient to pasteurize the tobacco material; adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 8.5, thereby forming a pH-adjusted slurry; and continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following the adding step.
1. A process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, comprising:
providing a slurry comprising water and a tobacco material, the slurry comprising at least about 75% by weight water, based on the total weight of the slurry;
heating the slurry to a temperature of at least about 60° C. for a time sufficient to pasteurize the tobacco material;
adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 8.5, thereby forming a pH-adjusted slurry; and
continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following said adding step.
2. The process of claim 1 , further comprising the step of adding a salt to the slurry prior to said heating step.
3. The process of claim 2 , wherein said salt addition step comprises adding about 1 to about 5% by weight of a sodium chloride, based on the dry weight of the tobacco material.
4. The process of claim 1 , further comprising cooling the slurry to a temperature of less than about 35° C.
5. The process of claim 4 , further comprising the step of adding a humectant during or following said cooling step.
6. The process of claim 1 , further comprising the step of drying the slurry to a moisture content of no more than about 15% by weight, based on the total weight of the dried tobacco material.
7. The process of claim 6 , further comprising the step of adding one or more flavorants and additional moisture to the dried tobacco material in an amount sufficient to raise the moisture content of the tobacco material to at least about 25% by weight.
8. The process of claim 1 , wherein said step of providing a slurry comprises providing a slurry having a water content of at least about 80% by weight of the slurry.
9. The process of claim 8 , wherein the water content of the slurry is about 80 to about 95% by weight.
10. The process of claim 1 , wherein said slurry heating step comprises heating the slurry to a temperature of at least about 70° C. for at least about 30 minutes.
11. The process of claim 1 , wherein said step of continuing to heat the pH-adjusted slurry comprises heating the pH-adjusted slurry for at least about 1.5 hours.
12. The process of claim 1 , wherein said adding step comprises adding sufficient base to raise the pH of the slurry to at least about 9.
13. The process of claim 1 , wherein the base is selected from the group consisting of alkali metal hydroxides, alkali metal carbonates, alkali metal bicarbonates, and mixtures thereof.
14. The process of claim 13 , wherein the base is selected from the group consisting of sodium carbonate, potassium carbonate, sodium bicarbonate, potassium bicarbonate, sodium hydroxide, potassium hydroxide, and mixtures thereof.
15. The process of claim 1 , wherein the rate of pH reduction is maintained at about 0.05 to about 0.15 pH units per hour following said adding step.
16. The process of claim 15 , wherein the rate of pH reduction is maintained at about 0.08 to about 0.10 pH units per hour following said adding step.
17. A process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, comprising:
providing a slurry comprising water and a tobacco material, the slurry comprising at least about 80% by weight water, based on the total weight of the slurry;
heating the slurry to a temperature of at least about 70° C. for a time sufficient to pasteurize the tobacco material;
adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 9, thereby forming a pH-adjusted slurry;
continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for a time sufficient for the pH of the slurry to drop at least about 0.5 pH unit following said adding step; and
cooling the pH-adjusted slurry to about ambient temperature, the pH-adjusted slurry having a pH of at least about 8 at the time the cooling step begins.
18. A process for preparing a tobacco composition suitable for use as a smokeless tobacco composition, comprising:
providing a slurry comprising water and a tobacco material, the slurry comprising at least about 80% by weight water, based on the total weight of the slurry;
heating the slurry to a temperature of at least about 70° C. for at least about 30 minutes;
adding an amount of a base to the slurry sufficient to raise the pH of the slurry to at least about 9.5, thereby forming a pH-adjusted slurry;
continuing to heat the pH-adjusted slurry to a temperature of at least about 60° C. for at least about 1.5 hours;
cooling the pH-adjusted slurry to about ambient temperature, the pH-adjusted slurry having a pH of at least about 8 at the time the cooling step begins;
adding a humectant to the pH-adjusted slurry during or after said cooling step; and
drying the pH-adjusted slurry at a temperature and for a time sufficient to decrease the moisture level of the tobacco material to less than about 15% by weight, based on the weight of the moist tobacco material.