IP Library Granted Patent US 7,678,796
Granted Patent B2
US 7,678,796 · App. 11/790,417 · Granted Mar 16, 2010

MGluR5 modulators I

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Quick Facts
Patent No.
US 7,678,796
App. No.
11/790,417
Granted
Mar 16, 2010
Kind
B2
Abstract

The present invention is directed to novel compounds, to a process for their preparation, their use in therapy and pharmaceutical compositions comprising the novel compounds.

Claims (68)

1. A compound of formula (I)

wherein

R 1 is methyl, halogen or cyano;

R 2 is hydrogen or fluoro;

R 3 is hydrogen, fluoro or C 1 -C 3 alkyl;

R 4 is C 1 -C 3 alkyl or cyclopropyl;

Y is a bond;

X is

and Z is

wherein

R 5 is hydrogen, C 1 -C 3 alkyl, C 1 -C 3 haloalkyl, C 1 -C 3 alkoxy; C 1 -C 3 haloalkoxy; or halogen;

R 6 is hydrogen, C 1 -C 3 alkyl, C 1 -C 3 haloalkyl, C 1 -C 3 alkoxy; C 1 -C 3 haloalkoxy; or halogen;

R 7 is hydrogen, fluoro or C 1 -C 3 alkyl;

as well as pharmaceutically acceptable salts, tautomers and/or enantiomers thereof.

2. A compound according to claim 1 , wherein R 1 is halogen or cyano.

3. A compound according to claim 2 , wherein R 1 is chloro.

4. A compound according to claim 2 , wherein R 1 is fluoro.

5. A compound according to claim 2 , wherein R 1 is methyl.

6. A compound according to claim 2 , wherein R 1 is cyano.

7. A compound according to claim 1 , wherein R 2 is hydrogen.

8. A compound according to claim 1 , wherein R 3 is hydrogen or fluoro.

9. A compound according to claim 1 , wherein R 4 is C 1 -C 2 alkyl.

10. A compound according to claim 9 , wherein R 4 is methyl.

11. A compound according to claim 1 , wherein R 5 is hydrogen, C 1 -C 2 alkyl or C 1 -C 2 alkoxy.

12. A compound according to claim 1 , wherein R 6 is hydrogen, C 1 -C 2 alkyl or C 1 -C 2 alkoxy.

13. A compound according to claim 1 , wherein R 7 is hydrogen or fluoro.

14. A compound according to claim 1 , wherein Z is

15. A compound according to claim 14 , wherein Z is

16. A compound according to claim 14 , wherein Z is

17. A compound according to claim 14 , wherein Z is

18. A compound selected from;

3-{3-[(R)-1-(4-Methyl-5-pyrimidin-5-yl-4H-[1,2,4]triazol-3-yl)-pyrrolidin-2-yl]-isoxazol-5-yl}-benzonitrile;

3-{5-[(R)-1-(4-Methyl-5-pyrazin-2-yl-4H-[1,2,4]triazol-3-yl)-pyrrolidin-2-yl]-tetrazol-2-yl}-benzonitrile;

3-{3-[(R)-1-(4-Methyl-5-pyrazin-2-yl-4H-[1,2,4]triazol-3-yl)-pyrrolidin-2-yl]-isoxazol-5-yl}-benzonitrile;

5-(5-{(R)-2-[2-(3-Chloro-phenyl)-2H-tetrazol-5-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-pyrimidine;

4-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1-methyl-1H-pyridin-2-one;

5-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1-methyl-1H-pyridin-2-one;

4-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-pyridazine;

(+/−)5-(5-{2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-pyrimidine;

2-(5-{(S)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-pyrazine;

4-(5-{(R)-2-[2-(3-Chloro-phenyl)-2H-tetrazol-5-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1-methyl-1H-pyridin-2-one;

4-(5-{(R)-2-[2-(3-Chloro-phenyl)-2H-tetrazol-5-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one;

4-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one;

6-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2-methyl-2H-pyridazin-3-one;

5-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2H-pyridazin-3-one;

5-(5-{(R)-2-[5-(3-Fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2H-pyridazin-3-one;

6-(5-{(R)-2-[5-(3-Fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2-methyl-2H-pyridazin-3-one;

1-Methyl-4-{4-methyl-5-[(R)-2-(5-m-tolylisoxazol-3-yl)pyrrolidin-1-yl]-4H-[1,2,4]triazol-3-yl}-1H-pyridin-2-one;

5-{4-Methyl-5-[(R)-2-(5-m-tolyl-isoxazol-3-yl)-pyrrolidin-1-yl]-4H-[1,2,4]triazol-3-yl}-2H-pyridazin-3-one;

4-(5-{(R)-2-[5-(3-Fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one;

2-Methyl-5-{4-methyl-5-[(R)-2-(5-m-tolyl-isoxazol-3-yl)-pyrrolidin-1-yl]-4H-[1,2,4]triazol-3-yl}-2H-pyridazin-3-one;

4-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1,6-dimethyl-1H-pyridin-2-one;

4-{4-Methyl-5-[(R)-2-(5-m-tolyl-isoxazol-3-yl)-pyrrolidin-1-yl]-4H-[1,2,4]triazol-3-yl}-1H-pyridin-2-one;

6-{4-Methyl-5-[(R)-2-(5-m-tolyl-isoxazol-3-yl)-pyrrolidin-1-yl]-4H-[1,2,4]triazol-3-yl}-3H-pyrimidin-4-one;

4-(5-{(R)-2-[2-(3-Chloro-phenyl)-2H-tetrazol-5-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-pyridazine;

5-(5-{(R)-2-[5-(3-Chlorophenyl)isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2-methyl-2H-pyridazin-3-one;

5-(5-{(R)-2-[5-(3-Fluorophenyl)isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2-methyl-2H-pyridazin-3-one;

6-(5-{(R)-2-[5-(3-Chlorophenyl)isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-3H-pyrimidin-4-one;

6-(5-{(R)-2-[5-(3-Chloro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one

5-(5-{(R)-2-[5-(2,5-Difluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2H-pyridazin-3-one;

6-(5-{(R)-2-[5-(5-Chloro-2-fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-1,2,4-triazol-3-yl)-3H-pyrimidin-4-one;

4-(5-{(R)-2-[5-(5-Chloro-2-fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one;

5-(5-{(R)-2-[5-(5-Chloro-2-fluoro-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-2H-pyridazin-3-one;

4-(5-{(R)-2-[5-(2-Fluoro-5-methyl-phenyl)-isoxazol-3-yl]-pyrrolidin-1-yl}-4-methyl-4H-[1,2,4]triazol-3-yl)-1H-pyridin-2-one; and

as well as pharmaceutically acceptable salts, tautomers and/or enantiomers thereof.

19. A pharmaceutical composition comprising a compound according to claim 1 as an active ingredient, together with a pharmacologically and pharmaceutically acceptable carrier.

20. A combination comprising (i) at least one compound according to claim 1 and (ii) at least one acid secretion inhibiting agent.

21. A combination according to claim 20 wherein the acid secretion inhibiting agent is selected from cimetidine, ranitidine, omeprazole, esomeprazole, lansoprazole, pantoprazole, rabeprazole or leminoprazole.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2007
From: NPS PHARMACEUTICALS, INC.; ASTRAZENECA AB
To: ASTRAZENECA AB
Reel/Frame 020045/0150 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 13, 2007
From: WALLBERG, ANDREAS; NILSSON, KAROLINA; HOLM, BJORN; NAGARD, MATS; GRANBERG, KENNETH; SLASSI, ABDELMALIK; EDWARDS, LOUISE; ISAAC, METHVIN; XIN, TAO; STEFANAC, TOMISLAV
To: ASTRAZENECA AB; NPS PHARMACEUTICALS, INC.
Reel/Frame 019423/0612 →