IP Library Granted Patent US 7,919,439
Granted Patent B2
US 7,919,439 · App. 11/798,950 · Granted Apr 5, 2011

Powdered lubricant composition for hot working and method for manufacturing seamless tubes

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Quick Facts
Patent No.
US 7,919,439
App. No.
11/798,950
Granted
Apr 5, 2011
Kind
B2
Abstract

With a powdered lubricant composition by the invention, in addition to the blending of one of anhydrous, pentahydrate or decahydrate salt in sodium borate and one of sodium or calcium salt of fat acid, mixing calcium or lithium carbonate as an auxiliary lubricant can prevent sodium borate (Na 2 B 4 O 7 ), solidified as amorphous after a tube-making process, from moisture absorbance, drying and crystallization to thereby suppress the formation of Na 2 B 4 O 7 .5H 2 O on inside surfaces of finished-product tubes, thus enabling to circumvent occurrence of the white scales. Concurrently, they provide good diffusivity toward the working surface of workpiece, thus enabling to prolong a life of the mandrel bar and to widely be adopted as the most suitable powdered lubricant for manufacturing seamless tubes by Mandrel Mill rolling.

Claims (29)

1. A powdered lubricant composition for hot working which is used in hot working, comprising a blend of:

a first group consisting of one or more components selected from the group consisting of anhydrous sodium borate, sodium borate pentahydrate and sodium borate decahydrate, the first group accounting for 40-90 mass %;

a second component selected from the group consisting of calcium carbonate, lithium carbonate, and mixtures thereof, the second component accounting for 5-30 mass % of said composition; and

a third component selected from the group consisting of sodium salt of fat acid, calcium salt of fat acid, and mixtures thereof, the third component accounting for 5-30 mass % of said composition;

wherein sodium carbonate is not included as an auxiliary lubricant.

2. The powdered lubricant composition for hot working which is used in hot working according to claim 1 , wherein said sodium borate pentahydrate is blended such that it accounts for 40-90 mass %.

3. A method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 1 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

4. The method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 2 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

5. The method for manufacturing seamless tubes according to claim 3 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

6. The method for manufacturing seamless tubes according to claim 4 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

7. A powdered lubricant composition for hot working which is used in hot working, comprising a blend of:

a first group consisting of one or more components selected from the group consisting of anhydrous sodium borate, sodium borate penta hydrate and sodium borate decahydrate, the first group accounting for 40-90 mass %;

a second component selected from the group consisting of calcium carbonate, lithium carbonate, and mixtures thereof, the second component accounting for 5-30 mass % of said composition

a third component selected from the group consisting of sodium salt of fat acid, calcium salt of fat acid, and mixtures thereof, the third component accounting for 5-30 mass % of said composition

wherein the inside surface of the product tube finished by mandrel mill rolling is free of white scales.

8. The powdered lubricant composition for hot working which is used in hot working according to claim 7 , wherein said sodium borate pentahydrate is blended such that it accounts for 40-90 mass.

9. A method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 7 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

10. The method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 8 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

11. The method for manufacturing seamless tubes according to claim 9 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

12. The method for manufacturing seamless tubes according to claim 10 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

13. A powdered lubricant composition for hot working which is used in hot working, consisting of a blend of:

a first group consisting of one or more components selected from the group consisting of anhydrous sodium borate, sodium borate penta hydrate and sodium borate decahydrate, the first group accounting for 40-90 mass %;

a second component selected from the group consisting of calcium carbonate, lithium carbonate, and mixtures thereof, the second component accounting for 5-30 mass % of said composition

a third component selected from the group consisting of sodium salt of fat acid, calcium salt of fat acid, and mixtures thereof, the third component accounting for 5-30 mass % of said composition.

14. The powdered lubricant composition for hot working which is used in hot working according to claim 13 , wherein said sodium borate pentahydrate is blended such that it accounts for 40-90 mass %.

15. A method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 13 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

16. The method for manufacturing seamless tubes, wherein a mandrel mill rolling process is applied after the powdered lubricant having the composition according to claim 14 is supplied on the working surface of workpiece that is heated to a predetermined hot working temperature.

17. The method for manufacturing seamless tubes according to claim 15 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

18. The method for manufacturing seamless tubes according to claim 16 , wherein said predetermined hot working temperature is set in the range of 1000 to 1300° C.

Assignments (3)
MERGER Recorded May 14, 2019
From: SUMITOMO METAL INDUSTRIES, LTD.
To: NIPPON STEEL & SUMITOMO METAL CORPORATION
Reel/Frame 049165/0517 →
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2008
From: SASAKI, KENICHI; IIDA, SUMIO; MORI, SHIZUO; ITO, ATSUSHI
To: SUMITOMO METAL INDUSTRIES, LTD.
Reel/Frame 020693/0799 →