Vaporization of thermally sensitive materials
View Patent ↗A vaporizer for receiving and vaporizing particulate material, comprising: a heater having a reticulated material structure composed of ligands that define voids adapted to receive particulate materials, wherein the voids comprise greater than 85% of the volume of the reticulated material structure so that delivery of particulate material into the voids and conduction of vaporized material from the voids is facilitated; causes heat to be produced or conducted by the ligands to cause the particulate material in the voids to vaporize and be conducted through the voids.
1. A vaporizing system for vaporizing particulate material, comprising:
(a) a source of particulate material;
(b) a heater having a reticulated material structure composed of ligands that define voids adapted to receive particulate materials, wherein the voids comprise greater than 85% of the volume of the reticulated material structure so that delivery of particulate material into the voids and conduction of vaporized material from the voids is facilitated;
(c) a manifold positioned to receive vaporized material produced by the heater;
(d) means for delivering the particulate material to the heater by gravity for causing such material to be disposed in the voids; and
(e) means for causing heat to be produced or conducted by the ligands to cause the particulate material in the voids to vaporize and be delivered to the manifold;
wherein the heater is set at an angle of 30 to 70 degrees relative to horizontal.
2. The vaporizing system of claim 1 wherein the reticulated material structure is electrically conductive and the heat-causing means causes current to flow through the ligands to cause heat to be produced.
3. The vaporizing system of claim 2 wherein the reticulated material structure includes vitreous carbon.
4. The vaporizing system of claim 2 wherein the reticulated material structure includes vitreous carbon and a conformal coating of a refractory metal or conductive ceramic on the ligands.
5. The vaporizing system of claim 4 wherein the refractory metal includes tungsten, tantalum, or molybdenum.
6. The vaporizing system of claim 4 wherein the conductive ceramic includes silicon carbide.
7. The vaporizing system of claim 1 wherein each void has an effective diameter equal to or greater than the effective diameter of the particulate material.
8. The vaporizing system of claim 7 wherein each void has an effective diameter greater than two times the effective diameter of the particulate material.
9. The vaporizing system of claim 1 wherein the average residence time of the particulate material in the reticulated material structure is less than 2 seconds.
10. The vaporizing system of claim 1 wherein the particulate material is selected to change from a solid to a vapor state, or through a liquid state before vaporizing.
11. The vaporizing system of claim 1 wherein the reticulated material structure is vibrated.
12. The vaporizing system of claim 1 wherein the heat-causing means is a separate heating element.
13. The vaporizing system of claim 1 further including means to cool the particulate material before it reaches the reticulated material structure.