IP Library Granted Patent US 8,168,037
Granted Patent B2
US 8,168,037 · App. 11/856,150 · Granted May 1, 2012

Method and systems for enhancing oil recovery from ethanol production byproducts

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Quick Facts
Patent No.
US 8,168,037
App. No.
11/856,150
Granted
May 1, 2012
Kind
B2
Abstract

Methods and related systems efficiently and effectively recover a significant amount of valuable, useable oil from byproducts formed during a dry milling process used for producing ethanol. The method may include forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may include evaporating the byproduct using a multi-stage evaporator, as well as recovering the oil before the final stage of the evaporator. Further, the step of recovering oil from the concentrate may include using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil.

Claims (32)

1. A method of processing thin stillage concentrate created during a dry milling process used for producing ethanol from corn, comprising:

recovering oil from the thin stillage concentrate

and subsequently evaporating the thin stillage concentrate in an evaporator to further reduce a moisture content and form an evaporated thin stillage concentrate, wherein the evaporated thin stillage concentrate has a lower moisture content than the thin stillage concentrate; and

mixing the evaporated thin stillage concentrate with distillers wet grains.

2. The method of claim 1 , wherein the recovering step comprises separating the oil from the thin stillage concentrate using a disk stack centrifuge.

3. The method of claim 2 , wherein the disk stack centrifuge produces suspended solids and the method further includes isolating and mixing the suspended solids with the distillers wet grains.

4. The method of claim 3 , wherein the disk stack centrifuge produces a syrup, and the method further comprises mixing the syrup and the suspended solids and the distillers wet grains to form a mixture.

5. The method of claim 3 , further including mixing the evaporated thin stillage concentrate with a mixture; and drying the mixture.

6. The method of claim 1 , wherein evaporating the thin stillage concentrate comprises removing an additional amount of water from the thin stillage concentrate in a multistage evaporator.

7. The method of claim 1 , wherein recovering the oil from the thin stillage concentrate comprises introducing the thin stillage concentrate to a disk stack centrifuge prior to a final stage of a multi-stage evaporator.

8. The method of claim 1 , wherein recovering the oil from the thin stillage concentrate comprises mechanically processing the thin stillage concentrate.

9. The method of claim 1 , further comprising drying the distiller wet grains and the evaporated thin stillage concentrate to produce dried distillers grains.

10. A method of processing thin stillage created by a dry milling process used for producing ethanol from corn in order to recover oil, comprising:

evaporating the thin stillage to reduce a moisture content and form a thin stillage concentrate;

introducing the thin stillage concentrate to a disk stack centrifuge and separating at least a portion of an oil from the thin stillage concentrate and subsequently

evaporating the thin stillage concentrate to further reduce the moisture content of the thin stillage concentrate and form an evaporated thin stillage concentrate; and

mixing the evaporated thin stillage concentrate with distillers wet grains.

11. The method of claim 10 , wherein the evaporating the thin stillage comprises using a multi-stage evaporator to form the thin stillage concentrate from the thin stillage and the step of introducing the thin stillage concentrate to the disk stack centrifuge is completed before a final stage of the multi-stage evaporator.

12. The method of claim 10 , wherein the evaporating the thin stillage or the thin stillage concentrate comprises using an evaporator including at least one scraped surface heat exchanger.

13. A method of processing thin stillage created by a dry milling process used for producing ethanol from corn in order to recover oil, comprising:

evaporating the thin stillage to reduce a moisture content and form a thin stillage concentrate, wherein the evaporating the thin stillage comprises using a multi-stage evaporator to form the concentrate from the thin stillage;

introducing the thin stillage concentrate to a centrifuge and separating oil from the thin stillage concentrate, wherein the step of introducing the concentrate to the centrifuge is completed before a final stage of the multi-stage evaporator;

evaporating the thin stillage concentrate to further reduce the moisture content of the thin stillage concentrate and form an evaporated thin stillage concentrate; and

mixing the evaporated thin stillage concentrate with the further reduced moisture content with distillers wet grains.

14. A method of processing thin stillage created by a dry milling process used for producing ethanol from corn in order to recover oil, comprising:

evaporating the thin stillage to reduce a moisture content and form a thin stillage concentrate;

introducing the thin stillage concentrate to a centrifuge and separating oil from the thin stillage concentrate;

evaporating the thin stillage concentrate to further reduce the moisture content of the thin stillage concentrate and form an evaporated thin stillage concentrate, wherein the evaporating the thin stillage and/or the thin stillage concentrate comprises using an evaporator including at least one scraped surface heat exchanger; and

mixing the evaporated thin stillage concentrate with the further reduced moisture content with distillers wet grains.

15. A method of processing concentrated thin stillage created during a dry milling process used for producing ethanol from corn, comprising:

recovering oil from the concentrated thin stillage, wherein recovering the oil from the thin stillage concentrate comprises introducing the thin stillage concentrate to a centrifuge prior to a final stage of a multi-stage evaporator; and

evaporating the concentrated thin stillage to reduce a moisture content and form an evaporated thin stillage concentrate prior to mixing with distillers wet grains, wherein the evaporated concentrated thin stillage has a lower moisture content than the concentrated thin stillage.

Assignments (5)
SECURITY AGREEMENT Recorded Jan 8, 2013
From: ECOSYSTEM TECHNOLOGIES, LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS AGRIFUELS CORPORATION; GS BIG MANAGEMENT, LLC; GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS COES (ADRIAN I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS GLOBAL BIODIESEL, LLC; GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS TECHNOLOGY, LLC; GREENSHIFT ENGINEERING, INC. (F/K/A GS CARBON DIOXIDE TECHNOLOGIES, INC.); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL, INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; VIRIDIS CAPITAL LLC
To: YA GLOBAL INVESTMENTS, L.P., AS COLLATERAL AGENT
Reel/Frame 029588/0092 →
SECURITY AGREEMENT Recorded Aug 31, 2010
From: VIRIDIUS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS AGRIFUELS CORPORATION; NEXTGEN, ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; GS GLOBAL BIODIESEL, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 024920/0795 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 18, 2009
From: GS ETHANOL TECHNOLOGIES, INC.
To: GS CLEANTECH CORPORATION
Reel/Frame 023252/0849 →
SECURITY AGREEMENT Recorded Sep 1, 2009
From: VIRIDIS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS GLOBAL BIODIESEL, LLC; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS LLC (F/K/A WARNECKE RENTALS, LLC); BOLLHEIMER & ASSOCIATES, INC.; ECOSYSTEM TECHNOLOGIES, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 023163/0954 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 7, 2008
From: WINSNESS, DAVID J.
To: GS ETHANOL TECHNOLOGIES, INC.
Reel/Frame 020477/0546 →