IP Library Granted Patent US 7,964,612
Granted Patent B2
US 7,964,612 · App. 11/871,311 · Granted Jun 21, 2011

Therapeutic pyrazolyl thienopyridines

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Quick Facts
Patent No.
US 7,964,612
App. No.
11/871,311
Granted
Jun 21, 2011
Kind
B2
Abstract

The present invention provides for compounds of Formula I, and pharmaceutically acceptable salts thereof, wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , and R 7 have any of the values defined therefor in the specification, and pharmaceutically acceptable salts thereof, that are useful as therapeutic agents in the treatment of TGFβ-mediated conditions, including cancer and fibrotic disorders. Also provided are pharmaceutical compositions comprising one or more compounds of Formula I.

Claims (20)

1. A compound of Formula I

or a pharmaceutically acceptable salt thereof, wherein:

R1 is a thieno[3,2-c]pyridinyl which may be optionally substituted with one to three substituents each independently selected from the group consisting of: C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)-S—(C 1 -C 3 -alkyl), —S—C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)- O—(C 1 -C 3 -alkyl), —O—C 1 -C 3 -alkyl, —C(O)O—C 1 -C 3 -alkyl, —C(O)O—H, —C(O)NR 30 R 31 , halo, —CN, —OH, wherein R 30 and R 31 are each independently selected from the group consisting of: H, and C 1 -C 3 alkyl-OH, C 1 -C 3 -alkyl, halo, and —O—C 1 -C 3 -alkyl;

R 2 and R 3 are independently selected from the group consisting of: hydrogen, C 1 -C 3 -alkyl, —C 1 -C 3 -alkyl)-S—(C 1 -C 3 -alkyl), —S—C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)-O—(C 1 -C 3 -alkyl), —O—C 1 -C 3 -alkyl, —C(O)O—C 1 -C 3 -alkyl, —C(O)O—H, —C(O)NR 30 R 31 , halo, —CN, —OH, and a C 3 -C 6 -cycloalkyl, wherein R 30 and R 31 are each independently selected from the group consisting of: H, and C 1 -C 3 alkyl; and

R 4 , R 5 , R 6 , and R 7 are selected from the group consisting of: H, —OH, C 3 -cycloalkyl, C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)-S—(C 1 -C 3 -alkyl), —S—C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)—O—-(C 1 -C 3 -alkyl), —O—C 1 -C 3 -alkyl, —C(O)O—C 1 -C 3 -alkyl, —C(O)O—H, —C(O)NR 30 R 31 , halo, —CN, —OH, wherein R 30 and R 31 are each independently selected from the group consisting of: H, and C 1 -C 3 alkyl, C 1 -C 3 -alkyl, —O—C 1 -C 3 -alkyl, and halo.

2. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein R 2 and R 3 are independently selected from the group consisting of: hydrogen, C 1 -C 3 -alkyl, —(C 1 -C 3 -alkyl)-O—(C 1 -C 3 -alkyl), —O—C 1 -C 3 -alkyl, —C(O)O—C 1 -C 3 -alkyl, —C(O)O—H, —C(O)NR 30 R 31 , halo, —CN, and —OH, wherein R 30 and R 31 are each independently selected from the group consisting of: H, and C 1 -C 3 alkyl.

3. The compound of claim 2 , or a pharmaceutically acceptable salt thereof, wherein R 2 and R 3 are independently selected from the group consisting of: hydrogen, and C 1 -C 3 alkyl.

4. The compound of claim 3 , or a pharmaceutically acceptable salt thereof, wherein R 2 is C 1 -C 2 alkyl and R 3 is hydrogen.

5. The compound of claim 4 , or a pharmaceutically acceptable salt thereof, or a pharmaceutically acceptable salt thereof wherein R 5 , R 6 , and R 7 are H, and R 4 is C 1 -C 3 -alkyl.

6. The compound of claim 5 , or a pharmaceutically acceptable salt thereof, wherein R 4 is methyl.

7. The compound of claim 6 , or a pharmaceutically acceptable salt thereof wherein R 1 is a thieno[3,2-c]pyridinyl which may be optionally substituted with one to three substituents each independently selected from the group consisting of: —OH, C l -C 3 alkyl, halo, and —O—C 1 -C 3 alkyl.

8. A compound selected from the group consisting of:

2-[1-(6-methylpyridin-2-yl)-1H-pyrazol-5-yl]thieno[3,2-c]pyridine;

2-[3,4-dimethyl-1-(6-methylpyridin-2-yl)-1 H-pyrazol-5-yl]thieno[3,2-c]pyridine; 2-[3-methyl-1-(6-methylpyridin-2-yl)-1 H-pyrazol-5-yl]thieno[3,2-c]pyridine;

2-[3-ethyl-1-(6-methylpyridin-2-yl)-1H-pyrazol-5-yl]thieno[3,2-c]pyridine;

2-[4-ethyl-1-(6-methylpyridin-2-yl)-1H-pyrazol-5-yl]thieno[3,2-c]pyridine; and a pharmaceutically acceptable salt of any one of the foregoing.

9. 2-[4-methyl-1 -(6-methylpyridin-2-yl)-1H-pyrazol-5-yl]thieno[3,2-c]pyridine or a pharmaceutically acceptable salt thereof.

10. A pharmaceutical composition comprising: a therapeutically effective amount of a compound of claim 1 , or pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable excipient.

11. The pharmaceutical composition of claim 10 , wherein said compound is 2-[4-methyl-1-(6-methylpyridin-2-yl)-1H-pyrazol-5-yl]thieno[3,2-c]pyridine; or a pharmaceutically acceptable salt thereof.

12. A topical pharmaceutical composition comprising: a therapeutically effective amount of a compound of claim 1 , or pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable excipient suitable for topical application.

Assignments (11)
CHANGE OF NAME Recorded Apr 15, 2021
From: FBM THERAPEUTICS, INC.
To: THIRONA BIO, INC.
Reel/Frame 056028/0290 →
ENTITY CONVERSION Recorded Apr 14, 2021
From: FBM THERAPEUTICS, LLC
To: FBM THERAPEUTICS, INC.
Reel/Frame 056830/0556 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 11, 2018
From: THESAN PHARMACEUTICALS, INC.
To: FBM THERAPEUTICS, LLC
Reel/Frame 045777/0324 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INADVERTENT PATENT NUMBERS ADDED PREVIOUSLY RECORDED AT REEL: 034749 FRAME: 0689. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT . Recorded Jan 29, 2018
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: BARCLAYS BANK PLC, AS SUCCESSOR AGENT
Reel/Frame 045177/0026 →
NOTICE OF SUCCESSION OF AGENCY Recorded Jan 9, 2015
From: GOLDMAN SACHS LENDING PARTNERS, LLC
To: BARCLAYS BANK PLC, AS SUCCESSOR AGENT
Reel/Frame 034749/0689 →
RELEASE OF SECURITY INTEREST Recorded Jan 10, 2014
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: MEDICIS PHARMACEUTICAL CORPORATION
Reel/Frame 031944/0190 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 25, 2013
From: MEDICIS PHARMACEUTICAL CORPORATION
To: THESAN PHARMACEUTICALS, INC.
Reel/Frame 031280/0766 →
SECURITY AGREEMENT Recorded Apr 24, 2013
From: MEDICIS PHARMACEUTICAL CORPORATION
To: GOLDMAN SACHS LENDING PARTNERS LLC
Reel/Frame 030281/0433 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2011
From: GRACEWAY PHARMACEUTICALS, LLC
To: MEDICIS PHARMACEUTICAL CORPORATION
Reel/Frame 027370/0813 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2009
From: BARRETT, STEPHEN D.; BOYS, MARK L.; CHEN, HUIFEN; KRAMER, JAMES B.
To: PFIZER INC.
Reel/Frame 023600/0131 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 8, 2009
From: PFIZER INC.; WARNER LAMBERT LLC
To: GRACEWAY PHARMACEUTICALS, LLC
Reel/Frame 022928/0146 →