IP Library Granted Patent US 9,044,702
Granted Patent B2
US 9,044,702 · App. 11/908,891 · Granted Jun 2, 2015

Method and systems for washing ethanol production byproducts to improve oil recovery

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Quick Facts
Patent No.
US 9,044,702
App. No.
11/908,891
Granted
Jun 2, 2015
Kind
B2
Abstract

In one aspect of the invention, a method and related system efficiently and effectively recover a significant amount of valuable, useable oil from byproducts formed during a dry milling process used for producing ethanol. The method may include forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct using a multi-stage evaporator, as well as recovering the oil before the final stage of the evaporator. Further, the step of recovering oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil.

Claims (17)

1. A method of processing whole stillage produced in a dry milling process used for producing ethanol from corn, comprising:

separating whole stillage into fractions comprising thin stillage and distillers wet grains;

combining the distillers wet grains fraction with the thin stillage fraction prior to concentrating the thin stillage fraction;

separating the combined fractions into thin stillage and distillers wet grains;

concentrating the thin stillage separated from the combined fractions or concentrating the thin stillage separated from the combined fractions and the thin stillage obtained from separating the whole stillage to form a thin stillage concentrate; and

recovering oil from the thin stillage concentrate.

2. The method of claim 1 , wherein separating the combined fractions into thin stillage and distillers wet grains comprises delivering the combined fractions to a separator.

3. The method of claim 2 , wherein the separator is a centrifuge.

4. The method of claim 1 , wherein the thin stillage further comprises a partially defatted thin stillage concentrate.

5. The method of claim 1 , wherein the thin stillage combined with the distillers wet grains fraction is at least a portion of the thin stillage fraction obtained prior to concentrating the portion of the thin stillage fraction.

6. A method for processing whole stillage including oil produced from dry milling corn, comprising:

separating the whole stillage in a three phase decanter to form a distillers wet grains fraction, a thin stillage fraction, and an oily fraction;

combining the distillers wet grains fraction with the thin stillage fraction prior to concentrating the thin stillage, and/or water and/or a defatted thin stillage fraction;

separating a liquid fraction from the combination of the distillers wet grains fraction with the thin stillage, and/or water and/or the defatted thin stillage fraction; and

concentrating the liquid fraction to form a thin stillage concentrate and recovering oil from the thin stillage concentrate.

7. The method of claim 6 , wherein the water is selected from the group consisting of potable water, condensate water, well water, and mixtures thereof.

8. The method of claim 6 , wherein the thin stillage fraction combined with the distillers wet grains fraction is at least a portion of the thin stillage fraction obtained prior to concentrating the portion of the thin stillage fraction.

Assignments (5)
SECURITY AGREEMENT Recorded Jan 8, 2013
From: ECOSYSTEM TECHNOLOGIES, LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS AGRIFUELS CORPORATION; GS BIG MANAGEMENT, LLC; GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS COES (ADRIAN I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS GLOBAL BIODIESEL, LLC; GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS TECHNOLOGY, LLC; GREENSHIFT ENGINEERING, INC. (F/K/A GS CARBON DIOXIDE TECHNOLOGIES, INC.); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL, INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; VIRIDIS CAPITAL LLC
To: YA GLOBAL INVESTMENTS, L.P., AS COLLATERAL AGENT
Reel/Frame 029588/0092 →
SECURITY AGREEMENT Recorded Aug 31, 2010
From: VIRIDIUS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS AGRIFUELS CORPORATION; NEXTGEN, ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; GS GLOBAL BIODIESEL, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 024920/0795 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2009
From: GS ETHANOL TECHNOLOGIES, INC.
To: GS CLEANTECH CORPORATION
Reel/Frame 023216/0641 →
SECURITY AGREEMENT Recorded Sep 1, 2009
From: VIRIDIS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS GLOBAL BIODIESEL, LLC; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS LLC (F/K/A WARNECKE RENTALS, LLC); BOLLHEIMER & ASSOCIATES, INC.; ECOSYSTEM TECHNOLOGIES, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 023163/0954 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 7, 2008
From: WINSNESS, DAVID J.
To: GS ETHANOL TECHNOLOGIES, INC.
Reel/Frame 020477/0546 →