IP Library Granted Patent US 7,888,344
Granted Patent B2
US 7,888,344 · App. 11/912,801 · Granted Feb 15, 2011

Fused thiazole derivatives as kinase inhibitors

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Quick Facts
Patent No.
US 7,888,344
App. No.
11/912,801
Granted
Feb 15, 2011
Kind
B2
Abstract

A series of 5,6-dihydro-1,3-benzothiazol-7(4H)-one derivatives, and analogues thereof, which are substituted in the 2-position by an optionally substituted morpholin-4-yl moiety, being selective inhibitors of PD kinase enzymes, are accordingly of benefit in medicine, for example in the treatment of inflammatory, autoimmune, cardiovascular, neurodegenerative, metabolic, oncological, nociceptive or ophthalmic conditions.

Claims (222)

1. A pharmaceutical composition comprising a compound of formula (I), or a pharmaceutically acceptable salt thereof:

wherein

—X— represents a group of formula (a), (b), (c), (d), (e), (f), (g) or (h):

R 1 and R 2 independently represent hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl-(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 1 and R 2 , when both are attached to the same carbon atom, represent, when taken together with the carbon atom to which they are both attached, C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; or

R 1 and R 2 , when attached to adjacent carbon atoms, represent, when taken together with the carbon atoms to which they are attached, C 5-7 cycloalkyl, phenyl or heteroaryl, any of which groups may be optionally benzo-fused and/or substituted by one or more substituents;

R 3 and R 4 independently represent hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, aryl(C 2-6 )alkenyl, aryl(C 2-6 )alkynyl, biaryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, C 3-7 heterocycloalkylcarbonyl, heteroaryl, heteroaryl(C 1-6 )alkyl, heteroaryl-aryl(C 1-6 )alkyl or aryl-heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 3 and R 4 , when both are attached to the same carbon atom, represent, when taken together with the carbon atom to which they are both attached, C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; or

R 3 and R 4 , when attached to adjacent carbon atoms, represent, when taken together with the carbon atoms to which they are attached, C 5-7 cycloalkyl, phenyl or heteroaryl, any of which groups may be optionally benzo-fused and/or substituted by one or more substituents; and

R 5 and R 6 independently represent hydrogen or C 1-6 alkyl,

together with a pharmaceutically acceptable carrier.

2. A compound of formula (I) or a pharmaceutically acceptable salt thereof:

wherein,

—X— represents a group of formula (a), (b), (c), (d), (e), (f), (g) or (h):

R 1 and R 2 independently represent hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-4 alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl-(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally, substituted by one or more substituents; or

R 1 and R 2 , when both are attached to the same carbon atom, represent, when taken together with the carbon atom to which they are both attached, C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; or

R 1 and R 2 , when attached to adjacent carbon atoms, represent, when taken together with the carbon atoms to which they are attached, C 5-7 cycloalkyl, phenyl or heteroaryl, any of which groups may be optionally benzo-fused and/or substituted by one or more substituents;

R 3 and R 4 independently represent hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 1-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, aryl(C 2-6 )alkenyl, aryl(C 2-6 )alkynyl, biaryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )allyl, C 3-7 heterocycloalkylcarbonyl, heteroaryl, heteroaryl(C 1-6 )alkyl, heteroaryl-aryl(C 1-6 )alkyl or aryl-heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 3 and R 4 , when both are attached to the same carbon atom, represent, when taken together with the carbon atom to which they are both attached, C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; or

R 3 , and R 4 , when attached to adjacent carbon atoms, represent, when taken together with the carbon atoms to which they are attached, C 5-7 cycloalkyl, phenyl or heteroaryl, any of which groups may be optionally benzo-fused and/or substituted by one or more substituents; and

R 5 and R 6 independently represent hydrogen or C 1-6 alkyl;

provided the compound is not:

2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-(morpholin-4-yl)-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one; and

7,7-dimethyl-2-(morpholin-4-yl)-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one.

3. A compound of formula (IIA), or a pharmaceutically acceptable salt thereof:

wherein

—X 1 — represents a group of formula (a) or (e):

R 6 represents hydrogen or C 1-6 alkyl;

R 11 represents hydrogen or optionally substituted C 2-6 alkyl; and

R 12 represents C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 11 and R 12 , when taken together with the carbon atom to which they are both attached, represent C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; and

R 13 represents hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, aryl(C 2-6 )alkenyl, aryl(C 2-6 )alkynyl, biaryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, C 3-7 heterocycloalkylcarbonyl, heteroaryl, heteroaryl(C 1-6 )alkyl, heteroaryl-aryl(C 1-6 )alkyl or aryl-heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents.

4. The compound of formula (IIB), or a pharmaceutically acceptable salt thereof:

wherein

—X 1 — represents a group of formula (a) or (e):

R 6 represents hydrogen or C 1-6 alkyl;

R 21 represents hydrogen or optionally substituted C 1-6 alkyl; and

R 22 represents hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 21 and R 22 , when taken together with the carbon atom to which they are both attached, represent C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents; and

R 23 represents C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, aryl(C 2-6 )alkenyl, aryl(C 2-6 )alkynyl, biaryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, C 3-7 heterocycloalkylcarbonyl, heteroaryl, heteroaryl(C 1-6 )alkyl, heteroaryl-aryl(C 1-6 )alkyl or aryl-heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents.

5. The compound as claimed in claim 4 wherein R 23 represents C 1-6 alkyl, aryl(C 1-6 )alkyl, biaryl-(C 1-6 )alkyl, heteroaryl(C 1-6 )alkyl or heteroaryl-aryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents.

6. The compound as claimed in claim 5 wherein R 23 represents substituted or unsubstituted indolylmethyl.

7. A compound of formula (IIC), or a pharmaceutically acceptable salt thereof:

wherein

—X 2 — represents a group of formula (b), (c), (d), (f), (g) or (h):

R 5 and R 6 independently represent hydrogen or C 1-6 alkyl;

R 13 represents hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-6 )alkyl, aryl(C 2-6 )alkenyl, aryl(C 2-6 )alkynyl, biaryl(C 1-6 )alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, C 3-7 heterocycloalkylcarbonyl, heteroaryl, heteroaryl(C 1-6 )alkyl, heteroaryl-aryl(C 1-6 )alkyl or aryl-heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents;

R 21 represents hydrogen or optionally substituted C 1-6 alkyl; and

R 22 represents hydrogen; or C 1-6 alkyl, C 3-7 cycloalkyl, C 3-7 cycloalkyl(C 1-6 )alkyl, aryl, aryl(C 1-4 alkyl, C 3-7 heterocycloalkyl, C 3-7 heterocycloalkyl(C 1-6 )alkyl, heteroaryl or heteroaryl(C 1-6 )alkyl, any of which groups may be optionally substituted by one or more substituents; or

R 21 and R 22 , when taken together with the carbon atom to which they are both attached, represent C 3-7 cycloalkyl or C 3-7 heterocycloalkyl, either of which groups may be optionally substituted by one or more substituents.

8. The compound as claimed in claim 4 , or a pharmaceutically acceptable salt thereof,

wherein

R 23 represents

and R 33 represents aryl or heteroaryl, either of which groups may be optionally substituted by one or more substituents.

9. The compound as claimed in claim 4 , or a pharmaceutically acceptable salt thereof:

wherein

R 23 represents

W represents CH or N; and

R 43 represents hydrogen, halogen, cyano, C 1-6 alkyl, hydroxy(C 1-6 )alkyl, trifluoromethyl, aryl(C 1-6 )alkyl, hydroxy, C 1-6 alkoxy, trifluoromethoxy, aryloxy, aryl(C 1-6 )alkoxy, C 1-6 alkylthio, arylsulphonyl, C 1-6 alkylsulphonyloxy, amino, C 2-6 alkylcarbonylamino, C 1-6 alkylsulphonylamino, C 2-6 alkylcarbonyl or aminocarbonyl.

10. The compound as claimed in claim 9 wherein W represents CH.

11. The compound as claimed in claim 9 wherein R 43 represents hydrogen.

12. The compound as claimed in claim 2 that is

2-(Morpholin-4-yl)-4H-spiro[1,3-benzothiazole-5,1′-cyclopentan]-7(6H)-one;

5-Isopropyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5-(4-Chlorophenyl)-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-(Morpholin-4-yl)-5-phenyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-(Morpholin-4-yl)-4H-spiro[1,3-benzothiazole-5,1′-cyclohexan]-7(6H)-one;

5-(4-Methoxyphenyl)-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-(Morpholin-4-yl)-5-propyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5-Methyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

6,6-Dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5-[4-(Methylthio)phenyl]-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7-(4H)-one;

5-(2-Furyl)-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

6-Methyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3R)-3-(1H-Indol-3-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(2-naphthylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(1-naphthylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2,3-(2-phenethyl)morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-Benzylmorpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(4aS,9aR)-2,3,9,9a-tetrahydroindeno[2,1-b][1,4]oxazin-4(4aH)-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(4-Chlorobenzyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(5-methyl-1H-indol-3-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{3-[4-(morpholin-4-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-(2,3-Dihydro-4H-1,4-benzoxazin-4-yl)-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{3-[(1-methyl-1H-indol-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(1-Acetyl-1H-indol-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-(2-phenylmorpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(4-Bromobenzyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(2,3-Dihydro-1H-indol-1-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(1H-indol-1-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-(trans-2,6-dimethylmorpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(Anilinomethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{3-[(N-methyl-N-phenylamino)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(3,4-Dihydroquinolin-1(2H)-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(3,4-Dihydroisoquinolin-2(1H)-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

(7E,Z)-5,5-Dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

7Z)-5,5-Dimethyl-2-(morpholin-4-O-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

(7E,Z)-2-(Morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

(7E,Z)-5,5-Dimethyl-2-[(3S)-3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

(7E,Z)-6-Methyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

(7E,Z)-6,6-Dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one oxime;

7,7-Dimethyl-2-[(3S)-3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

6-Methyl-2-(morpholin-4-yl)-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

6,6-Dimethyl-2-(morpholin-4-yl)-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

5,5-Dimethyl-2-(morpholin-4-yl)-4,5,6,7-tetrahydro-1,3-benzothiazol-7-ol;

5,5-Dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazole-7(4H)-thione;

2-[(3S)-3-(3-Bromobenzyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-(Biphenyl-3-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one:

5,5-Dimethyl-2-[(3S)-3-(3-(pyridin-3-yl)benzyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(3-thienyl)benzyl morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(3-(pyridin-4-yl)benzyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(3-(pyrimidin-5-yl)benzyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-(3-Bromobenzyl)morpholin-4-yl]-7,7-dimethyl-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

2-[(3S)-3-(Biphenyl-3-ylmethyl)morpholin-4-yl]-7,7-dimethyl-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

7,7-Dimethyl-2-[(3S)-3-(3-(pyridin-3-yl)benzyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

5,5-Dimethyl-2-[3-(1H-pyrrolo[2,3-b]pyridin-3-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

7,7-Dimethyl-2-[(3R)-3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

7,7-Dimethyl-2-[3-(1H-pyrrolo[2,3-b]pyridin-3-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

5,5-Dimethyl-2-{(3R)-3-[(phenylthio)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(41-1)-one;

5,5-Dimethyl-2-[3-(phenoxymethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

7,7-Dimethyl-2-(morpholin-4-yl)-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepine-4-thione;

7,7-Dimethyl-2-[(3S)-3-(1H-indol-3-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepine-4-thione;

5,5-Dimethyl-2-[3-[(pyridin-3-ylamino)methyl]morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(piperidin-1-ylcarbonyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(3,4-Dihydroquinolin-1(2H)-ylcarbonyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(1-Benzothien-3-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(Biphenyl-4-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(4-(pyridin-3-yl)benzyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[3-(5-methyl-1H-indol-3-yl)methyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazole-7(4H)-thione;

5,5-Dimethyl-2-[3-(1-naphthylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazole-7(4H)-thione;

2-[3-(1-Benzothien-3-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazole-7(4H)-thione;

N-{[4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-3-yl]methyl}benzenesulfonamide;

2-[3-(1-Benzothien-2-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

7,7-Dimethyl-2-[3-(isoquinolin-4-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

7,7-Dimethyl-2-[3-(quinolin-5-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

7,7-Dimethyl-2-[3-(quinolin-8-ylmethyl)morpholin-4-yl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

5,5-Dimethyl-2-[3-(quinolin-8-ylmethyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(3-(pyrroldin-1-yl)benzyl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{3-[(6-Bromopyridin-2-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one:

5,5-Dimethyl-2-{3-[(6-phenylpyridin-2-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one:

5,5-Dimethyl-2-{(3S)-3-[2(2′-methylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3′-methoxybiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[2′-(trifluoromethyl)biphenyl-3-yl]methyl morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2{(3S)-3-[(2′-Chlorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(1-naphthyl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(2-naphthyl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′-Chlorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(3′-fluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(2′-fluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(2′,6′-Difluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′,4′-Dichlorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{[4′-(methylthio)biphenyl-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-[3-(1-Benzofuran-2-yl)benzyl]morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(1-Benzothien-2-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(3′-methylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(2′-methoxybiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(thien-2-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-[(3′-ethoxybiphenyl-3-yl)methyl]morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(4-methylthien-2-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(5-Acetylthien-2-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(1-Benzothien-3-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3(4′-methylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′-Acetylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(4′-Acetylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3(2′-Bromobiphenyl-3-yl]methyl)morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′-Bromobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(4′-Bromobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-{[3′,5′-Bis(trifluoromethyl)biphenyl-3-yl]methyl}morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(4′-Chlorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(2′,5′-Dichlorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′,5′-Difluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′,4′-Dimethoxybiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(2′,3′-Dimethylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(3′,5′-Dimethylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[(2′,5′-Dimethylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(4′-fluoro-3′-methylbiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(4′-fluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[(4′-methoxybiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(1,3-benzodioxol-5-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[4′-phenoxybiphenyl-3-yl)methyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{[3′-(trifluoromethyl)biphenyl-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3′,4′-Difluorobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

N-(3′-{[(3S)-4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-3-yl]methyl}biphenyl-3-yl)acetamide;

2-{(3S)-3-[(3′-Aminobiphenyl-3-yl)methyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

3′-{[(3S)-4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-3-yl]methyl}biphenyl-4-carbonitrile;

5,5-Dimethyl-2-[(3S)-3-{[3′-(hydroxymethyl)biphenyl-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{[2′-(hydroxymethyl)biphenyl-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{[3′-(trifluoromethoxy)biphenyl-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(6-methoxypyridin-3-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

N-(3′-{[(3S)-4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-3-yl]methyl}biphenyl-3-yl)methanesulfonamide;

2-{(3S)-3-[3-(3,5-Dimethylisoxazol-4-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{3-[1-(phenylsulfonyl)-1H-indol-3-yl]benzyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(6-Chloropyridin-3-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

3′-{[(3S)-4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-3-yl]methyl}biphenyl-4-carboxamide;

5,5-dimethyl-2-{(3S)-3-[3-(3-fluoropyridin-4-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-{(3S)-3-[3-(1-Benzyl-1H-pyrazol-4-yl)benzyl]morpholin-4-yl}-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{(3S)-3-[3-(1-methyl-1H-pyrazol-4-yl)benzyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

7,7-Dimethyl-2-(morpholin-4-yl)-4,6,7,8-tetrahydro-5H-[1,3]thiazolo[5,4-b]azepin-5-one;

2-[(3S)-3-{[5-(Benzyloxy)-1H-indol-3-yl]methyl}morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-{[5-(hydroxy)-1H-indol-3-yl]methyl}morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

7,7-Dimethyl-2-{(3S)-3-[(5-hydroxy-1H-indol-3-yl)methyl]morpholin-4-yl}-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-c]azepin-4-one;

3-{[(3S)-4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-Amorpholin-3-yl]methyl}-1H-indol-5-yl methanesulfonate;

2-[3-(3,4-Dihydroisoquinolin-2(1H)-ylcarbonyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[3-(3,4-Dihydroquinoxalin-1(2H)-ylcarbonyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{3-[(6-methyl-3,4-dihydroquinolin-1(2H)-yl)carbonyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-{3-[(6-methoxy-3,4-dihydroquinolin-1(2H)-ylcarbonyl]morpholin-4-yl}-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

5,5-Dimethyl-2-[(3S)-3-(3-phenylprop-2-yn-1-yl)morpholin-4-yl]-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-(1H-Benzotriazol-1-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[(3S)-3-(1H-Benzimidazol-1-ylmethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

2-[2-(Aminomethyl)morpholin-4-yl]-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one;

N-(1-Benzothien-3-ylmethyl)-2-[4-(5,5-dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-2-yl]acetamide;

N-{[4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-2-yl]methyl}-1-benzofuran-2-carboxamide;

N-{[4-(5,5-Dimethyl-7-oxo-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)morpholin-2-yl]methyl}benzenesulfonamide; or

(7E)-5,5-Dimethyl-2-(morpholin-4-yl)-5,6-dihydro-1,3-benzothiazol-7(4H)-one hydrazone.

13. The pharmaceutical composition comprising a compound according to claim 2 and a pharmaceutically acceptable carrier.

14. The compound as claimed in claim 10 wherein R 43 represents hydrogen.

15. The pharmaceutical composition comprising a compound according to claim 3 and a pharmaceutically acceptable carrier.

16. The pharmaceutical composition comprising a compound according to claim 4 and a pharmaceutically acceptable carrier.

Assignments (2)
CONFIRMATORY ASSIGNMENT Recorded Jun 10, 2016
From: UCB PHARMA, S.A.
To: UCB BIOPHARMA SPRL
Reel/Frame 038953/0312 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 25, 2008
From: ALEXANDER, RIKKI PETER; AUJLA, PAVANDEEP; BATCHELOR, MARK JAMES; BROOKINGS, DANIEL CHRISTOPHER; BUCKLEY, GEORGE MARTIN; LUCILE CREPY, KAREN VIVIANE; KULISA, CLAIRE LOUISE; TURNER, JAMES PETRIE
To: UCB PHARMA S.A.
Reel/Frame 021146/0448 →