IP Library Granted Patent US 8,215,825
Granted Patent B2
US 8,215,825 · App. 11/915,010 · Granted Jul 10, 2012

Fluid mixing apparatus and method

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Quick Facts
Patent No.
US 8,215,825
App. No.
11/915,010
Granted
Jul 10, 2012
Kind
B2
Abstract

Methods and apparatus are provided for influencing mixing of a first fluid injected through a slot into a second fluid flowing through a conduit, by automatically or remotely adjusting the slot width to provide at least a certain slot velocity of the first fluid being introduced into the conduit. In particular, methods and apparatus are provided for mixing control in injecting titanium tetrachloride into an oxygen stream in a process for making titanium dioxide.

Claims (31)

1. A method for mixing two fluids, comprising the steps of:

introducing a first fluid through a circumferential injection slot and into a conduit transporting a second fluid, wherein the circumferential injection slot is defined by a moveable wall that is transversely movable relative to the introduction of the first fluid therethrough; and

automatically or remotely adjusting the circumferential injection slot, by transversely moving the moveable wall so as to adjust the width of the circumferential injection slot to maintain at least a certain slot velocity of the first fluid through the circumferential injection slot.

2. A method according to claim 1 , wherein the injection slot is remotely adjusted to alter the slot velocity of the first fluid through the injection slot from a first value to a second value.

3. A method according to claim 1 , wherein the circumferential injection slot is automatically adjusted to maintain a substantially constant slot velocity of the first fluid through the circumferential injection slot.

4. A method according to claim 3 , wherein the substantially constant slot velocity is from about 200 feet per second to about 300 feet per second.

5. A method according to claim 3 , wherein the step of automatically adjusting maintains a substantially constant pressure drop across the circumferential injection slot.

6. A method according to claim 5 , wherein the substantially constant pressure drop is from about 1 psi to about 2 psi.

7. A method according to claim 5 , wherein the circumferential injection slot is adjusted so that the introducing step is performed at a substantially constant pressure.

8. A method according to claim 7 , wherein a bellows is utilized to maintain the substantially constant pressure of the introducing step.

9. A method according to claim 1 , wherein the first fluid comprises titanium tetrachloride and the second fluid comprises oxygen.

10. A method according to claim 1 , further comprising the step of remotely adjusting the circumferential injection slot to alter the slot velocity of the first fluid through the circumferential injection slot from a first value to a second value.

11. A method for mixing two fluids, comprising the steps of:

introducing, at a first pressure, a first fluid through a circumferential injection slot and into a conduit transporting a second fluid, wherein the circumferential injection slot is defined by a moveable wall that is transversely movable relative to the introduction of the first fluid therethrough;

monitoring the first pressure; and

automatically or remotely adjusting the circumferential injection slot in accordance with the monitored first pressure by transversely moving the moveable wall so as to adjust the width of the circumferential injection slot.

12. A method according to claim 11 , wherein the circumferential injection slot is adjusted to maintain a substantially constant first pressure.

13. A method according to claim 11 , wherein the first fluid comprises titanium tetrachloride and the second fluid comprises oxygen.

14. A method for mixing two fluids, comprising the steps of:

introducing, at a first flow rate and a first pressure, a first fluid through a circumferential injection slot and into a conduit transporting a second fluid, wherein the circumferential injection slot is defined by a moveable wall that is transversely movable relative to the introduction of the first fluid therethrough;

monitoring the first flow rate; and

automatically or remotely adjusting the size of the circumferential injection slot in accordance with the monitored first flow rate by transversely moving the moveable wall so as to adjust the width of the circumferential injection slot.

15. A method according to claim 14 , wherein the circumferential injection slot is adjusted to maintain a substantially constant first pressure.

16. A method according to claim 14 , wherein the first fluid comprises titanium tetrachloride and the second fluid comprises oxygen.

17. A method for adjusting a circumferential injection slot in an apparatus for injecting a first fluid into a conduit transporting a second fluid, the circumferential injection slot defined by a moveable wall that is transversely moveable relative to the injection of the first fluid therethrough, comprising the step of: automatically or remotely adjusting the circumferential injection slot to maintain a substantially constant slot velocity by transversely moving the moveable wall so as to adjust the width of the circumferential injection slot.

18. A method according to claim 17 , wherein the automatically or remotely adjusting step maintains a substantially constant pressure drop across the circumferential injection slot.

19. A method according to claim 18 , wherein the substantially constant pressure drop is from about 1 psi to about 2 psi.

20. A method according to claim 17 , wherein the first fluid comprises titanium tetrachloride and the second fluid comprises oxygen.

21. A method for mixing two fluids, comprising the steps of:

introducing a first fluid through a circumferential injection slot and into a conduit transporting a second fluid, wherein the circumferential injection slot is defined by a moveable wall that is transversely movable relative to the introduction of the first fluid therethrough; and

automatically adjusting the circumferential injection slot, by transversely moving the moveable wall so as to adjust the width of the circumferential injection slot to maintain at least a substantially constant slot velocity of the first fluid through the circumferential injection slot and maintain a substantially constant pressure drop across the circumferential injection slot and so that the introducing step is preformed at a substantially constant pressure wherein a bellows is utilized to maintain the substantially constant pressure of the introducing step and the bellows has a side attached to the movable wall.

Assignments (6)
ASSIGNMENT OF SECURITY INTEREST IN PATENT COLLATERAL RECORDED AT REEL/FRAME 044100/0339 Recorded Mar 12, 2021
From: BANK OF AMERICA, N.A.
To: HSBC BANK USA, NATIONAL ASSOCIATION, AS THE SUCCESSOR ADMINISTRATIVE AGENT AND COLLATERAL AGENT
Reel/Frame 055578/0880 →
PATENT SECURITY AGREEMENT Recorded Oct 2, 2017
From: TRONOX LLC
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 044100/0339 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL AT REEL/FRAME NOS. 027682/0086 AND 030047/0422 Recorded Sep 26, 2017
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: TRONOX LLC
Reel/Frame 044018/0893 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Sep 25, 2017
From: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
To: TRONOX LLC; TRONOX WORLDWIDE LLC
Reel/Frame 043993/0306 →
PATENT SECURITY AGREEMENT Recorded Jul 18, 2012
From: TRONOX LLC; TRONOX WORLDWIDE LLC
To: UBS AG, STAMFORD BRANCH
Reel/Frame 028582/0669 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 12, 2012
From: WELLS FARGO CAPITAL FINANCE, LLC
To: TRONOX LLC; TRONOX WORLDWIDE LLC
Reel/Frame 028535/0362 →