IP Library Granted Patent US 9,120,849
Granted Patent B2
US 9,120,849 · App. 11/929,089 · Granted Sep 1, 2015

Nucleic acid amplification controls

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Quick Facts
Patent No.
US 9,120,849
App. No.
11/929,089
Granted
Sep 1, 2015
Kind
B2
Abstract

The present invention discloses positive control material for nucleic acid amplification based detection of microorganisms in biological samples. The control material comprises purified microorganism that is rendered non-infectious but is amenable to nucleic acid amplification. Also disclosed is a process for making and using the control material.

Claims (11)

1. A method for producing a positive control for the detection of microorganisms which comprises

(a) purifying microorganisms from a source; (b) exposing the purified microorganism to an aldehyde at a temperature of 2-8° C. such that one or more surface proteins are irreversibly modified while leaving the nuclear components substantially intact, and the purified microorganism is thereby rendered non-pathogenic and is capable of nucleic acid amplification; and (c) suspending the microorganism in a liquid matrix comprising a biological fluid or a synthetic biological fluid,

wherein the composition is useful as a positive internal control for nucleic acid amplification detection tests.

2. The method of claim 1 , wherein the aldehyde is selected from the group consisting of formaldehyde, acetaldehyde, propionaldehyde, n-butyraldehyde, benzaldehyde, p-nitrobenzaldehyde, p-tolualdehyde, salicylaldehyde, phenylacetaldehyde.

3. The method of claim 1 , wherein the aldehyde comprises two or more reactive functional groups.

4. The method of claim 3 , wherein the aldehyde is paraformaldehyde.

5. The method of claim 4 , wherein paraformaldehyde is used at a concentration of no more than 5%.

6. The method of claim 1 , wherein the microorganism is a virus.

7. The method claim 6 , wherein the virus is chosen from the group consisting of human immunodeficiency virus, hepatitis C virus, hepatitis B virus, cytomegalovirus, human lymphotrophic virus, Epstein-Barr virus, parvovirus, herpes simplex virus, human herpes virus 8 and hepatitis A virus.

8. The method of claim 1 , wherein the microorganism is an intracellular parasite.

9. The method of claim 8 , wherein the parasite is chosen from the group consisting of Chlamydia trachomatis, Chlamydia psittaci, Rickettsia prowazeki, Rickettsia typhi, Rickettsia rickettsi, Rickettsia sibtncus, Rickettsia conori, Rickettsia australis, Rickettsia akari, Rickettsia tsutsugamushi, Coxiella bumeti and Rochalimaea quintana.

Assignments (9)
PATENT SECURITY AGREEMENT Recorded Jun 11, 2025
From: COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC; ZEPTOMETRIX LLC; CONTROL 3, LLC; ENVIRONMENTAL EXPRESS, INC.; ENVIRONMENTAL MONITORING SYSTEMS, LLC
To: UBS, AG, STAMFORD BRANCH
Reel/Frame 071511/0113 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDEDNOVEMBER 9, 2021 AT REEL 058066 FRAME 0423 Recorded Jun 10, 2025
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: ZEPTOMETRIX LLC; ENVIRONMENTAL EXPRESS, INC.; COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
Reel/Frame 071587/0751 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CORTLAND CAPITAL MARKET SERVICES LLC, AS COLLATERAL AGENT
To: ZEPTOMETRIX LLC (F/K/A ZEPTOMETRIC CORPORATION)
Reel/Frame 058073/0453 →
SECURITY INTEREST Recorded Nov 9, 2021
From: ZEPTOMETRIX LLC; ENVIRONMENTAL EXPRESS, INC.; COLE-PARMER INSTRUMENT COMPANY LLC; SPEX CERTIPREP, LLC; SPEX SAMPLEPREP, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 058066/0423 →
RELEASE OF FIRST LIEN SECURITY INTEREST (REEL/FRAME 054888/0063) Recorded Nov 1, 2021
From: JEFFERIES FINANCE LLC
To: ZEPTOMETRIX CORPORATION
Reel/Frame 057988/0285 →
CHANGE OF NAME Recorded Mar 24, 2021
From: ZEPTOMETRIX CORPORATION
To: ZEPTOMETRIX LLC
Reel/Frame 055701/0548 →
FIRST LIEN SECURITY AGREEMENT Recorded Jan 4, 2021
From: ZEPTOMETRIX CORPORATION
To: JEFFERIES FINANCE LLC
Reel/Frame 054888/0063 →
SECOND LIEN SECURITY AGREEMENT Recorded Jan 4, 2021
From: ZEPTOMETRIX CORPORATION
To: CORTLAND CAPITAL MARKET SERVICES LLC
Reel/Frame 054888/0153 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 16, 2015
From: CHIKLIS, GREGORY R.; HENGST, JAMES C. D.
To: ZEPTOMETRIX CORPORATION
Reel/Frame 036112/0736 →