IP Library Granted Patent US 8,663,695
Granted Patent B2
US 8,663,695 · App. 11/931,484 · Granted Mar 4, 2014

Formulations and methods for treating rhinosinusitis

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Quick Facts
Patent No.
US 8,663,695
App. No.
11/931,484
Granted
Mar 4, 2014
Kind
B2
Abstract

The invention involves methods and formulations for treating or preventing rhinosinusitis, including fungus-induced rhinosinusitis in mammals. In one embodiment, the formulation of the present invention comprises a steroidal anti-inflammatory agent having a specific particle size distribution profile. The formulation may also comprise an antifungal agent, antibiotic or antiviral agent.

Claims (41)

1. A nasal formulation for the treatment of fungus-induced rhinosinusitis comprising an aqueous suspension of steroidal anti-inflammatory particles, said suspended solid steroidal anti-inflammatory particles comprising beclomethasone dipropionate monohydrate equivalent to 0.042% w/w beclomethasone dipropionate and having the following particle size distribution profile:

(i) about 10% or less of the steroidal anti-inflammatory particles have a particle size of less than 0.3 microns;

(ii) about 25% or less of the steroidal anti-inflammatory particles have a particle size of less than 0.55 microns;

(iii) about 50% or less of the steroidal anti-inflammatory particles have a particle size of less than 1.1 microns;

(iv) about 75% or less of the steroidal anti-inflammatory particles have a particle size of less than 1.8 microns; and

(v) about 90% or less of the steroidal anti-inflammatory particles have a particle size of less than 2.7 microns; and

wherein the formulation is suitable for administration to the nasal-paranasal mucosa and said formulation is sterile and has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 80% of the beclomethasone originally present in the formulation still remains in the formulation.

2. The nasal formulation of claim 1 , further comprising from 0.01% to 10% w/w of a tonicity agent.

3. The nasal formulation of claim 2 , wherein the tonicity agent is anhydrous dextrose.

4. The nasal formulation of claim 1 , wherein said formulation has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 95% of the beclomethasone originally present in the formulation still remains in the formulation.

5. The nasal formulation of claim 1 , further comprising about 20 to about 70 mg of an antifungal agent selected from the group consisting of itraconazole, ketoconazole and voriconazole.

6. A nasal formulation for the treatment of fungus-induced rhinosinusitis comprising an aqueous suspension of beclomethasone particles, said suspended solid beclomethasone particles having the following particle size distribution profile:

(i) about 10% or less of the beclomethasone particles have a particle size of less than 0.3 microns;

(ii) about 25% or less of the beclomethasone particles have a particle size of less than 0.55 microns;

(iii) about 50% or less of the beclomethasone particles have a particle size of less than 1.1 microns;

(iv) about 75% or less of the beclomethasone particles have a particle size of less than 1.8 microns; and

(v) about 90% or less of the beclomethasone particles have a particle size of less than 2.7 microns; and

about 0.1 mg/mL to about 0.2 mg/mL of sodium edetate; wherein the formulation is suitable for administration to the nasal-paranasal mucosa; and

said formulation is sterile and has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 80% of the beclomethasone originally present in the formulation still remains in the formulation.

7. The nasal formulation of claim 6 , wherein said suspended solid beclomethasone particles having the following particle size distribution profile:

(i) about 10% or less of the beclomethasone particles have a particle size of less than 0.3 microns;

(ii) about 25% or less of the beclomethasone particles have a particle size of less than 0.55 microns;

(iii) about 50% or less of the beclomethasone particles have a particle size of less than 1.1 microns;

(iv) about 75% or less of the beclomethasone particles have a particle size of less than 1.8 microns; and

(v) about 90% or less of the beclomethasone particles have a particle size of less than 2.7 microns; and

about 575 to about 700 mg of an antibiotic agent and about 0.1 mg/mL to about 0.2 mg/mL of sodium edetate; wherein the formulation is suitable for administration to the nasal-paranasal mucosa.

8. The nasal formulation of claim 6 , further comprising from 0.01% to 10% w/w of a tonicity agent.

9. The nasal formulation of claim 8 , wherein the tonicity agent is anhydrous dextrose.

10. The nasal formulation of claim 6 , wherein said formulation has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 95% of the beclomethasone originally present in the formulation still remains in the formulation.

11. The nasal formulation of claim 6 , further comprising about 575 to about 700 mg of an antibiotic agent.

12. A method of treating fungus-induced rhinosinusitis in a mammal comprising the steps of applying to the mammal's nasal-paranasal mucosa an aqueous suspension of suspended solid steroidal anti-inflammatory particles comprising beclomethasone dipropionate monohydrate equivalent to 0.042% w/w beclomethasone dipropionate particles, and about 0.1 mg/mL to about 0.2 mg/mL of sodium edetate, said suspended solid beclomethasone particles having the following particle size distribution profile:

(i) about 10% of the beclomethasone particles have a particle size of less than 0.3 microns;

(ii) about 25% of the beclomethasone particles have a particle size of less than 0.55 microns;

(iii) about 50% of the beclomethasone particles have a particle size of less than 1.1 microns;

(iv) about 75% of the beclomethasone particles have a particle size of less than 1.8 microns; and

(v) about 90% of the beclomethasone particles have a particle size of less than 2.7 microns; and

said formulation is sterile and has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 80% of the beclomethasone originally present in the formulation still remains in the formulation.

13. The method of claim 12 , wherein the aqueous suspension further comprises from 0.01% to 10% w/w of a tonicity agent.

14. The method of claim 13 , wherein the tonicity agent is anhydrous dextrose.

15. The method of claim 12 , wherein said formulation has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 95% of the beclomethasone originally present in the formulation still remains in the formulation.

16. The method of claim 12 , wherein the formulation further comprises about 20 to about 70 mg of an antifungal agent.

Assignments (8)
ADDRESS CHANGE Recorded Mar 15, 2022
From: MYLAN SPECIALTY L.P.
To: MYLAN SPECIALTY L.P.
Reel/Frame 059366/0851 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2013
From: DEY PHARMA, L.P.
To: MYLAN SPECIALTY L.P.
Reel/Frame 030482/0242 →
PATENT RELEASE Recorded Dec 10, 2012
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: DEY PHARMA L.P. (F/K/A DEY, L.P.); MYLAN PHARMACEUTICALS, INC.; MYLAN BERTEK PHARMACEUTICALS INC.; MYLAN TECHNOLOGIES, INC.; SOMERSET PHARMACEUTICALS, INC.; MYLAN INSTITUTIONAL INC. (F/K/A UDL LABORATORIES, INC.); MYLAN INC.
Reel/Frame 029440/0967 →
CHANGE OF NAME Recorded Dec 9, 2011
From: DEY, L.P.
To: DEY PHARMA, L.P.
Reel/Frame 027360/0090 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 9, 2011
From: CHAUDRY, IMTIAZ, PHD
To: DEY, L.P.
Reel/Frame 027359/0936 →
SECURITY AGREEMENT Recorded Nov 21, 2011
From: MYLAN PHARMACEUTICALS, INC.; MYLAN BERTEK PHARMACEUTICALS INC.; MYLAN TECHNOLOGIES, INC.; MYLAN INSTITUTIONAL INC. (F/K/A UDL LABORATORIES, INC.); SOMERSET PHARMACEUTICALS, INC.; DEY PHARMA, L.P. (F/K/A DEY L.P.)
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 027270/0799 →
PATENT RELEASE Recorded Nov 18, 2011
From: JPMORGAN CHASE BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: DEY PHARMA, L.P. (F/K/A DEY, L.P.); MYLAN INC.; MYLAN TECHNOLOGIES, INC.; MYLAN PHARMACEUTICALS, INC.
Reel/Frame 027302/0391 →
SECURITY AGREEMENT Recorded Jun 14, 2010
From: MYLAN INC.; DEY PHARMA, L.P.; DEY, INC.; MYLAN TECHNOLOGIES, INC.; MYLAN PHARMACEUTICALS INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 024532/0227 →