IP Library Granted Patent US 7,838,703
Granted Patent B2
US 7,838,703 · App. 11/941,806 · Granted Nov 23, 2010

Diaromatic amine derivatives as antioxidants

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Quick Facts
Patent No.
US 7,838,703
App. No.
11/941,806
Granted
Nov 23, 2010
Kind
B2
Abstract

A diaromatic amine compound having the general formula: wherein R 1 and R 2 together with the carbon atoms to which they are bonded are joined together to form a C 3 -C 30 ring, and R 3 is an allyl, benzyl, or methallyl group. R 4 , R 5 , and R 6 are independently hydrogen, C 1 -C 30 alkyl group, C 2 -C 30 alkenyl group, C 3 -C 12 cycloalkyl group, C 5 -C 25 aryl group, C 6 -C 25 arylalkyl group, or C 1 -C 30 alkoxy group.

Claims (30)

1. A diaromatic amine compound having the general formula:

wherein R 1 and R 2 together with the carbon atoms to which they are bonded are joined together to form a first C 3 -C 30 ring;

R 3 is an allyl, benzyl, or methallyl group;

R 4 and R 6 together with the carbon atoms to which the are bonded are joined together to form a second C 3 -C 30 , ring; and

R 5 is hydrogen, substituted or unsubstituted C 1 -C 30 alkyl group, substituted or unsubstituted C 2 -C 30 alkenyl group, substituted or unsubstituted C 3 -C 12 cycloalkyl group, substituted or unsubstituted C 5 -C 25 aryl group, C 6 -C 25 arylalkyl group, or C 1 -C 30 alkoxy group.

2. The compound of claim 1 , where any of the C 3 -C 30 rings, C 1 -C 30 alkyl group, C 2 -C 30 alkenyl group, C 3 -C 12 cycloalkyl group, C 5 -C 25 aryl group, C 6 -C 25 arylalkyl group, or C 1 -C 30 alkoxy group is substituted with one or more substituents, the substituents are selected from hydroxy, halogen, carboxyl, cyano, nitro, oxo, thio, substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted alkenyl, substituted or unsubstituted alkynyl, substituted or unsubstituted aryl, substituted or unsubstituted arylalkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted cycloalkenyl, substituted or unsubstituted amino, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted heterocycloalkyl ring, substituted or unsubstituted heteroarylalkyl, substituted or unsubstituted heterocyclic ring, —COOR x , —C(O)NR x R y , —NR x R x , C(O)R x , —OR x , —OC(O)R x , —OC(O)NR x R x , —SR x , —SOR x , —SO 2 R x , wherein R x and R x in each comprises a saturated or unsaturated chain of 1 to 30 carbons.

3. The compound of claim 1 , wherein R 1 and R 2 are joined together to form a saturated 5-, 6- or 7-membered ring.

4. The compound of claim 1 , wherein R 1 and R 2 are joined together to form a partially unsaturated or fully unsaturated 5-, 6- or 7-membered ring.

5. The compound of claim 1 of general formula:

6. The compound of claim 1 of general formula:

wherein Z and Y are heteroatoms.

7. The compound of claim of general formula:

8. The compound of claim of the formula:

9. A lubricating oil composition comprising:

at least one oil of lubricating viscosity; and

an antioxidant improving effective amount of at least one diaromatic amine compound having the general formula of claim 1 .

10. The lubricating oil composition of claim 9 , wherein the at least one oil of lubricating viscosity is selected from the group consisting of engine oils, transmission fluids, hydraulic fluids, gear oils, marine cylinder oils, compressor oils, refrigeration lubricants and mixtures thereof.

11. The lubricating oil composition of claim 9 , further comprising at least one lubricating oil additive selected from the group consisting of antioxidants, anti-wear agents, detergents, rust inhibitors, dehazing agents, demulsifying agents, metal deactivating agents, friction modifiers, pour point depressants, antifoaming agents, co-solvents, package compatibilisers, corrosion-inhibitors, ashless dispersants, dyes, extreme pressure agents and mixtures thereof.

12. The lubricating oil composition of claim 11 , wherein the lubricating oil composition with the at least one lubricating oil additive has a phosphorous content of less than about 0.1 weight percent.

13. The lubricating oil composition of claim 9 , further comprising at least one lubricating oil additive selected from the group consisting of an alkylated diphenylamine, alkylated hindered phenolic, alkylated substituted or unsubstituted phenylenediamine, alkylated oil soluble copper compound, alkylated sulfur containing compound known to impart oxidation stability and mixtures thereof.

14. The lubricating oil composition of claim 13 , wherein the alkylated sulfur containing compound known to impart oxidation stability is selected from the group consisting of phenothiazines, sulfurized olefins, thiocarbamates, sulfur bearing hindered phenolics, zinc dialkyldithiophosphates and mixtures thereof.

15. An additive package comprising about 0.1 to about 75 weight percent of at least one diaromatic amine compound having the general formula of claim 1 .

16. A stabilizer-containing composition comprising:

(a) an organic material subject to oxidative, thermal, and/or light-induced degradation and in need of stabilization to prevent or inhibit such degradation; and

(b) a stabilization effective amount of at least one diaromatic amine compound having the general formula of claim 1 .

17. A method for stabilizing an organic material subject to oxidative, thermal, and/or light-induced degradation and in need of stabilization to prevent or inhibit such degradation, the method comprising adding to the organic material a stabilizing amount of at least one diaromatic amine compound having the general formula of claim 1 .

18. A compound comprising:

a diaromatic amine having at least two phenyl groups bonded to a nitrogen, wherein the nitrogen is further bonded to a carbon containing substituent group such that the compound is incapable of being an electron withdrawing group;

a first ring fused to one of the phenyl groups; and

further comprising a second ring fused to one of the other phenyl groups.

Assignments (10)
MERGER AND CHANGE OF NAME Recorded Sep 7, 2018
From: CHEMTURA CORPORATION; LANXESS SOLUTIONS US INC.
To: LANXESS SOLUTIONS US INC.
Reel/Frame 046811/0266 →
RELEASE OF AMENDED AND RESTATED SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 12, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; CROMPTON COLORS INCORPORATED; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION
Reel/Frame 042452/0759 →
RELEASE OF THIRD LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 12, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; CROMPTON COLORS INCORPORATED; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION
Reel/Frame 042452/0894 →
RELEASE OF FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042447/0508 →
RELEASE OF SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042449/0001 →
AMENDED AND RESTATED SECOND LIEN INTELLECTUAL PROPERY SECURITY AGREEMENT Recorded Jul 18, 2014
From: CHEMTURA CORPORATION; CROMPTON COLORS INCORPORATED; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION
To: BANK OF AMERICA, N.A.
Reel/Frame 033360/0225 →
THIRD LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jul 18, 2014
From: CHEMTURA CORPORATION; CROMPTON COLORS INCORPORATED; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION
To: BANK OF AMERICA, N.A.
Reel/Frame 033360/0325 →
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT. Recorded Mar 21, 2011
From: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 026028/0622 →
INTELLECTUAL PROPERTY SECURITY RELEASE AGREEMENT Recorded Mar 21, 2011
From: CITIBANK, N.A.
To: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; ASCK, INC; BIOLAB COMPANY STORE, LLC; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIOLAB TEXTILES ADDITIVES, LLC; BIOLAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON MONOCHEM, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GT SEED TREATMENT, INC.; ISCI, INC; GREAT LAKES CHEMICAL GLOBAL, INC.; HOMECARE LABS, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; NAUGATUCK TREATMENT COMPANY; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); MONOCHEM, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC; WRL OF INDIANA, INC.; BIOLAB FRANCHISE COMPANY, LLC
Reel/Frame 026039/0142 →
AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Feb 22, 2010
From: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; AQUA CLEAR INDUSTRIES, LLC; ASCK, INC.; ASEPSIS, INC.; BIOLAB COMPANY STORE, LLC; BIOLAB FRANCHISE COMPANY, LLC; BIOLAB TEXTILE ADDITIVES, LLC; BIO-LAB, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; CROMPTON MONOCHEM, INC.; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; ISCI, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; MONOCHEM, INC.; NAUGATUCK TREATMENT COMPANY; RECREATIONAL WATER PRODUCTS, INC.; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); WEBER CITY ROAD LLC; WRL OF INDIANA, INC.
To: CITIBANK, N.A.
Reel/Frame 023998/0001 →