IP Library Granted Patent US 8,372,486
Granted Patent B2
US 8,372,486 · App. 11/958,171 · Granted Feb 12, 2013

Lubricated metal article

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Quick Facts
Patent No.
US 8,372,486
App. No.
11/958,171
Granted
Feb 12, 2013
Kind
B2
Abstract

Liquid hydrofluorocarbons provide low corrosivity lubrication of metallic surfaces especially at elevated temperatures.

Claims (17)

1. An article comprising a metallic surface and anamorphous liquid hydrofluorocarbon co-telomer coatingly contacting said surface, said co-telomer comprising 30-65 mol-% of monomer units derived from hexafluoropropylene and having a H:F molar ratio in the range of 0.05 to 1, and wherein said metallic surface is at a temperature in the range of 200 to 280° C.

2. The article of claim 1 wherein the viscosity of the liquid hydrofluorocarbon ranges from 1 to 10,000 cSt at 40° C.

3. The article of claim 1 wherein the liquid hydrofluorocarbon further comprises monomer units derived from tetrafluoroethylene, vinylidene fluoride, or ethylene.

4. The article of claim 3 wherein the liquid hydrofluorocarbon further comprises one or more monomer units derived from comonomers besides tetrafluoroethylene, vinylidene fluoride, or ethylene, and wherein one of tetrafluoroethylene, vinylidene fluoride, or ethylene is the predominant co-monomer.

5. The article of claim 3 wherein the total of the concentrations of vinylidene fluoride, ethylene, and tetrafluoroethylene is 10 weight % or less.

6. The article of claim 4 wherein the one or more monomer units are derived from one or more olefinically unsaturated comonomers selected from the group consisting of perfluoropropylvinyl ether, perfluoromethylvinyl ether, perfluoroisopropylvinyl ether, hexafluoroisobutylene, perfluorobutylethylene, 3,3,3-trifluoropropene, vinyl fluoride, and trifuoroethylene.

7. The article of claim 4 wherein the olefinically unsaturated co-monomer is ethylene at a concentration of ≦3 weight-%.

8. The article of claim 1 wherein the metallic surface is stainless steel.

9. A method for lubricating a metallic surface at high temperature comprising depositing a coating on a metallic surface, and heating said surface to a temperature in the range of 200 to 280° C., wherein said coating comprises an amorphous liquid hydrofluorocarbon co-telomer comprising 30-65 mol-% of monomer units derived from hexafluoropropylene and having a H:F molar ratio in the range of 0.05 to 1.

10. The method of claim 9 wherein the viscosity of the liquid hydrofluorocarbon ranges from 1 to 10,000 cSt at 40° C.

11. The method of claim 9 wherein the liquid hydrofluorocarbon further comprises monomer units derived from tetrafluoroethylene, vinylidene fluoride, or ethylene.

12. The method of claim 11 wherein the liquid hydrofluorocarbon further comprises one or more monomer units derived from comonomers besides tetrafluoroethylene, vinylidene fluoride, or ethylene, and wherein one of tetrafluoroethylene, vinylidene fluoride, or ethylene is the predominant co-monomer.

13. The method of claim 11 wherein the total of the concentrations of vinylidene fluoride, ethylene, and tetrafluoroethylene is 10 weight % or less.

14. The method of claim 12 wherein the one or more monomer units are derived from one or more olefinically unsaturated comonomers selected from the group consisting of perfluoropropylvinyl ether, perfluoromethylvinyl ether, perfluoroisopropylvinyl ether, hexafluoroisobutylene, perfluorobutylethylene, 3,3,3-trifluoropropene, vinyl fluoride, and trifuoroethylene.

15. The method of claim 12 wherein the olefinically unsaturated co-monomer is ethylene at a concentration of ≦3 weight-%.

16. The method of claim 9 wherein the metallic surface is stainless steel.

17. The method of claim 9 wherein the step of coating the metallic surface preceeds the step of heating the surface to a temperature in the range of 200-280° C.

Assignments (5)
SECURITY INTEREST Recorded Apr 4, 2018
From: THE CHEMOURS COMPANY FC, LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 045846/0011 →
RELEASE OF SECURITY INTEREST Recorded Apr 4, 2018
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: THE CHEMOURS COMPANY FC, LLC
Reel/Frame 045845/0913 →
SECURITY AGREEMENT Recorded Jun 10, 2015
From: THE CHEMOURS COMPANY FC LLC; THE CHEMOURS COMPANY TT, LLC
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 035839/0675 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 15, 2015
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: THE CHEMOURS COMPANY FC, LLC
Reel/Frame 035432/0023 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 19, 2008
From: BELL, GREGORY A.; HOWELL, JON LEE; WHELAND, ROBERT CLAYTON; JONES, CLAY WOODWARD
To: E. I. DU PONT DE NEMOURS AND COMPANY
Reel/Frame 020674/0500 →