IP Library Granted Patent US 8,115,000
Granted Patent B2
US 8,115,000 · App. 11/995,223 · Granted Feb 14, 2012

Pyrazine derivatives and uses thereof in renal monitoring

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Quick Facts
Patent No.
US 8,115,000
App. No.
11/995,223
Granted
Feb 14, 2012
Kind
B2
Abstract

The present invention relates to pyrazine derivatives such as those represented by Formulas (I) and (II) below. X 1 to X 4 of the compounds of Formulas I and II may be characterized as electron withdrawing groups. In contrast, Y 1 to Y 4 of the compounds of Formulas I and II may be characterized as electron donating groups. Pyrazine derivatives of the present invention may be utilized in assessing renal function. In particular, an effective amount of a pyrazine derivative of the invention may be administered into a body of a patient. The pyrazine derivative that is in the body may be exposed to visible and/or infrared light to cause spectral energy to emanate from the pyrazine derivative. This emanating spectral energy may be detected and utilized to determine renal function of the patient.

Claims (24)

1. A compound of Formula I, wherein:

X 1 and X 2 are independently —CO(AA);

Y 1 and Y 2 are independently —OR 10 , —SR 11 , —NR 12 R 13 , —N(R 14 )COR 15 , —P(R 16 ) 2 or —P(OR 17 ) 2 ,

R 10 to R 17 are independently —H, —(CH 2 ) a OR 43 , —CH 2 (CHOH) a R 44 , —CH 2 (CHOH) a CO 2 H, —(CHCO 2 H) a CO 2 H, —(CH 2 ) a NR 45 R 46 , —CH[(CH 2 ) b NH 2 ] a CO 2 H, —CH[(CH 2 ) b NH 2 ] a CH 2 OH, —CH 2 (CHNH 2 ) a CH 2 NR 47 R 48 , —(CH 2 CH 2 O) c R 49 , —(CH 2 ) d CO(CH 2 CH 2 O) c R 50 , —(CH 2 ) a SO 3 H, —(CH 2 ) a SO 3 − , —(CH 2 ) a OSO 3 H, —(CH 2 ) a OSO 3 − , —(CH 2 ) a NHSO 3 H, —(CH 2 ) a NHSO 3 − , —(CH 2 ) a PO 3 H 2 , —(CH 2 ) a PO 3 H − , —(CH 2 ) a PO 3 = , —(CH 2 ) a OPO 3 H 2 , —(CH 2 ) a OPO 3 H − and —(CH 2 ) a OPO 3 ;

R 43 to R 50 are independently —H or —CH 3 ;

(AA) is a polypeptide chain comprising one or more natural or unnatural α-amino acids linked together by peptide bonds; and

‘a’, ‘b’, and ‘d’ independently vary from 1 to 10, and ‘c’ varies from 1 to 100.

2. The compound of claim 1 , wherein Y 1 and Y 2 are each independently —NR 12 R 13 .

3. The compound of claim 1 , wherein R 10 to R 17 are independently —H, —(CH 2 ) a OR 43 , —CH 2 (CHOH) a R 44 , —(CH 2 ) a NR 45 R 46 , —(CH 2 CH 2 O) c R 49 , or —(CH 2 ) d CO(CH 2 CH 2 O) d R 50 .

4. The compound of claim 1 , wherein R 10 to R 17 are independently —H, —(CH 2 ) a OR 43 , —CH 2 (CHOH) a R 44 , —(CH 2 ) a NR 45 R 46 , or —(CH 2 ) d CO(CH 2 CH 2 O) d R 50 .

5. The compound of claim 1 , wherein ‘a’, ‘b’, and ‘d’ independently vary from 1 to 6.

6. The compound of claim 1 , wherein ‘c’ varies from 1 to 20.

7. The compound of claim 1 , wherein the one or more α-amino acids of the polypeptide chain (AA) are selected from aspartic acid, asparigine, arginine, histidine, lysine, glutamic acid, glutamine, serine, and homoserine.

8. The compound of claim 1 , wherein the one or more α-amino acids of the polypeptide chain (AA) are selected from aspartic acid, glutamic acid, serine, and homoserine.

9. The compound of claim 1 , wherein the polypeptide chain (AA) is a homopolypeptide chain.

10. The compound of claim 1 , wherein the polypeptide chain (AA) is a heteropolypeptide chain.

11. The compound of claim 1 , wherein the polypeptide chain (AA) is aspartic acid or serine.

12. The compound of claim 2 , wherein each of R 12 and R 13 is —H.

13. The compound of claim 1 , wherein each (AA) is a single natural or unnatural α-amino acid.

14. The compound of claim 2 , wherein each (AA) is a single natural or unnatural α-amino acid.

15. The compound of claim 12 , wherein each (AA) is a single natural or unnatural α-amino acid.

16. The compound of claim 1 , wherein each (AA) is serine.

17. The compound of claim 16 , wherein each of Y 1 and Y 2 is —NR 12 R 13 .

18. The compound of claim 17 , wherein each of R 12 and R 13 is —H.

Assignments (6)
ENTITY CONVERSION Recorded Feb 7, 2025
From: MEDIBEACON, INC.
To: MEDIBEACON INC.
Reel/Frame 070149/0242 →
ENTITY CONVERSION Recorded Oct 13, 2015
From: MEDIBEACON, LLC
To: MEDIBEACON, INC.
Reel/Frame 036852/0201 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 10, 2014
From: MALLINCKRODT LLC
To: MEDIBEACON DEVELOPMENT, LLC
Reel/Frame 032186/0430 →
CHANGE OF NAME Recorded Feb 10, 2014
From: MEDIBEACON DEVELOPMENT, LLC
To: MEDIBEACON, LLC
Reel/Frame 032186/0495 →
CHANGE OF LEGAL ENTITY Recorded Aug 16, 2011
From: MALLINCKRODT INC.
To: MALLINCKRODT LLC
Reel/Frame 026754/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 10, 2008
From: RAJAGOPALAN, RAGHAVAN; DORSHOW, RICHARD B.; NEUMANN, WILLIAM L.
To: MALLINCKRODT INC.
Reel/Frame 020347/0167 →