IP Library Granted Patent US 7,851,502
Granted Patent B2
US 7,851,502 · App. 12/053,442 · Granted Dec 14, 2010

Pharmaceutical formulations containing an SGLT2 inhibitor

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Quick Facts
Patent No.
US 7,851,502
App. No.
12/053,442
Granted
Dec 14, 2010
Kind
B2
Abstract

Pharmaceutical formulations are provided which are in the form of capsules or tablets for oral use and which include a medicament dapagliflozin or its propylene glycol hydrate and a pharmaceutical acceptable carrier therefor, which formulation is designed for immediate release.

Claims (41)

1. A pharmaceutical formulation comprising:

a) dapagliflozin propylene glycol hydrate, wherein the dapagliflozin propylene glycol hydrate is present in an amount within the range of from about 0.1% to about 15% by weight of tablet or capsule fill;

b) microcrystalline cellulose, wherein the microcrystalline cellulose is present in an amount sufficient to make the total weight of the tablet or capsule fill 100%;

c) lactose, wherein the lactose is present in an amount within the range of from about 10% to about 30% by weight of tablet or capsule fill;

d) crospovidone, wherein the crospovidone is present in an amount within the range of from about 3% to about 10% by weight of tablet or capsule fill;

e) silicon dioxide, wherein the silicon dioxide is present in an amount within the range of from about 0.5% to about 4% by weight of tablet or capsule fill; and

f) magnesium stearate, wherein the magnesium stearate is present in an amount within the range of from about 0.5% to about 2% by weight of tablet or capsule fill;

wherein the pharmaceutical formulation is in a form selected from the group consisting of a tablet, a stock granulation, and a capsule and wherein the pharmaceutical formulation is an immediate release formulation.

2. The formulation as defined in claim 1 , wherein said formulation is in the form of a 1.0 mg tablet comprising:

a) dapagliflozin propylene glycol hydrate, wherein the dapagliflozin propylene glycol hydrate is present in an amount of 1.23 mg;

b) microcrystalline cellulose, wherein the microcrystalline cellulose is present in an amount of about 50 mg to about 90 mg;

c) lactose, wherein the lactose is present in an amount of about 10 mg to about 30 mg;

d) crospovidone, wherein the crospovidone is present in an amount of about 2 mg to about 10 mg;

e) silicon dioxide, wherein the silicon dioxide is present in an amount of about 0.5 mg to about 4.0 mg;

f) magnesium stearate, wherein the magnesium stearate is present in an amount of about 0.5 mg to about 2.0 mg; and

g) an antioxidant and/or chelating agent, wherein the antioxidant and/or chelating agent is present in an amount of about 0 mg to about 0.5 mg.

3. The formulation as defined in claim 1 , wherein said formulation is in the form of a 2.5 mg tablet comprising:

a) dapagliflozin propylene glycol hydrate, wherein the dapagliflozin propylene glycol hydrate is present in an amount of 3.075 mg;

b) microcrystalline cellulose, wherein the microcrystalline cellulose is present in an amount of about 60 mg to about 115 mg;

c) lactose, wherein the lactose is present in an amount of about 12.5 mg to about 38 mg;

d) crospovidone, wherein the crospovidone is present in an amount of about 2.5 mg to about 13 mg;

e) silicon dioxide, wherein the silicon dioxide is present in an amount of about 0.6 mg to about 5.0 mg;

f) magnesium stearate, wherein the magnesium stearate is present in an amount of about 0.6 mg to about 2.5 mg; and

g) an antioxidant and/or chelating agent, wherein the antioxidant and/or chelating agent is present in an amount of about 0 mg to about 0.6 mg.

4. The formulation as defined in claim 1 , wherein said formulation is in the form of a 5.0 mg tablet comprising:

a) dapagliflozin propylene glycol hydrate, wherein the dapagliflozin propylene glycol hydrate is present in an amount of 6.15 mg;

b) microcrystalline cellulose, wherein the microcrystalline cellulose is present in an amount of about 60 mg to about 115 mg;

c) lactose, wherein the lactose is present in an amount of about 12.5 mg to about 38 mg;

d) crospovidone, wherein the crospovidone is present in an amount of about 2.5 mg to about 13 mg;

e) silicon dioxide, wherein the silicon dioxide is present in an amount of about 0.6 mg to about 5.0 mg;

f) magnesium stearate, wherein the magnesium stearate is present in an amount of about 0.6 mg to about 2.5 mg; and

g) an antioxidant and/or chelating agent, wherein the antioxidant and/or chelating agent is present in an amount of about 0 mg to about 0.6 mg.

5. The formulation as defined in claim 1 , wherein said formulation is in the form of a 10 mg tablet comprising:

a) dapagliflozin propylene glycol hydrate, wherein the dapagliflozin propylene glycol hydrate is present in an amount of 12.3 mg;

b) microcrystalline cellulose, wherein the microcrystalline cellulose is present in an amount of about 120 mg to about 230 mg;

c) lactose, wherein the lactose is present in an amount of about 25 mg to about 75 mg;

d) crospovidone, wherein the crospovidone is present in an amount of about 5 mg to about 25 mg;

e) silicon dioxide, wherein the silicon dioxide is present in an amount of about 1.0 mg to about 10 mg;

f) magnesium stearate, wherein the magnesium stearate is present in an amount of about 1.0 mg to about 5 mg; and

g) an antioxidant and/or chelating agent, wherein the antioxidant and/or chelating agent is present in an amount of about 0 mg to about 1.25 mg.

6. The pharmaceutical formulation as in any one of claims 1 - 5 , wherein the dapagliflozin propylene glycol hydrate is

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE ADDRESS PREVIOUSLY RECORDED ON REEL 032541 FRAME 0698. ASSIGNOR(S) HEREBY CONFIRMS THE ADDRESS OF THE ASSIGNEE SHOULD BE SE-151 85, SODERTALJE, SWEDEN. Recorded May 9, 2014
From: BRISTOL-MYERS SQUIBB COMPANY
To: ASTRAZENECA AB
Reel/Frame 032858/0978 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 27, 2014
From: BRISTOL-MYERS SQUIBB COMPANY
To: ASTRAZENECA AB
Reel/Frame 032541/0698 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2008
From: BINDRA, DILBIR S.; DALI, MANDAR V; PARAB, PRAKASH V.; PATEL, JATIN M.; TAO, LI; TEJWANI, RAVINDRA W.; VATSARAJ, NIPA; WU, YONGMEI
To: BRISTOL-MYERS SQUIBB COMPANY
Reel/Frame 021015/0307 →