High-pressure tubing
View Patent ↗A method for making conduits includes inserting an inner tube into an outer tube and melting a portion of the inner tube to form a bond with the outer tube. The inner tube includes a polymeric material and the outer tube includes a material having a greater yield strength than the polymeric material. A conduit includes one or more inner tubes at least one of which is melt-bonded to one or more outer tubes. An analytical instrument includes a separation column, a solvent reservoir and pump, a sample injector, a detector to observe an eluent of the separation column, and tubing to transport fluid between components of the instrument.
1. A method for making tubing, comprising:
providing an inner tube comprising a polymeric material;
providing an outer tube comprising a material having a greater yield strength than the polymeric material;
inserting at least a portion of the inner tube into the outer tube; and
bonding the inner tube to the outer tube, wherein bonding comprises melting at least a first portion of the polymeric material of the inner tube after inserting, wherein the melted first portion of the polymeric material of the inner tube is adjacent to an end of the outer tube and wherein extracting heat comprises extracting sufficient heat to maintain a passageway through a lumen defined by the interior surface of the inner tube, wherein extracting heat comprises extracting sufficient heat to maintain a passageway through a lumen defined by the interior surface of the inner tube, and wherein extracting heat further comprises maintaining a substantially solid inner surface of the inner tube, and wherein extracting heat comprises flowing a fluid comprising a substantially inert gas through the lumen of the inner tube.
2. The method of claim 1 , wherein the melted first portion of the polymeric material forms a bond that substantially prevents fluid leakage along an interface between the outer and inner tubes.
3. The method of claim 1 , wherein the melted first portion of the polymeric material substantially surrounds the inner tube.
4. The method of claim 1 , wherein bonding comprises melting the first portion and a second portion of the polymeric material, wherein the first and second portions are adjacent to opposite ends of the outer tube and bound an unmelted portion of the inner tube.
5. The method of claim 1 , wherein melting comprises heating portions of the outer tube adjacent to opposite ends of the outer tube without substantially heating an intermediate portion of the outer tube.
6. The method of claim 1 , wherein providing the inner tube comprises selecting a length of the inner tube to be greater than a length of the outer tube.
7. The method of claim 6 , wherein the length of the inner tube is selected to accommodate shrink-back of the inner tube during bonding.
8. The method of claim 6 , wherein inserting comprises disposing the inner tube in the outer tube so that opposite end portions of the inner tube extend beyond associated ends of the outer tube.
9. The method of claim 8 , further comprising trimming the end portions of the inner tube substantially flush with the ends of the outer tube after bonding.
10. The method of claim 1 , wherein bonding comprises maintaining an unmelted portion of the polymeric material of the inner tube in a substantially solid state while melting the first portion of the polymeric material of the inner tube.
11. The method of claim 1 , wherein a combined mechanical strength of the bonded outer and inner tubes is sufficient to perform liquid chromatography at a pressure of about 15 Kpsi or greater.
12. The method of claim 1 , wherein providing the inner tube comprises providing a plurality of inner tubes, and inserting comprises inserting the plurality of inner tubes in a serial or a parallel arrangement.
13. The method of claim 1 , wherein the material of the outer tube comprises a material selected from the group of materials consisting of steel, titanium, and silica.