IP Library Granted Patent US 8,241,648
Granted Patent B2
US 8,241,648 · App. 12/073,230 · Granted Aug 14, 2012

Amphiphilic or lipophilic polar functionalized fullerenes and their uses

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Quick Facts
Patent No.
US 8,241,648
App. No.
12/073,230
Granted
Aug 14, 2012
Kind
B2
Abstract

Described herein are synthetically modified fullerene molecules, wherein the fullerene is preferably ellipsoid in shape with an equatorial band and two opposing poles, comprising an adduct at one or both poles, at least one adduct being a hydrophobic chemical moiety capable of anchoring the fullerene on or in a lipid membrane.

Claims (23)

1. A synthetically modified fullerene molecule having the formula

Z m —F—Y n ;

wherein F is fullerene of formula C p , the fullerene having two opposing poles and an equatorial region;

Z and Y are positioned near respective opposite poles of C p ;

m=1-5 and Z is a hydrophilic chemical moiety;

n=1-5 and Y is a lipophilic chemical moiety;

p=60-120 and p is an even number.

2. The synthetically modified fullerene of claim 1 , wherein each chemical moiety Z is composed of formula A r B in which A is a hydrophilic chemical moiety, r=1-4, and B is a chemical linker connecting said A to the fullerene, and each chemical moiety Y is composed of formula DE v in which E is a lipophilic chemical moiety and, v=1-4, and D is a chemical linker connecting the lipophilic chemical moiety to the fullerene.

3. The synthetically modified fullerene of claim 1 , wherein F is a prolate ellipsoid shaped fullerene having a major axis and said poles are located at opposing ends of the major axis of the prolate ellipsoid fullerene.

4. The synthetically modified fullerene of claim 1 , wherein Z and Y are configured such that when the molecule is contacted with a lipid bilayer in an aqueous medium, the equatorial region of F is selectively located within or in close proximity to the bilayer.

5. The synthetically modified fullerene of claim 2 , wherein Z and Y are configured such that when the molecule is contacted with a lipid bilayer in an aqueous medium, the equatorial region of F is selectively located within or in close proximity to the bilayer.

6. The synthetically modified fullerene of claim 1 , wherein the molecule in an extended configuration has an aspect ratio of about 2.1 to 15, and a diameter less than about 2 nm.

7. The synthetically modified fullerene of claim 2 , wherein the molecule in an extended configuration has an aspect ratio of about 2.1 to 15, and a diameter less than about 2 nm.

8. The synthetically modified fullerene of claim 1 , wherein p=60.

9. The synthetically modified fullerene of claim 1 , wherein p=70.

10. A therapeutic or cosmetic composition comprising the synthetically modified fullerene of claim 1 uniformly dispersed within phospholipid bilayers.

11. A composition of claim 10 , in which the molar ratio of fullerene to phospholipid is from about 1:10 to 1:2.

12. A topical composition in the form of a ointment, cream, lotion, moisturized patch or moisture-free patch, shampoo, gel, rinse, face lotion, milky lotion, paste, shaving cream, foundation, cologne, or pack comprising a synthetically modified fullerene according to claim 1 .

13. A synthetic fullerene molecule having the formula Z(C 70 )Y; wherein Y is a lipophilic moiety covalently connected to C 70 , optionally through a linking group, near a pole thereof, and wherein Z is a hydrophilic moiety covalently connected to C 70 , optionally through a linking group, at or near a pole opposite to said Y; and, wherein said lipophilic moiety Y is capable of anchoring the synthetic fullerene molecule to a lipid membrane.

14. A composition comprising a plurality of synthetic fullerene molecules according to claim 13 uniformly dispersed in phospholipids.

15. A topical composition in the form of a ointment, cream, lotion, moisturized patch or moisture-free patch, shampoo, gel, rinse, face lotion, milky lotion, paste, shaving cream, foundation, cologne, or pack comprising a synthetic fullerene molecule according to claim 13 .

16. A composition comprising in a pharmaceutically acceptable medium, a synthetic fullerene molecule according to claim 13 and another pharmaceutical molecule.

17. The composition of claim 16 , wherein the pharmaceutical molecule is insulin.

Assignments (9)
RELEASE OF SECURITY INTEREST Recorded Jan 29, 2026
From: M&T BANK
To: LUNA LABS USA, LLC
Reel/Frame 073628/0060 →
RELEASE OF SECURITY INTEREST Recorded Mar 25, 2022
From: PNC BANK, NATIONAL ASSOCIATION
To: LUNA LABS USA, LLC
Reel/Frame 059396/0791 →
SECURITY INTEREST Recorded Mar 9, 2022
From: LUNA LABS USA, LLC
To: M&T BANK
Reel/Frame 059211/0861 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2022
From: LUNA INNOVATIONS INCORPORATED
To: LUNA LABS USA, LLC
Reel/Frame 059109/0181 →
SECURITY INTEREST Recorded Mar 4, 2021
From: LUNA INNOVATIONS INCORPORATED; FORMER LUNA SUBSIDIARY, INC.; GENERAL PHOTONICS CORP.
To: PNC BANK, NATIONAL ASSOCIATION
Reel/Frame 056455/0331 →
RELEASE OF SECURITY INTEREST Recorded Dec 9, 2013
From: HANSEN MEDICAL, INC.
To: LUNA INNOVATIONS INCORPORATED
Reel/Frame 031784/0755 →
SECURITY AGREEMENT Recorded Feb 25, 2010
From: LUNA INNOVATIONS INCORPORATED
To: SILICON VALLEY BANK
Reel/Frame 023985/0718 →
SECURITY AGREEMENT Recorded Jan 14, 2010
From: LUNA INNOVATIONS INCORPORATED
To: HANSEN MEDICAL, INC.
Reel/Frame 023792/0388 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 8, 2008
From: ZHOU, ZHIGUO; LENK, ROBERT P.; MACFARLAND, DARREN; WALKER, KENNETH L.; ZHANG, JING; WILSON, STEPHEN R.
To: LUNA INNOVATIONS INCORPORATED
Reel/Frame 020927/0778 →