IP Library Granted Patent US 7,785,038
Granted Patent B2
US 7,785,038 · App. 12/089,735 · Granted Aug 31, 2010

Oxidation of organic compounds

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Quick Facts
Patent No.
US 7,785,038
App. No.
12/089,735
Granted
Aug 31, 2010
Kind
B2
Abstract

An improved method and compositions for treating organic compounds present in soil, groundwater and other environments is disclosed. The method involves the use of a composition comprising a solid state, water soluble peroxygen compound and zero valent iron.

Claims (13)

1. A method of oxidizing a contaminant present in an environmental medium, said method comprising contacting the contaminant with a composition comprising a water soluble persulfate compound and zero valent iron wherein the persulfate compound is a dipersulfate.

2. A method as in claim 1 , wherein the dipersulfate is selected from sodium, potassium or ammonium persulfate or a combination thereof.

3. A method as in claim 1 , wherein the persulfate compound is a combination of a dipersulfate and monopersulfate.

4. A method as in claim 1 , wherein the environmental medium is selected from soil, groundwater, process water or wastewater.

5. A method as in claim 1 , wherein the contaminant is an organic compound selected from the group consisting of volatile organic compounds, semi-volatile organic compounds, polyaromatic hydrocarbons, polychlorobiphenyls, pesticides and herbicides.

6. A method as in claim 1 wherein the zero valent iron has a nanoscale particle size of from about 10 nanometers to about 1 micron.

7. A method as in claim 1 wherein the zero valent iron has a micro scale particle size of from about 1 micron to about 5 microns.

8. A method as in claim 1 wherein the concentration of the persulfate compound is from about 0.5 mg/L to about 250,000 mg/L.

9. A method as in claim 1 wherein the concentration of the zero valent iron is from about 1 ppm to about 1000 ppm on a metal basis.

10. A method as in claim 1 wherein the oxidation is performed in situ or ex situ.

11. A method as in claim 1 wherein the water soluble persulfate compound is sodium persulfate.

12. A method as in claim 11 wherein the zero valent iron and the sodium persulfate are present in a suspension.

13. A method as in claim 5 wherein the organic compound is selected from the group consisting of trichioroethylene (TCE), vinyl chloride, tetrachloroethylene (PCE), methylene chloride, 1,2-dichloroethane, 1,1,1-trichloroethane (TCA), carbon tetrachloride, chloroform, chlorobenzenes, benzene, toluene, xylene, ethyl benzene, ethylene dibromide, methyl tertiary butyl ether, polyaromatic hydrocarbons, polychlorobiphenyls, phthalates, I,4-dioxane, nitrosodimethyl amine, and methyl tertbutyl ether.

Assignments (12)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 24, 2024
From: EVONIK ACTIVE OXYGENS, LLC
To: EVONIK CORPORATION
Reel/Frame 069002/0662 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THE ASSIGNEE'S NAME PREVIOUSLY RECORDED AT REEL: 061456 FRAME: 0614. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 12, 2023
From: PEROXYCHEM LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 063632/0389 →
CHANGE OF ADDRESS Recorded May 10, 2023
From: EVONIK ACTIVE OXYGENS, LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 063602/0729 →
CHANGE OF NAME Recorded Sep 16, 2022
From: PEROXYCHEM LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 061456/0614 →
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 050605/0305 Recorded Feb 3, 2020
From: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
To: PEROXYCHEM LLC
Reel/Frame 051777/0957 →
RELEASE OF SECURITY INTEREST Recorded Oct 2, 2019
From: BANK OF AMERICA, N.A., AS AGENT
To: PEROXYCHEM LLC
Reel/Frame 050606/0329 →
SECURITY INTEREST Recorded Oct 2, 2019
From: PEROXYCHEM LLC
To: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
Reel/Frame 050605/0305 →
RELEASE OF SECURITY INTEREST Recorded Nov 4, 2015
From: MACQUARIE US TRADING LLC, AS COLLATERAL AGENT
To: PEROXYCHEM LLC
Reel/Frame 036953/0766 →
SECURITY INTEREST Recorded Oct 21, 2015
From: PEROXYCHEM LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036847/0594 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2014
From: FMC CORPORATION
To: PEROXYCHEM LLC
Reel/Frame 032558/0681 →
SHORT FORM PATENT SECURITY AGREEMENT Recorded Mar 3, 2014
From: PEROXYCHEM LLC
To: MACQUARIE US TRADING LLC
Reel/Frame 032379/0931 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 20, 2009
From: BLOCK, PHILIP A.; BROWN, RICHARD A.
To: FMC CORPORATION
Reel/Frame 023123/0946 →