IP Library Granted Patent US 7,920,258
Granted Patent B2
US 7,920,258 · App. 12/094,475 · Granted Apr 5, 2011

Optical analysis system and elements to isolate spectral region

Assignee: Halliburton Energy Services, Inc.
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Quick Facts
Patent No.
US 7,920,258
App. No.
12/094,475
Granted
Apr 5, 2011
Kind
B2
Abstract

A method of selecting components for a multivariate optical computing and analysis system to isolate a spectral region includes selecting a spectral region of interest; selecting a spectral element with a predetermined transmission characteristic to control a spectral range of an illumination source; illuminating a sample with the illumination source; and analyzing an optical frequency returned by the sample relative to the spectral region of interest.

Claims (39)

1. A method of selecting components for a multivariate optical computing and analysis system to isolate a spectral region, the method comprising:

selecting a spectral region of interest;

selecting a spectral element with a predetermined transmission characteristic to control a spectral range of an illumination source; the spectral element being made of a solid state material;

illuminating a sample with the illumination source;

analyzing an optical frequency returned by the sample relative to the spectral region of interest; and

controlling at least one of a cut-on wavelength or a cut-off wavelength by altering a thickness of the solid state material.

2. The method as in claim 1 , wherein the spectral region of interest is a near IR region of about 700 nm to about 3500 nm.

3. The method as in claim 1 , wherein the spectral region of interest is a visible/ultraviolet region of about 200 nm to about 1000 nm.

4. The method as in claim 1 , wherein the spectral region of interest is a mid IR region of about 200 nm to about 1000 nm.

5. The method as in claim 1 , wherein the spectral element is a plurality of spectral elements and at least one of the spectral elements is a multivariate optical element.

6. A method of selecting components for a multivariate optical computing and analysis system to isolate a spectral region, the method comprising:

selecting a spectral region of interest;

selecting a spectral element with a predetennined transmission characteristic to control a spectral range of an illumination source; the spectral element being made of a chemical material;

illuminating a sample with the illumination source;

analyzing an optical frequency returned by the sample relative to the spectral region of interest; and

deleting an absorbance of a gas from an optical spectrum of a sample, the gas being an interferent or the gas being ambient in the system.

7. The method as in claim 6 , further comprising pressurizing the gas.

8. The method as in claim 6 , further comprising placing the gas in a high- pressure cell.

9. The method as in claim 6 , further comprising dissolving the gas in a fluid.

10. A method of selecting components for a multivariate optical computing and analysis system to isolate a spectral region, the method comprising:

selecting a spectral region of interest;

selecting a spectral element with a predetermined transmission characteristic to control a spectral range of an illumination source;

illuminating a sample with the illumination source; and

analyzing an optical frequency returned by the sample relative to the spectral region of interest;

wherein the spectral element is made of a mixture of materials.

11. The method as in claim 10 , wherein the mixture of materials includes a solution of a gas in a solid material.

12. The method as in claim 10 , wherein the mixture of materials includes a dispersion of a liquid in a solid material.

13. The method as in claim 10 , wherein the mixture of materials includes a clathrate-type material.

14. A method of selecting components for a multivariate optical computing and analysis system to isolate a spectral region, the method comprising:

selecting a spectral region of interest;

selecting a spectral element with a predetermined transmission characteristic to control a spectral range of an illumination source;

illuminating a sample with the illumination source; and

analyzing an optical frequency returned by the sample relative to the spectral region of interest;

wherein the spectral element is made of a synthetic material.

15. The method as in claim 14 , further comprising stabilizing a spectral characteristic of the synthetic material in a transmissive region.

16. The method as in claim 14 , further comprising analyzing a performance of the synthetic material and accounting for a characteristic of the synthetic material.

17. The method as in claim 14 , further comprising analyzing a performance of the synthetic material and incorporating a variation based on the synthetic material into a design of a multivariate optical element.

18. The method as in claim 1 , further comprising selecting the spectral element for a detector, the spectral element being configured to minimize a band-edge effect in the spectral region of interest.

19. The method as in claim 1 , further comprising blocking a band-edge region in the spectral region of interest using a filtering medium.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 14, 2011
From: UNIVERSITY OF SOUTH CAROLINA
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 025790/0442 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 3, 2008
From: MYRICK, MICHAEL L.; FREESE, ROBERT P.; PROFETA, LUISA T.M.; JAMES, JONATHAN H.; BLACKBURN, JOHN C.; PRIORE, RYAN J.
To: UNIVERSITY OF SOUTH CAROLINA
Reel/Frame 021629/0433 →
Continuity (3)
Provisional Application 60740179 · Nov 28, 2005
Provisional Application 60740180 · Nov 28, 2005
Related Publication 20090219512A1 · Sep 3, 2009