IP Library Granted Patent US 7,641,979
Granted Patent B2
US 7,641,979 · App. 12/113,167 · Granted Jan 5, 2010

Poly(vinyl butyral) pellets

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Quick Facts
Patent No.
US 7,641,979
App. No.
12/113,167
Granted
Jan 5, 2010
Kind
B2
Abstract

The present invention is in the field of thermoplastic polymeric compositions, and, specifically, the present invention is in the field of poly(vinyl butyral) formation, storage, and use in multiple layer glazing panel interlayers, among other uses.

Claims (30)

1. A method of manufacturing a multiple layer glazing panel, comprising the steps:

providing a thermoplastic polymer pellet comprising plasticized poly(vinyl butyral) and an antiblocking agent;

heating said pellet to form a melt; and,

extruding said melt to form a polymer layer, wherein said polymer layer is disposed between two glazing panes, wherein said antiblocking agent is a fatty acid amide having the general formula:

wherein R defines an anti-blocking segment comprising a hydrocarbon chain having about 12 to about 40 carbon atoms, and R′ defines H or a hydrocarbon chain having 1 to about 40 carbon atoms.

2. The method of claim 1 , wherein said fatty acid amide is selected from the group consisting of erucamide, behenamide, oleyl palmitamide, stearyl erucamide, erucyl stearamide, hydroxystearamide, oleic acid diethanolamide, stearic acid diethanolamide, poly(ethylene glycol) oleic amide, octadecanamide, and mixtures of the foregoing.

3. The method of claim 1 , wherein said fatty acid amide is a mono-amide.

4. The method of claim 1 , wherein said fatty acid amide is a secondary mono-amide.

5. The method of claim 1 , wherein said fatty acid amide is 0.001 to 6.0 weight percent of said pellet.

6. The method of claim 1 , wherein said fatty acid amide is 0.01 to 0.6 weight percent of said pellet.

7. The method of claim 1 , wherein said fatty acid amide is 0.1 to 0.3 weight percent of said pellet.

8. The method of claim 1 , wherein said fatty acid amide is N-oleyl palmitamide.

9. The method of claim 8 , wherein said fatty acid amide is 0.001 to 6.0 weight percent of said pellet.

10. The method of claim 8 , wherein said fatty acid amide is 0.01 to 0.6 weight percent of said pellet.

11. The method of claim 8 , wherein said fatty acid amide is 0.1 to 0.3 weight percent of said pellet.

12. A multiple layer glazing panel produced by the method comprising the steps:

providing a thermoplastic polymer pellet comprising plasticized poly(vinyl butyral) and an antiblocking agent;

heating said pellet to form a melt; and,

extruding said melt to form a polymer layer, wherein said polymer layer is disposed between two glazing panes to form said multiple layer glazing panel, wherein said antiblocking agent is a fatty acid amide having the general formula:

wherein R defines an anti-blocking segment comprising a hydrocarbon chain having about 12 to about 40 carbon atoms, and R′ defines H or a hydrocarbon chain having 1 to about 40 carbon atoms.

13. The panel of claim 12 , wherein said fatty acid amide is selected from the group consisting of erucamide, behenamide, oleyl palmitamide, stearyl erucamide, erucyl stearamide, hydroxystearamide, oleic acid diethanolamide, stearic acid diethanolamide, poly(ethylene glycol)oleic amide, octadecanamide, and mixtures of the foregoing.

14. The panel of claim 12 , wherein said fatty acid amide is a mono-amide.

15. The panel of claim 12 , wherein said fatty acid amide is a secondary mono-amide.

16. The panel of claim 12 , wherein said fatty acid amide is 0.001 to 6.0 weight percent of said pellet.

17. The panel of claim 12 , wherein said fatty acid amide is 0.01 to 0.6 weight percent of said pellet.

18. The panel of claim 12 , wherein said fatty acid amide is 0.1 to 0.3 weight percent of said pellet.

19. The panel of claim 12 , wherein said fatty acid amide is N-oleyl palmitamide.

20. The panel of claim 19 , wherein said fatty acid amide is 0.001 to 6.0 weight percent of said pellet.

21. The panel of claim 19 , wherein said fatty acid amide is 0.01 to 0.6 weight percent of said pellet.

22. The panel of claim 19 , wherein said fatty acid amide is 0.1 to 0.3 weight percent of said pellet.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Jul 17, 2012
From: DEUTSCHE BANK TRUST COMPANY AMERICAS, AS COLLATERAL AGENT
To: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
Reel/Frame 028563/0241 →
SECURITY AGREEMENT Recorded May 17, 2010
From: SOLUTIA INC.; CP FILMS INC.; FLEXSYS AMERICA L.P.
To: DEUTSCHE BANK TRUST COMPANY AMERICAS, AS COLLATERAL AGENT
Reel/Frame 024390/0281 →
RELEASE OF ABL SECURITY INTEREST IN PATENTS - REEL/FRAME 022043/0539 Recorded Mar 23, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.
Reel/Frame 024120/0499 →
RELEASE OF TERM LOAN SECURITY INTEREST IN PATENTS RECORDED AT REEL/FRAME 022043/0533 Recorded Mar 23, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.
Reel/Frame 024120/0461 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Dec 31, 2008
From: SOLUTIA INC.
To: CITIBANK, N.A.
Reel/Frame 022043/0533 →
ABL PATENT SECURITY AGREEMENT Recorded Dec 31, 2008
From: SOLUTIA INC.
To: CITIBANK, N.A.
Reel/Frame 022043/0539 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 30, 2008
From: CHEN, WENJIE; SMITH, ANDREW NEIL; KARAGIANNIS, ARISTOTELIS
To: SOLUTIA, INC.
Reel/Frame 020882/0645 →