Close-coupled purgeable vaporizer valve
View Patent ↗A method and system are provided for an integrated fluid and vapor delivery system design that optimizes vapor delivery. The method and system utilize a purgeable valve assembly which is closely coupled to a vaporizer. The purgeable valve assembly includes a liquid control valve and a purge gas valve which are connected by an outlet to the vaporizer in a manner minimizing the dead volume of the liquid supplied to the vaporizer. The system does not require the liquid precursor to be subjected to vacuum prior to entry into the vaporizer.
1. A fluid and vapor delivery system comprising: a source of liquid precursor; a flow meter; a purgeable valve assembly comprising a liquid control valve, a gas valve, and a passageway between the liquid control valve and the gas valve, the passageway connected to a passageway outlet extending from the purgeable valve assembly; a vaporizer in fluid communication with the passageway outlet of the purgeable valve assembly; and a shutoff valve disposed downstream of the flow meter and upstream of the purgeable valve assembly; wherein the purgeable valve assembly is closely coupled to the vaporizer.
2. The fluid and vapor delivery system of claim 1 , wherein a spacer is positioned between the purgeable valve assembly and the vaporizer.
3. The fluid and vapor delivery system of claim 2 , wherein the spacer is at least partially composed of a ceramic material.
4. The fluid and vapor delivery system of claim 2 , wherein the spacer is an insulator.
5. The fluid and vapor delivery system of claim 1 , wherein the liquid precursor is not subject to vacuum prior to entering the vaporizer.
6. The fluid and vapor delivery system of claim 1 , wherein the liquid control valve and the gas valve of the purgeable valve assembly are positioned along a single axis.
7. The fluid and vapor delivery system of claim 1 , wherein the volume of the passageway and the passageway outlet is a maximum dead zone volume.
8. The fluid and vapor delivery system of claim 6 , wherein the maximum dead zone volume is less than 0.005 ml.
9. A method for providing a liquid to a vaporizer, the method comprising the steps of: providing a source of liquid to a liquid control valve of a purgeable valve assembly;
providing a flow meter;
providing a shutoff valve disposed downstream of the flow meter and upstream of the purgeable valve assembly;
closely coupling the purgeable valve assembly to the vaporizer;
opening the liquid control valve to direct a flow of liquid through a passageway of the purgeable valve assembly and into the vaporizer;
closing the liquid control valve to halt the flow of liquid into the vaporizer;
providing a source of gas to a gas valve of a purgeable valve assembly; and
opening the gas valve to direct a low flow of purge gas into the passageway of the purgeable valve assembly and into the vaporizer to sweep away liquid downstream of the liquid control valve.
10. The method of claim 9 , wherein the step of closely coupling the purgeable valve assembly to the vaporizer includes the step of spacing the purgeable valve assembly from the vaporizer using a spacer.
11. The method of claim 9 , wherein the liquid is not subjected to vacuum prior to entry into the vaporizer.
12. The method of claim 9 , comprising the step of using the flow meter with the purgeable valve assembly to optimize the pressure rise and fall of a vapor outlet manifold downstream of the vaporizer.
13. A method for providing a liquid to a vaporizer, the method comprising the steps of:
closely coupling a purgeable valve assembly to a vaporizer, the purgeable valve assembly comprising a liquid control valve and a purge gas valve;
providing a flow meter;
providing a shutoff valve disposed downstream of the flow meter and upstream of the purgeable valve assembly;
providing a source of liquid to the liquid control valve;
opening the liquid control valve to direct a flow of liquid through a passageway of the purgeable valve assembly and into the vaporizer;
closing the liquid control valve to halt the flow of liquid into the vaporizer;
providing a source of gas to the purge gas valve; and
opening the purge gas valve to direct a low flow of purge gas into the passageway of the purgeable valve assembly and into the vaporizer to sweep away liquid downstream of the liquid control valve.
14. The method of claim 13 , wherein the step of closely coupling the purgeable valve assembly to the vaporizer includes the step of spacing the purgeable valve assembly from the vaporizer using a spacer.
15. The method of claim 13 , wherein the liquid is not subjected t vacuum prior to entry into the vaporizer.
16. The method of claim 13 , comprising the step of using the flow meter with the purgeable valve assembly to optimize the pressure rise and fall of a vapor outlet manifold downstream of the vaporizer.