IP Library Granted Patent US 10,231,344
Granted Patent B2
US 10,231,344 · App. 12/121,260 · Granted Mar 12, 2019

Metallic ink

Inventors: Yunjun Li (Austin, TX); David Max Roundhill (Austin, TX); Mohshi Yang (Austin, TX); Igor Pavlovsky (Cedar Park, TX); Richard Lee Fink (Austin, TX); Zvi Yaniv (Austin, TX)
Assignees: APPLIED NANOTECH HOLDINGS, INC.; ISHIHARA CHEMICAL CO., LTD.
H05K3/02B22F1/0074B22F1/025C22C47/04C23C18/14H01B1/026B22F2999/00H05K1/0393H05K2201/0257H05K2203/0514H05K2203/107H05K2203/1131H05K2203/1545
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Quick Facts
Patent No.
US 10,231,344
App. No.
12/121,260
Granted
Mar 12, 2019
Kind
B2
Abstract

Forming a conductive film comprising depositing a non-conductive film on a surface of a substrate, wherein the film contains a plurality of copper nanoparticles and exposing at least a portion of the film to light to make the exposed portion conductive. Exposing of the film to light photosinters or fuses the copper nanoparticles.

Claims (21)

1. A method of forming a conductive layer comprising:

depositing a film containing a plurality of copper nanoparticle structures on a surface of a substrate;

exposing at least a portion of the film to light to make the exposed portion conductive, so as to form the conductive layer, wherein the exposing at least a portion of the film photosinters at least a portion of the copper nanoparticle structures, wherein the photosintering of copper nanoparticle structures comprises a photoreduction of CuO and Cu 2 O in the copper nanoparticle structures to Cu;

wherein the film is exposed to the light through a backside of the substrate which further fuses the copper nanoparticle structures with the substrate.

2. A method of forming a conductive layer comprising:

depositing a film containing a plurality of copper nanoparticle structures on a surface of a substrate;

exposing at least a portion of the film to light to make the exposed portion conductive, so as to form the conductive layer, wherein the exposing at least a portion of the film photosinters at least a portion of the copper nanoparticle structures, wherein the photosintering of copper nanoparticle structures comprises a photoreduction of CuO and Cu 2 O in the copper nanoparticle structures to Cu;

wherein the film has a viscosity in a range of 8-20 centipoise, and a surface tension in a range of 20-60 dyne/cm 2 .

3. A method of forming a conductive layer comprising:

depositing a film containing a plurality of copper nanoparticle structures on a surface of a substrate; and

exposing at least a portion of the film to light to make the exposed portion conductive, so as to form the conductive layer, wherein the exposing at least a portion of the film to light causes at least a portion of the copper nanoparticle structures to fuse together, wherein copper oxides in the copper nanoparticle structures are reduced during the fusion, wherein a loading concentration of copper oxides in the fused film does not exceed 30%, wherein the fused film has a resistivity in a range of about 10 −5 ohm-cm to 3×10 −6 ohm-cm.

4. A method of forming a conductive layer comprising:

depositing a film containing a plurality of copper nanoparticle structures on a surface of a substrate;

exposing at least a portion of the film to light to make the exposed portion conductive, so as to form the conductive layer, wherein the exposing at least a portion of the film photosinters at least a portion of the copper nanoparticle structures, wherein the photosintering of copper nanoparticle structures comprises a photoreduction of CuO and Cu 2 O in the copper nanoparticle structures to Cu;

wherein, before the exposing of at least a portion of the film, the film is non-conductive and is deposited from a solution containing the copper nanoparticle structures; and

wherein the solution comprises hexylamine.

5. A method of forming a conductive layer comprising:

depositing a film containing a plurality of copper nanoparticle structures on a surface of a substrate;

exposing at least a portion of the film to light to make the exposed portion conductive, so as to form the conductive layer, wherein the exposing at least a portion of the film photosinters at least a portion of the copper nanoparticle structures, wherein the photosintering of copper nanoparticle structures comprises a photoreduction of CuO and Cu 2 O in the copper nanoparticle structures to Cu;

wherein, before the exposing of at least a portion of the film, the film is non-conductive and is deposited from a solution containing the copper nanoparticle structures, comprising adding the copper nanoparticle structures to a solvent to form the solution prior to depositing the film; and adding a dispersant to the solution;

wherein a loading concentration of the copper nanoparticle structures in the solution is about 10%-50%, and wherein the dispersant comprises hexylamine in a loading concentration in the solution of about 1%-30%, wherein the deposited film is dried in air at about 100° C., wherein after the photosintering, the portion of the film has a resistivity in a range of about 10 −5 ohm-cm to 3×10 −6 ohm-cm.

Assignments (8)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 3, 2022
From: NANO MAGIC HOLDINGS INC.
To: APPLIED NANOTECH, INC.
Reel/Frame 060098/0228 →
CHANGE OF NAME Recorded May 25, 2022
From: PEN INC.
To: NANO MAGIC INC.
Reel/Frame 060177/0348 →
CHANGE OF NAME Recorded May 25, 2022
From: NANO MAGIC INC.
To: NANO MAGIC HOLDINGS INC.
Reel/Frame 060177/0559 →
MERGER AND CHANGE OF NAME Recorded May 24, 2022
From: APPLIED NANOTECH HOLDINGS INC.; PEN INC.
To: PEN INC.
Reel/Frame 060007/0591 →
EXCLUSIVITY AGREEMENT Recorded Oct 23, 2013
From: APPLIED NANOTECH HOLDINGS, INC.; APPLIED NANOTECH, INC.
To: ISHIHARA CHEMICAL COMPANY, LTD
Reel/Frame 031477/0086 →
CHANGE OF NAME Recorded Aug 14, 2008
From: NANO-PROPRIETARY, INC.
To: APPLIED NANOTECH HOLDINGS, INC.
Reel/Frame 021390/0009 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 14, 2008
From: APPLIED NANOTECH HOLDINGS, INC.
To: ISHIHARA CHEMICAL CO., LTD.
Reel/Frame 021390/0063 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2008
From: LI, YUNJUN; ROUNDHILL, DAVID MAX; YANG, MOHSHI; PAVLOVSKY, IGOR; FINK, RICHARD LEE; YANIV, ZVI
To: NANO-PROPRIETARY, INC.
Reel/Frame 021119/0037 →
Continuity (2)
Provisional Application 60938975 · May 18, 2007
Related Publication 20080286488A1 · Nov 20, 2008