IP Library Patent Application 12130515
Patent Application
App. No. 12/130,515

INHIBITION OF WATER FORMED SCALE IN ACID CONDITIONS

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Quick Facts
Patent No.
US None
App. No.
12/130,515
Abstract

The current invention relates to the inhibition of scale deposits in an acidic slurry or solution. The current invention uses an aqueous synthetic mixture comprising a phosphate, phosphonate, anionic polymer, or combinations thereof in the slurry and/or solution to inhibit scale during the processing of ore. The production of scale in an acidic environment is difficult because of the acidic solution neutralizing most known inhibitors. The claimed invention has a significant decrease in the scale production allowing for reduced down time of systems for de-scaling procedures.

Claims (18)

1 . A process for inhibiting the formation of scale in acid production wherein an ore is combined with an acidic solution in a digestion process to react forming an acidic slurry which is passed through a filtration process to form an acidic stream where a scale inhibiting composition is added to the acidic stream at any point from filtration onward in the acid production and evaporation processes.

2 . The process of claim 1 wherein the scale inhibiting composition is additionally added at digestion.

3 . The process of claim 1 wherein the scale inhibiting composition is additionally added to the acidic slurry.

4 . The process of claim 1 wherein the scale inhibiting composition is added to the acidic stream during evaporation.

5 . The process of claim 1 wherein the scale inhibiting composition is added to the acidic stream prior to entering the evaporation process.

6 . The process of claim 1 wherein the ore is a phosphate containing ore.

7 . The process of claim 6 wherein the acidic solution is sulfuric acid.

8 . The process of claim 1 where the scale inhibiting composition is one or a combination of an organic phosphate, a phosphonate, an inorganic phosphate, a polycarboxylate homopolymer or copolymer.

9 . The process of claim 1 where the scale inhibiting composition is added in substoichiometric amounts.

10 . The process of claim 1 where the scale inhibiting composition is added from 0.1 to 5000 ppm.

11 . The process of claim 1 where the scale inhibiting composition is added from 0.1 to 100 ppm.

12 . The process of claim 1 where the scale inhibiting composition is added from 0.1 to 50 ppm.

13 . The process of claim 1 where the scale inhibiting composition is added prior to the production of the acidic slurry.

14 . A process for inhibiting the formation of scale in acid production wherein a phosphate containing ore is combined with an acidic solution for digestion and forms an acidic slurry where a scale inhibiting composition is added to the acidic slurry at any point through the filtration process.

15 . The process of claim 14 wherein the scale inhibiting composition is added prior to digestion.

16 . The process of claim 14 wherein the phosphate containing ore is beneficiated prior to being combined with the acidic solution.

17 . The process of claim 14 wherein the acidic solution is sulfuric acid.

18 . The process of claim 14 where the scale inhibiting composition is one or a combination of an organic phosphate, a phosphonate, an inorganic phosphate, a polycarboxylate homopolymer or copolymer.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 4, 2017
From: NALCO COMPANY
To: ECOLAB USA INC.
Reel/Frame 042147/0420 →
CHANGE OF NAME Recorded Feb 28, 2017
From: NALCO COMPANY
To: NALCO COMPANY LLC
Reel/Frame 041835/0903 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2017
From: NALCO COMPANY LLC; CALGON CORPORATION; CALGON LLC; ONDEO NALCO ENERGY SERVICES, L.P.
To: ECOLAB USA INC.
Reel/Frame 041836/0437 →
RELEASE OF SECURITY INTEREST Recorded Feb 24, 2017
From: BANK OF AMERICA, N.A.
To: NALCO COMPANY
Reel/Frame 041808/0713 →
RELEASE OF SECURITY INTEREST Recorded May 26, 2015
From: BANK OF AMERICA, N.A.
To: NALCO COMPANY
Reel/Frame 035771/0668 →
SECURITY AGREEMENT Recorded May 18, 2009
From: NALCO COMPANY; CALGON LLC; NALCO ONE SOURCE LLC; NALCO CROSSBOW WATER LLC
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 022703/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 30, 2008
From: GILL, JASBIR S.; HAY, DANIEL N.T.
To: NALCO COMAPANY
Reel/Frame 021192/0182 →