IP Library Granted Patent US 8,299,025
Granted Patent B2
US 8,299,025 · App. 12/148,896 · Granted Oct 30, 2012

Suspension formulations of insulinotropic peptides and uses thereof

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Quick Facts
Patent No.
US 8,299,025
App. No.
12/148,896
Granted
Oct 30, 2012
Kind
B2
Abstract

A suspension formulation of an insulinotropic peptide (e.g., glucagon-like peptide-1 (GLP-1) or exenatide) is described. The suspension formulation comprises (i) a non-aqueous, single-phase vehicle, comprising one or more polymer and one or more one solvent, wherein the vehicle exhibits viscous fluid characteristics, and (ii) a particle formulation comprising the insulinotropic peptide, wherein the peptide is dispersed in the vehicle. The particle formulation further includes a stabilizing component comprising one or more stabilizers, for example, carbohydrates, antioxidants, amino acids, and buffers. Devices for delivering the suspension formulations and methods of use are also described.

Claims (21)

1. A suspension formulation suitable for use in an osmotic delivery device comprising,

a particle formulation comprising an insulinotropic peptide, a disaccharide, methionine, and a buffer; and

a non-aqueous, single-phase suspension vehicle that consists essentially of about 20 wt % to about 60 wt % benzyl benzoate and about 80 wt % to about 40 wt % polyvinylpyrrolidone, the suspension vehicle having a viscosity of between about 12,000 to about 18,000 poise at 33° C.;

wherein the suspension vehicle exhibits viscous fluid characteristics, and the particle formulation is dispersed in the vehicle.

2. The formulation of claim 1 , wherein the insulinotropic peptide is a glucagon-like peptide-1 (GLP-1), a derivative of GLP-1, or an analogue of GLP-1.

3. The formulation of claim 2 , wherein the insulinotropic peptide is GLP-1(7-36) amide.

4. The formulation of claim 1 , wherein the insulinotropic peptide is exenatide, a derivative of exenatide, or an analogue of exenatide.

5. The formulation of claim 4 , wherein the insulinotropic peptide is exenatide having the amino acid sequence of SEQ ID NO:2.

6. The formulation of claim 1 , wherein the buffer is selected from the group consisting of citrate, histidine, succinate, and mixtures thereof.

7. The formulation of claim 6 , wherein the buffer is a citrate buffer.

8. The formulation of claim 1 , wherein the disaccharide is selected from the group consisting of lactose, sucrose, trehalose, cellobiose, and mixtures thereof.

9. The formulation of claim 1 , wherein the particle formulation is a spray dried preparation of particles.

10. The formulation of claim 1 , wherein the vehicle is about 50% solvent and about 50% polymer.

11. The formulation of claim 1 , wherein the suspension formulation has an overall moisture content of less than or equal to about 10 wt %.

12. An osmotic delivery device, comprising the suspension formulation of claim 1 .

13. A method of manufacturing an osmotic delivery device comprising,

loading the suspension formulation of claim 1 into a reservoir of the osmotic delivery device.

14. A method of treating type II diabetes in a subject in need of such treatment, comprising

delivering the suspension formulation of claim 1 from an osmotic delivery device at a substantially uniform rate for a period of about one month to about a year.

15. The method of claim 14 , wherein the insulinotropic peptide is GLP-1(7-36) amide and delivering the suspension formulation is at a substantially uniform rate of between about 100 μg/day and about 600 μg/day.

16. The method of claim 14 , wherein the insulinotropic peptide is exenatide and delivering the suspension formulation is at a substantially uniform rate of between about 5 μg/day and about 160 μg/day.

Assignments (10)
RELEASE OF SECURITY INTEREST Recorded Apr 17, 2020
From: MIDCAP FINANCIAL TRUST, AS AGENT
To: INTARCIA THERAPEUTICS, INC.; INTARCIA IRELAND LIMITED
Reel/Frame 052433/0001 →
RELEASE OF SECURITY INTEREST Recorded Jan 29, 2020
From: BAUPOST PRIVATE INVESTMENTS BVIV-3, L.L.C. AS COLLATERAL AGENT
To: INTARCIA THERAPEUTICS, INC.
Reel/Frame 051739/0453 →
SECURITY INTEREST Recorded Oct 23, 2019
From: INTARCIA THERAPEUTICS, INC.
To: BAUPOST PRIVATE INVESTMENTS BVIV-3, L.L.C., AS COLLATERAL AGENT
Reel/Frame 050801/0267 →
SECURITY INTEREST Recorded Oct 9, 2019
From: INTARCIA THERAPEUTICS, INC.; INTARCIA IRELAND LIMITED
To: MIDCAP FINANCIAL TRUST, AS AGENT
Reel/Frame 050673/0020 →
RELEASE OF SECURITY INTEREST Recorded Oct 23, 2015
From: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: INTARCIA THERAPEUTICS, INC.
Reel/Frame 036942/0544 →
SECURITY AGREEMENT Recorded Nov 14, 2012
From: INTARCIA THERAPEUTICS, INC.
To: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 029299/0678 →
RELEASE OF SECURITY INTEREST Recorded Sep 23, 2011
From: OXFORD FINANCE CORPORATION; SILICON VALLEY BANK
To: INTARCIA THERAPEUTICS, INC.
Reel/Frame 026962/0062 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 13, 2011
From: ALESSI, THOMAS R.; MERCER, RYAN D.; ROHLOFF, CATHERINE M.; YANG, BING
To: INTARCIA THERAPEUTICS, INC.
Reel/Frame 026279/0629 →
SECURITY AGREEMENT Recorded Sep 8, 2010
From: INTARCIA THERAPEUTICS, INC.
To: OXFORD FINANCE CORPORATION; SILICON VALLEY BANK
Reel/Frame 024953/0525 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 12, 2008
From: ALESSI, THOMAS R.; MERCER, RYAN D.; ROHLOFF, CATHERINE M.; YANG, BING
To: INTARCIA THERAPEUTICS, INC.
Reel/Frame 021093/0549 →