IP Library Granted Patent US 7,586,008
Granted Patent B2
US 7,586,008 · App. 12/170,314 · Granted Sep 8, 2009

Propofol analogs, process for their preparation, and methods of use

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Quick Facts
Patent No.
US 7,586,008
App. No.
12/170,314
Granted
Sep 8, 2009
Kind
B2
Abstract

The invention provides para substituted dialkylphenol derivatives of propofol. The invention further provides pharmaceutical compositions comprising such analogs, methods for preparing such analogs, and methods of using such analogs to induce general anesthesia, sedation, and/or hypnotic or sleep effects in a patient.

Claims (57)

1. A compound of the formula

wherein

X is C═O and Y═H, R 1 is C 4 -C 20 aryl, R 2 is hydrogen, and R 3 is methyl, ethyl or propyl with the proviso that R 1 is not phenyl.

2. A compound of the formula

wherein

R 1 is selected from the group consisting of 4-fluorophenyl, 3-fluorophenyl, 2-fluorophenyl, 4-bromophenyl, 3-bromophenyl, 2-bromophenyl, 4-chlorophenyl, 3-chlorophenyl, 2-chlorophenyl, 4-trifluoromethylphenyl, 3-trifluoromethylphenyl, 2-trifluoromethylphenyl, 4-methoxyphenyl, 3-methoxyphenyl, 2-methoxyphenyl, 4-nitrophenyl, 3-nitrophenyl, 2-nitrophenyl, 4-cyanophenyl, 3-cyanophenyl, 2-methylphenyl, 4-methylphenyl, 3-chloromethylphenyl, 2-iodophenyl, 4-iodophenyl, 4-trifluoromethoxyphenyl, 3-propylphenyl, 2-ethylphenyl, 4-bromomethylphenyl, 4-dimethylaminophenyl, 4-biphenyl, 1-naphthalenyl, 2-naphthalenyl, 2-furanyl, 5-nitro-2-furanyl, 2-thiophenyl, 3,4-methylenedioxyphenyl, 2,3-difluorophenyl, 2,4-difluorophenyl, 2,5-difluorophenyl, 2,6-difluorophenyl, 3,4-difluorophenyl, 3,5-difluorophenyl, 2,4-dichlorophenyl, 2,6-dichlorophenyl, 3,5-dichlorophenyl, 2,5-bis(trifluoromethyl)phenyl, 3,5-bis(trifluoromethyl)phenyl, 4-chloro-3-nitrophenyl, 5-bromo-2-methoxyphenyl, 4-methyl-3-nitrophenyl, 2-fluoro-3-trifluoromethylphenyl, 2-fluoro-5-trifluoromethylphenyl, 2-fluoro-6-trifluoromethylphenyl, 3-fluoro-4-trifluoromethylphenyl, 3-fluoro-5-trifluoromethylphenyl, 2,4-dimethoxyphenyl, 2,6-dimethoxyphenyl, 3,4-dimethoxyphenyl, 3,5-dimethoxyphenyl, 3,5-dichloro-4-methoxyphenyl, 2,3,4-trifluorophenyl, 2,3,6-trifluorophenyl, 2,4,5-trifluorophenyl, 2,4,6-trichlorophenyl, 2,4-dichloro-5-fluorophenyl, 3,4,5-trimethoxyphenyl, 2,4,5-trifluoro-3-methoxyphenyl, 2,3,4,5-tetrafluorophenyl, and pentafluorophenyl;

R 2 and R 3 are C 1 -C 6 alkyl;

X is C═O, C═S, C═C, CR 4 R 5 , C(OR 6 )R 7 or C═N—OR 8 ;

Y is hydrogen, COR 4 , COOR 4 , CONR 4 R 5 , COSR 4 or phosphate;

wherein R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

3. The compound of claim 2 , wherein Y is H.

4. A compound of the formula

wherein Y is phosphate;

R 1 is hydrogen, C 1 -C 6 alkyl, or C 4 -C 20 aryl;

R 2 and R 3 are C 1 -C 6 alkyl;

X is C═O, C═S, C═C, CR 4 R 5 , C(OR 6 )R 7 or C═N—OR 8 ;

wherein R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl;

except when X is C═O and R 2 and R 3 are methyl, then R 1 is not phenyl.

5. A compound of the formula

wherein X is C═O, R 1 is 4-chlorophenyl, and R 2 and R 3 are each methyl;

Y is hydrogen, COR 4 , COOR 4 , CONR 4 R 5 , COSR 4 or phosphate; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

6. A compound of the formula

wherein X is C═O and Y is H, R 1 is 4-chlorophenyl, and R 2 and R 3 are each methyl; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

7. A compound of the formula

wherein X is C═O, R 1 is 4-trifluoromethylphenyl, and R 2 and R 3 are each methyl;

Y is hydrogen, COR 4 , COOR 4 , CONR 4 R 5 , COSR 4 or phosphate; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

8. A compound of the formula

wherein X is C═O and Y is H, R 1 is 4-trifluoromethylphenyl, and R 2 and R 3 are each methyl; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

9. A compound of the formula

wherein X is C═O, R 1 is 4-iodophenyl, and R 2 and R 3 are each methyl;

Y is hydrogen, COR 4 , COOR 4 , CONR 4 R 5 , COSR 4 or phosphate; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or C 1 -C 6 alkyl.

10. A compound of the formula

wherein X is C═O and Y is H, R 1 is 4-iodophenyl, and R 2 and R 3 are each methyl; and

R 4 , R 5 , R 6 , R 7 and R 8 are hydrogen or 1 - 6 alkyl.

11. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 2 and a pharmaceutically acceptable carrier.

12. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 3 and a pharmaceutically acceptable carrier.

13. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 4 and a pharmaceutically acceptable carrier.

14. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 5 and a pharmaceutically acceptable carrier.

15. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 6 and a pharmaceutically acceptable carrier.

16. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 7 and a pharmaceutically acceptable carrier.

17. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 8 and a pharmaceutically acceptable carrier.

18. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 9 and a pharmaceutically acceptable carrier.

19. A pharmaceutical composition comprising a therapeutically effective amount of the compound of claim 10 and a pharmaceutically acceptable carrier.

20. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 2 .

21. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 3 .

22. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 4 .

23. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 5 .

24. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 6 .

25. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 7 .

26. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 8 .

27. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 9 .

28. A method of inducing sedation, hypnosis and/or sleep effect, or general anesthesia in a patient, which method comprises administering to the patient a therapeutically effective amount of the compound of claim 10 .