IP Library Granted Patent US 7,968,022
Granted Patent B1
US 7,968,022 · App. 12/177,001 · Granted Jun 28, 2011

Method for processing and analyzing contaminated mixed waste plastics to produce reformulated blended feed materials having a desired rheology

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,968,022
App. No.
12/177,001
Granted
Jun 28, 2011
Kind
B1
Abstract

A method for reformulating reclaimed, contaminated mixed waste plastics into useful articles wherein a plurality of batches of the mixed waste plastics are preprocessed to produce substantially homogeneous mixtures of a desired particle size range that are characterized according to their respective apparent densities, and are thereafter blended to produce a mixed plastic feed material having a rheology predetermined to be desirable for reprocessing into at least one of such useful articles.

Claims (30)

1. A method for preparing a reformulated feed material having a rheology suitable for use in manufacturing a desired product comprising contaminated reclaimed mixed waste plastic:

preprocessing a plurality of batches of contaminated, reclaimed mixed waste plastic, including injection molding representative sample material selected from each batch;

analyzing operating parameters of equipment used to injection mold the sample material from each batch of preprocessed, reclaimed mixed waste plastic to characterize the batch by its rheology, from which the melt index is then determined;

temporarily storing each batch of preprocessed, reclaimed mixed waste plastic;

calculating a reformulated blend for the feed material using preprocessed, reclaimed mixed waste plastic from the plurality of batches to achieve a desired rheology; and

blending the feed material according to the reformulated blend.

2. The method of claim 1 wherein the preprocessing includes gross contaminant removal, shredding, densification and size reduction.

3. The method of claim 2 wherein the mixed waste plastic has a particle size that is reduced to about −10 mesh.

4. The method of claim 2 wherein the mixed waste plastic has a bulk density that is reduced to about 16 pounds per cubic foot.

5. The method of claim 1 wherein the sample material from each batch is milled prior to injection molding representative sample material from each batch and prior to analyzing the injection molded sample material.

6. The method of claim 1 wherein the injection molded sample material is analyzed using a differential scanning calorimeter to determine the heat flux required to melt the mixed waste plastic as a function of temperature.

7. The method of claim 1 wherein the infection molded sample material is analyzed to determine an apparent density of the mixed waste plastic.

8. The method of claim 1 wherein the injection molded sample material is analyzed to determine a plastic content of the mixed waste plastic.

9. The method of claim 1 wherein the injection molded sample material is analyzed to determine a level of contaminants.

10. The method of claim 1 wherein the injection molded sample material is analyzed to determine color.

11. The method of claim 1 wherein the blending is done under conditions that promote thorough mixing.

12. A method for preparing a reformulated feed material having a rheology suitable for use in manufacturing a desired product comprising reclaimed waste plastic, comprising:

selecting a sample of each of a plurality of batches of unsorted reclaimed mixed waste plastic, wherein each of the plurality of batches is substantially free of gross contaminants and comprises particles within a desired size range;

preparing an injection molded sample material for each of the plurality of batches;

analyzing the sample material from each of the plurality of batches to characterize each batch according to its rheology as determined based upon one or more operating parameters of equipment used to injection mold the sample material;

calculating a reformulated blend to produce a reformulated feed material having a desired rheology based on the analysis of the plurality of batches; and

blending one or more of the plurality of batches, and optionally one or more batches of virgin resin, according to the reformulated blend to create the reformulated feed material.

13. The method of claim 12 , wherein each of the selected samples comprises particles having a particle size of below about −10 mesh and a bulk density below about 16 pounds per cubic foot.

14. The method of claim 12 wherein the operating parameters of the equipment are selected from the group consisting of the amperage draw needed for an electric motor to turn an extruder screw, the torque required to turn a screw in a hydraulically driven machine, the pressure required to inject the sample material into a mold, and combinations thereof.

15. The method of claim 14 wherein the operating parameters of the equipment are used to determine the melt index for each of the sample materials.

16. The method of claim 12 where there is a desired operating temperature range for the feed material and wherein:

the rheology of sample material from each batch is determined over the desired operating temperature range to generate a rheology curve; and

the rheology curve for each batch of feed material is used in calculating the reformulated blend.

17. The method of claim 12 wherein each sample material from each batch is also analyzed to determine a contaminant level for each of the plurality of batches and the contaminant level for each of the plurality of batches is also used in calculating a reformulated blend.

18. The method of claim 17 wherein a contaminant level for the sample material from each of the plurality of batches is determined using a differential scanning calorimeter.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 3, 2021
From: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
To: MOISTURESHIELD, INC.
Reel/Frame 056426/0909 →
SECURITY AGREEMENT Recorded Nov 4, 2015
From: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
To: WEBSTER BUSINESS CREDIT CORPORATION
Reel/Frame 037043/0687 →
RELEASE OF SECURITY INTEREST Recorded Nov 2, 2015
From: ALOSTAR BANK OF COMMERCE
To: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
Reel/Frame 036933/0989 →
SECURITY AGREEMENT Recorded Nov 25, 2012
From: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
To: ALOSTAR BANK OF COMMERCE
Reel/Frame 029344/0329 →
FIRST AMENDMENT TO PATENT SECURITY AGREEMENT Recorded Nov 16, 2012
From: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
To: H.I.G. AERT, LLC
Reel/Frame 029311/0293 →
SECURITY AGREEMENT Recorded Mar 22, 2011
From: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
To: H.I.G. AERT, L.L.C., AS ADMINISTRATIVE AGENT
Reel/Frame 026000/0071 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 20, 2009
From: BROOKS, JOE G.
To: ADVANCED ENVIRONMENTAL RECYCLING TECHNOLOGIES, INC.
Reel/Frame 022129/0010 →