IP Library Granted Patent US 7,959,842
Granted Patent B2
US 7,959,842 · App. 12/198,835 · Granted Jun 14, 2011

Carbon nanotube structure

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Quick Facts
Patent No.
US 7,959,842
App. No.
12/198,835
Granted
Jun 14, 2011
Kind
B2
Abstract

Techniques for forming a carbon nanotube (CNT) structure are disclosed.

Claims (30)

1. A method for forming a carbon nanotube (CNT) structure comprising:

providing a CNT colloidal solution including carbon nanotubes (CNTs); providing a sacrificial element; immersing the sacrificial element into the CNT colloidal solution to form a CNT structure on the sacrificial element; withdrawing the sacrificial element from the CNT colloidal solution, wherein the sacrificial element is substantially vertically withdrawn relative to the CNT colloidal solution at a speed ranging from about 0.3 mm/min to about 3 mm/min; and separating the CNT structure from the sacrificial element, wherein after separation, the formed CNT structure remains, and wherein separating the CNT structure comprises destroying at least part of a surface of the sacrificial element contacting the CNT structure.

2. The method of claim 1 , wherein the CNT colloidal solution comprises about 0.05 mg/mL to about 0.2 mg/mL CNT dispersed in a solvent.

3. The method of claim 1 , wherein the sacrificial element includes a polymer.

4. The method of claim 3 , wherein the polymer includes a photo-sensitizer material.

5. The method of claim 3 , wherein the sacrificial element includes a SAM (self-assembled monolayer) coating.

6. The method of claim 3 , wherein destroying at least part of a surface of the sacrificial element comprises at least partially dissolving the sacrificial element.

7. The method of claim 6 , wherein at least partially dissolving the sacrificial element comprises contacting the CNT structure and the sacrificial element with an acetone solution.

8. The method of claim 3 , wherein the sacrificial elements comprises an inner metal portion and an outer polymer portion.

9. The method of claim 1 , wherein the formed CNT structure comprises a hollow portion defined by the shape of the sacrificial element.

10. The method of claim 1 , wherein the sacrificial element is a cylinder.

11. The method of claim 1 , where the sacrificial element is a plate.

12. The method claim 1 , wherein the CNT structure is dried before separation.

13. The formed CNT structure prepared according to claim 1 .

14. A method for forming a carbon nanotube (CNT) structure comprising:

forming the CNT structure, wherein forming the CNT structure comprises:

immersing the sacrificial element into the CNT colloidal solution to form a CNT structure on the sacrificial element, and withdrawing the sacrificial element from the CNT colloidal solution wherein the sacrificial element is substantially vertically withdrawn relative to the CNT colloidal solution at a speed ranging from about 0.3 mm/min to about 3 mm/min and separating the CNT structure from the sacrificial element, wherein after separation, the formed CNT structure remains, and wherein separating the CNT structure comprises destroying at least part of a surface of the sacrificial element contacting the CNT structure.

15. The method of claim 14 , wherein the CNT structure forms as the sacrificial element is withdrawn.

16. The method of claim 14 , wherein the CNT colloidal solution comprises about 0.05 mg/mL to about 0.2 mg/mL CNT dispersed in a solvent.

17. The method of claim 14 , wherein the sacrificial element includes a polymer.

18. The method of claim 17 , wherein the polymer includes a photo-sensitizer material.

19. The method of claim 18 , wherein the sacrificial element includes a SAM (self-assembled monolayer) coating.

20. The method of claim 17 , wherein destroying at least part of a surface of the sacrificial element comprises at least partially dissolving the sacrificial element.

21. The method of claim 17 , wherein at least partially dissolving the sacrificial element comprises contacting the CNT structure and the sacrificial element with an acetone solution.

22. The method of claim 17 , wherein the sacrificial elements comprises an inner metal portion and an outer polymer portion.

23. The method of claim 14 , wherein the formed CNT structure comprises a hollow portion defined by the shape of the sacrificial element.

24. The method of claim 14 , wherein the sacrificial element is a cylinder.

25. The method of claim 14 , where the sacrificial element is a plate.

26. The method claim 14 , wherein the CNT structure is dried before separation.

27. The formed CNT structure prepared according to claim 14 .

Assignments (5)
RELEASE OF SECURITY INTEREST IN PATENTS, RECORDED ON JANUARY 29, 2019 AT REEL 048373 FRAME 0217 Recorded Sep 22, 2025
From: CRESTLINE DIRECT FINANCE, L.P., AS COLLATERAL AGENT
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 072936/0464 →
RELEASE OF SECURITY INTEREST Recorded Jul 31, 2019
From: CRESTLINE DIRECT FINANCE, L.P.
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 049924/0794 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2008
From: KIM, YONG-HYUP; JANG, EUI YUN
To: SNU R&DB FOUNDATION
Reel/Frame 021978/0336 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 12, 2008
From: KIM, YONG-HYUP; JANG, EUI YUN
To: SNU & R&DB FOUNDATION
Reel/Frame 021978/0341 →