IP Library Granted Patent US 8,784,866
Granted Patent B2
US 8,784,866 · App. 12/245,438 · Granted Jul 22, 2014

Water-soluble carbon nanotube compositions for drug delivery and medicinal applications

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Quick Facts
Patent No.
US 8,784,866
App. No.
12/245,438
Granted
Jul 22, 2014
Kind
B2
Abstract

Compositions comprising a plurality of functionalized carbon nanotubes and at least one type of payload molecule are provided herein. The compositions are soluble in water and PBS in some embodiments. In certain embodiments, the payload molecules are insoluble in water. Methods are described for making the compositions and administering the compositions. An extended release formulation for paclitaxel utilizing functionalized carbon nanotubes is also described.

Claims (31)

1. A composition comprising:

a plurality of functionalized single-wall carbon nanotubes;

wherein the functionalized single-wall carbon nanotubes are water-soluble; and

wherein the functionalized single-wall carbon nanotubes are covalently functionalized with a plurality of PEG moieties; and

a drug molecule comprising paclitaxel;

wherein the paclitaxel is insoluble in water;

wherein the paclitaxel is non-covalently associated with the functionalized single-wall carbon nanotubes; and

wherein the paclitaxel is sequestered from its surrounding environment by the non-covalent association with the functionalized single-wall carbon nanotubes.

2. The composition of claim 1 , wherein the composition is soluble in aqueous PBS buffer.

3. The composition of claim 1 , wherein the non-covalent association does not comprise π-stacking of the paclitaxel with the functionalized single-wall carbon nanotubes.

4. The composition of claim 1 , wherein the PEG moieties have an average molecular weight greater than about 400.

5. The composition of claim 4 , wherein the PEG moieties have an average molecular weight greater than about 2000.

6. The composition of claim 5 , wherein the PEG moieties have an average molecular weight greater than about 5000.

7. The composition of claim 1 , wherein the functionalized single-wall carbon nanotubes comprise at least one tissue-targeting moiety selected from a group consisting of aptamers, antibodies, antibody fragments, saccharides, peptides, proteins, hormones, and receptor ligands.

8. The composition of claim 1 , wherein the functionalized single-wall carbon nanotubes comprise at least one folate moiety.

9. The composition of claim 1 , wherein the composition provides an extended in vivo release of paclitaxel;

wherein the extended in vivo release comprises a greater in vivo residence time of paclitaxel compared to that of paclitaxel alone.

10. The composition of claim 1 , wherein the composition provides intracellular delivery of paclitaxel.

11. A paclitaxel extended release formulation comprising:

a solution of functionalized single-wall carbon nanotubes;

wherein the functionalized single-wall carbon nanotubes are water-soluble;

wherein the functionalized single-wall carbon nanotubes are covalently functionalized with a plurality of PEG moieties; and

wherein the solution comprises water; and

a quantity of paclitaxel, wherein the paclitaxel is non-covalently associated with the functionalized single-wall carbon nanotubes and sequestered from its surrounding environment by the non-covalent association with the functionalized single-wall carbon nanotubes.

12. The extended release formulation of claim 11 , wherein the solution is a PBS buffer.

13. The extended release formulation of claim 11 , wherein the PEG moieties have an average molecular weight greater than about 400.

14. The extended release formulation of claim 13 , wherein the PEG moieties have an average molecular weight greater than about 2000.

15. The extended release formulation of claim 14 , wherein the PEG moieties have an average molecular weight greater than about 5000.

16. The extended release formulation of claim 11 , wherein the quantity of paclitaxel is at least 1 mg of paclitaxel per 1 mL of the solution.

17. The extended release formulation of claim 11 , wherein an in vivo paclitaxel residence time is greater than that of paclitaxel alone.

18. The extended release formulation of claim 11 , wherein the paclitaxel is delivered intracellularly.

Assignments (5)
CONFIRMATORY LICENSE Recorded Apr 9, 2019
From: RICE UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 048839/0517 →
CONFIRMATORY LICENSE Recorded Feb 9, 2018
From: RICE UNIVERSITY
To: DARPA
Reel/Frame 045299/0132 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2014
From: MYERS, JEFFREY N.; MILAS, ZVONIMIR L.; MILAS, LUKA; MASON, KATHY A.
To: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM
Reel/Frame 033042/0901 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2011
From: TOUR, JAMES M.; LUCENTE-SCHULTZ, REBECCA; LEONARD, ASHLEY; KOSYNKIN, DMITRY V.; PRICE, BRANDI KATHERINE; HUDSON, JARED L.
To: WILLIAM MARSH RICE UNIVERSITY
Reel/Frame 026103/0423 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2008
From: MOORE, VALERIE C.; CASSCELLS, S. WARD; CONYERS, JODIE L.
To: BOARD OF REGENTS OF THE UNIVERSITY OF TEXAS SYSTEM
Reel/Frame 022022/0166 →