IP Library Granted Patent US 8,865,632
Granted Patent B1
US 8,865,632 · App. 12/268,408 · Granted Oct 21, 2014

Drag-reducing copolymer compositions

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Quick Facts
Patent No.
US 8,865,632
App. No.
12/268,408
Granted
Oct 21, 2014
Kind
B1
Abstract

A drag-reducing additive includes 40-85% by weight of a polymer emulsion that includes a polymer, a first surfactant, and a first solvent; 10-35% by weight of a second surfactant with an HLB greater than 8; and 5-30% by weight of a second solvent. In a preferred embodiment, the second solvent includes a terpene. In another preferred embodiment, the polymer is a copolymer that includes acrylamide and acrylic acid.

Claims (30)

1. A well treatment composition for reducing drag in a well, pipeline, or gathering line, the well treatment composition comprising:

a drag reducing additive, the drag reducing additive comprising:

40-85% by weight of a polymer emulsion, wherein the polymer emulsion comprises a polymer, a first surfactant, and a first solvent;

10-35% by weight of a second surfactant with an HLB greater than 8; and

5-30% by weight of a second solvent; and

a well treatment fluid.

2. The well treatment composition of claim 1 , wherein the polymer is a copolymer that comprises acrylamide and acrylic acid.

3. The well treatment composition of claim 2 , wherein the copolymer comprises 60-99% by weight acrylamide and 1-40% by weight acrylic acid.

4. The well treatment composition of claim 1 , wherein the copolymer comprises polyacrylamide and a monomer selected from the group consisting of sodium acrylate, methyacrylamidopropyltrimethylammonium chloride, diallyldimethylammonium chloride, and dimethylaminoethylacrylate methyl chloride quaternary salt.

5. The well treatment composition of claim 1 , wherein the polymer is a water-soluble homopolymer.

6. The well treatment composition of claim 1 , wherein the second solvent comprises a terpene.

7. The well treatment composition of claim 1 , wherein the second solvent comprises d-limonene.

8. The well treatment composition of claim 1 , wherein the second solvent is selected from the group consisting of citrus, pine, eucalyptus, and mint-derived terpenes.

9. The well treatment composition of claim 1 , wherein the second surfactant is selected from the group consisting of ethoxylated alcohols, ethoxylated castor oils, and ethoxylated sorbitan monooleates.

10. A well treatment composition for reducing drag in a well, pipeline, or gathering line, the well treatment composition comprising:

from about 0.001% to about 4.7% by volume of a drag reducing additive, the drag reducing additive comprising:

50-99% by weight of a drag-reducing polymer; and

1-50% by weight of a surfactant with an HLB greater than 7; and

from about 99.999% to about 95.3% by volume of a well treatment fluid, wherein the well treatment fluid is a fracturing fluid.

11. The well treatment composition of claim 10 , wherein the drag-reducing polymer comprises:

about 72-99% of the drag-reducing polymer;

about 1-28% of the surfactant with an HLB greater than 7; and

wherein the drag-reducing additive is a highly viscous, paste-like material.

12. The well treatment composition of claim 11 , wherein the drag-reducing polymer is a copolymer that comprises acrylamide and acrylic acid.

13. The well treatment composition of claim 11 , wherein the drag-reducing polymer is a copolymer that comprises 60-99% by weight acrylamide and 1-40% by weight acrylic acid.

14. The well treatment composition of claim 11 , wherein the drag-reducing polymer is a copolymer that comprises acrylamide and a monomer selected from the group consisting of sodium acrylate, methyacrylamidopropyltrimethylammonium chloride, diallyldimethylammonium chloride, and dimethylaminoethylacrylate methyl chloride quaternary salt.

15. The well treatment composition of claim 11 , further comprising 1 to 35% of a second solvent.

16. The well treatment composition of claim 15 , wherein the second solvent comprises d-limonene.

17. The well treatment composition of claim 15 , wherein the second solvent is selected from the group consisting of citrus, pine, eucalyptus, and mint-derived terpenes.

18. The well treatment composition of claim 15 , wherein the surfactant is selected from the group consisting of ethoxylated alcohols, ethoxylated castor oils, and ethoxylated sorbitan monooleates.

Assignments (8)
RELEASE OF SECURITY INTEREST Recorded Apr 17, 2019
From: PNC BANK NATIONAL ASSOCIATION
To: CESI CHEMICAL, INC.
Reel/Frame 048916/0850 →
CONVERSION Recorded Jan 15, 2016
From: CESI CHEMICAL, INC.
To: FLOTEK CHEMISTRY, LLC
Reel/Frame 037540/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2013
From: FLOTEK INDUSTRIES, INC.; CESI CHEMICAL, INC.; CESI MANUFACTURING, LLC; MATERIAL TRANSLOGISTICS, INC.; TELEDRIFT COMPANY; TURBECO, INC.; USA PETROVALVE, INC.; FLOTEK ACQUISITION INC.; FLORIDA CHEMICAL COMPANY, INC.
To: PNC BANK, NATIONAL ASSOCIATION
Reel/Frame 030569/0758 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jan 6, 2012
From: FLOTEK INDUSTRIES, INC.; CESI CHEMICAL, INC.; CESI MANUFACTURING, LLC; MATERIAL TRANSLOGISTICS, INC.; SOONER ENERGY SERVICES, LLC; TELEDRIFT COMPANY; TURBECO, INC.; USA PETROVALVE, INC.
To: PNC BANK, NATIONAL ASSOCIATION
Reel/Frame 027491/0420 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jan 4, 2012
From: WHITEBOX ADVISORS LLC
To: FLOTEK INDUSTRIES, INC.
Reel/Frame 027480/0209 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2011
From: PARNELL, EARL; SANNER, TODD; HOLTMYER, MARLIN; PHILPOT, DAVID; ZELENEV, ANDREI; GILZOW, GYDEON; CHAMPAGNE, LAKIA; SIFFERMAN, THOMAS
To: CESI CHEMICAL, INC.
Reel/Frame 027010/0569 →
SECURITY AGREEMENT Recorded Apr 7, 2010
From: FLOTEK INDUSTRIES, INC.; TELEDRIFT COMPANY; FLOTEK PAYMASTER INC.; MATERIAL TRANSLOGISTICS, INC.; PETROVALVE, INC.; TURBECO, INC.; USA PETROVALVE, INC.; FLOTEK INTERNATIONAL, INC.; PADKO INTERNATIONAL INCORPORATED; FLOTEK ECUADOR MANAGEMENT, LLC; FLOTEK ECUADOR INVESTMENTS, LLC; CESI CHEMICAL, INC.; CESI MANUFACTURING, LLC; SOONER ENERGY SERVICES, LLC; FLOTEK INDUSTRIES FZE
To: WHITEBOX ADVISORS LLC; WHITEBOX HEDGED HIGH YIELD PARTNERS, LP; IAM MINI-FUND 14 LIMITED; PANDORA SELECT PARTNERS, LP; WHITEBOX SPECIAL OPPORTUNITIES FUND, LP - SERIES B; WHITEBOX COMBINED PARTNERS, LP; WHITEBOX CONVERTIBLE ARBITRAGE PARTNERS, LP; ECF VALUE FUND, L.P.; ECF VALUE FUND II, L.P.; ECF VALUE FUND INTERNATIONAL LTD.
Reel/Frame 024195/0637 →
SECURITY AGREEMENT Recorded Apr 7, 2010
From: FLOTEK INDUSTRIES, INC.; TELEDRIFT COMPANY; FLOTEK PAYMASTER INC.; MATERIAL TRANSLOGISTICS, INC.; PETROVALVE, INC.; TURBECO, INC.; USA PETROVALVE, INC.; FLOTEK INTERNATIONAL, INC.; PADKO INTERNATIONAL INCORPORATED; FLOTEK ECUADOR MANAGEMENT, LLC; FLOTEK ECUADOR INVESTMENTS, LLC; CESI CHEMICAL, INC.; CESI MANUFACTURING, LLC; SOONER ENERGY SERVICES, LLC; FLOTEK INDUSTRIES FZE
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 024195/0979 →