IP Library Granted Patent US 7,902,222
Granted Patent B2
US 7,902,222 · App. 12/274,529 · Granted Mar 8, 2011

Biaryl substituted azabicyclic alkane derivatives

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Quick Facts
Patent No.
US 7,902,222
App. No.
12/274,529
Granted
Mar 8, 2011
Kind
B2
Abstract

The invention relates to biaryl substituted azabicyclic alkane derivatives, compositions comprising such compounds, and methods of treating conditions and disorders using such compounds and compositions.

Claims (83)

1. A compound of formula (I),

or a pharmaceutically acceptable salt, or prodrug thereof, wherein

n is 1, 2 or 3;

A is N or —N + —O − ;

R z is hydrogen, alkyl, cycloalkyl or arylalkyl;

L is selected from the group consisting of O, S, and —N(R a )—;

Ar 1 is a 5-membered heteroaryl group;

Ar 2 is an aryl or heteroaryl group; and

R a is selected from the group consisting of hydrogen, alkyl and alkylcarbonyl.

2. The compound of claim 1 , wherein Ar 1 is selected from the group consisting of:

wherein

R 1 , R 2 , R 3 and R 4 are independently hydrogen, acyl, acyloxy, alkenyl, alkoxy, alkoxyalkoxy, alkoxyalkyl, alkoxycarbonyl, alkoxyimino, alkoxysulfonyl, alkyl, alkylsulfonyl, alkynyl, amino, carboxy, cyano, formyl, haloalkoxy, haloalkyl, halo, hydroxy, hydroxyalkyl, mercapto, nitro, thioalkoxy, —NR g R j , (NR g R j )alkyl, (NR g R j )alkoxy, (NR g R j )carbonyl, or (NR g R j )sulfonyl;

R 5 is hydrogen, acyl, alkyl, or alkylsulfonyl; and R g and R j are each independently hydrogen or alkyl or alkylcarbonyl.

3. The compound of claim 1 , wherein Ar 2 is

wherein

Z 1 , Z 2 , Z 3 , Z 4 and Z 5 are each independently nitrogen or are carbon, wherein the carbon atom is optionally substituted with a substituent selected from the group consisting of hydrogen, halogen, alkyl, —OR c , -alkyl-OR c , —NR d R e , and -alkyl-NR d R e ;

R 6 and R 7 are each independently selected from the group consisting of hydrogen, alkenyl, alkoxy, alkoxyalkoxy, alkoxyalkyl, alkoxycarbonyl, alkoxyimino, alkoxysulfonyl, alkyl, alkylcarbonyl, alkylcarbonyloxy, alkylsulfonyl, alkynyl, carboxy, cyano, formyl, haloalkoxy, haloalkyl, halo, hydrogen, hydroxy, hydroxyalkyl, mercapto, nitro, thioalkoxy, —NR f R g , (NR f R g )alkyl, (NR f R g )alkoxy, (NR f R g )carbonyl, and (NR f R g )sulfonyl; R a , R b , R c , R d , R e , R f , and R g are each independently hydrogen, alkyl, or alkylcarbonyl.

4. A compound of formula (I),

or a pharmaceutically acceptable salt or prodrug thereof, or a tautomer thereof when R 6 or R 7 is hydroxy, wherein

n is 1, 2 or 3;

A is N or —N + —O − ;

R z is hydrogen, alkyl, cycloalkyl or arylalkyl;

L is selected from the group consisting of O, S and —N(R a )—; R a is selected from the group consisting of hydrogen, alkyl and alkylcarbonyl

Ar 1 is a 5-membered heteroaryl group;

Ar 2 is

wherein

Z 1 , Z 2 , Z 3 , Z 4 and Z 5 are each independently nitrogen or are carbon, wherein the carbon atom is optionally substituted with a substituent selected from the group consisting of hydrogen, halogen, alkyl, —OR c , -alkyl-OR c , —NR d R e , -alkyl-NR d R e ;

R 6 and R 7 are each independently selected from the group consisting of hydrogen, alkenyl, alkoxy, alkoxyalkoxy, alkoxyalkyl, alkoxycarbonyl, alkoxyimino, alkoxysulfonyl, alkyl, alkylcarbonyl, alkylcarbonyloxy, alkylsulfonyl, alkynyl, carboxy, cyano, formyl, haloalkoxy, haloalkyl, halo, hydrogen, hydroxy, hydroxyalkyl, mercapto, nitro, thioalkoxy, —NR f R g , (NR f R g )alkyl, (NR f R g )alkoxy, (NR f R g )carbonyl, and (NR f R g )sulfonyl; R a , R b , R c , R d , R e , R f , and R g are each independently hydrogen, alkyl, or alkylcarbonyl.

5. The compound of claim 2 , wherein

A is N;

R z is H or methyl;

L is O;

n is 2; and

Ar 1 is:

6. The compound of claim 3 , wherein

A is N;

R z is H or methyl;

L is O;

n is 2;

Ar 2 is

7. The compound of claim 2 , wherein

A is N;

R z is H or methyl;

L is O;

n is 2;

Ar 1 is

Ar 2 is

8. The compound of claim 1 , selected from the group consisting of:

2-[(endo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-(1H-indol-5-yl)-thiazole;

2-[(endo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-phenyl-thiazole;

2-[(endo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-(pyridin-3-yl))-thiazole;

5-(1H-Indol-6-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]thiazole;

5-(1H-Indol-4-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]thiazole;

5-(Benzofuran-5-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]thiazole;

5-(Benzo[b]thiophen-5-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]thiazole;

5-(2-(Trifluoromethyl)-1H-indol-5-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy])thiazole;

5-(Dibenzo[b,d]thiophen-2-yl)-2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]thiazole;

2-[(exo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-(1H-indol-5-yl)-thiazole;

2-[(exo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-(1H-indol-6-yl)-thiazole;

2-[(exo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-phenyl-thiazole;

2-[(exo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-(pyridin-3-yl)-thiazole;

2-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-phenyl-1,3,4-thiadiazole;

2-(1H-Indol-5-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(Benzofuran-5-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy)-1,3,4-thiadiazole;

2-(Benzo[b]thiophen-5-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Fluorophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-[(endo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-5-m-tolyl-1,3,4-thiadiazole;

2-(4-Fluorophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Chlorophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(1H-Indol-6-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(1H-Indol-4-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Cyanophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Trifluoromethylphenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy)-1,3,4-thiadiazole;

2-(4-Chlorophenyl)-5-41R,3R,5S)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy)-1,3,4-thiadiazole;

2-(2-(Trifluoromethyl)-1H-indol-5-yl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Chloro-4-fluorophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy)-1,3,4-thiadiazole;

2-(4-(Trifluoromethyl)phenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(4-Methoxyphenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(3-Aminophenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(4-Ethylphenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole;

2-(4-Acetylphenyl)-5-[(endo)-8-methyl-8-azabicyclo[3.2.1]octan-3-yloxy]-1,3,4-thiadiazole; and

N-[(endo)-8-Methyl-8-azabicyclo[3.2.1]octan-3-yl]-5-phenyl-1,3,4-thiadiazol-2-amine.

9. A pharmaceutical composition comprising a therapeutically effective amount of a compound of claim 1 and a pharmaceutically acceptable carrier.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 17, 2013
From: ABBOTT LABORATORIES
To: ABBVIE INC.
Reel/Frame 030237/0588 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 9, 2009
From: JI, JIANGUO; LI, TAO; SIPPY, KEVIN B.; LEE, CHIH-HUNG; GOPALAKRISHNAN, MURALI
To: ABBOTT LABORATORIES
Reel/Frame 022524/0615 →