Process and apparatus for preparing a soap concentrate, a lubricating composition, and combinations thereof
View Patent ↗The invention provides for a process and apparatus for preparing a soap concentrate, including: (a) introducing feed components to a first feeding zone; (b) first reacting in a first reacting zone; (c) first venting in a first venting zone; and (d) cooling in a cooling zone. The process may further include, after (c) and before (d): (i) continued reacting in a continued reacting zone; and (ii) second venting in a second venting zone. The invention also provides for a process and apparatus for preparing a lubricating composition comprising: (aa) introducing a soap concentrate and a base oil to a lubricating composition feeding zone; (bb) dispersing the soap concentrate in a lubricating composition dispersing zone; (cc) mixing the soap concentrate and the base oil in a lubricating composition mixing zone; and (dd) cooling in a lubricating composition cooling zone.
1. A process for preparing a soap concentrate comprising:
providing an apparatus comprising an extruder and a plurality of zones arranged in series and in fluid communication, wherein the plurality of zones comprise (a) a first feeding zone; (b) a first reacting zone; (c) a first venting zone; and (d) a cooling zone, and wherein the zones are in the order (a), (b), (c), (d);
introducing feed components to the first feeding zone (a);
allowing the feed components to react in the first reacting zone (b);
allowing venting from the first venting zone (c);
allowing output to be cooled within the cooling zone (d); and
thereby obtaining the soap concentrate.
2. A process according to claim 1 wherein the apparatus further comprises a continued reacting zone and a second venting zone and further comprising, after (c) and before (d), (i) allowing continued reacting in the continued reacting zone; and (ii) allowing second venting in the second venting zone.
3. A process according to claim 1 wherein the apparatus further comprises a second feeding zone and further comprising introducing one or more initial additives to the second feeding zone.
4. A process according to claim 1 wherein the apparatus further comprises a water injecting zone and further comprising injecting water in the water injecting zone.
5. A process according to claim 1 wherein the soap concentrate comprises at least one concentrate selected from the group consisting of lithium soap concentrate, lithium complex soap concentrate, lithium-calcium soap concentrate, and calcium complex soap concentrate.
6. A process according to claim 1 further comprising combining the soap concentrate with a base oil to prepare a base grease.
7. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil in an amount of 75 weight percent to 95 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, and a combination thereof in an amount of 8 weight percent to 20 weight percent, based on the total weight of the soap concentrate.
8. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil in an amount of 75 weight percent to 95 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, calcium hydroxide, and a combination thereof in an amount of 8 weight percent to 20 weight percent, based on the total weight of the soap concentrate.
9. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil fatty acid in an amount of 75 weight percent to 95 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, and a combination thereof in an amount of 8 weight percent to 20 weight percent, based on the total weight of the soap concentrate.
10. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil fatty acid in an amount of 75 weight percent to 95 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, calcium hydroxide, and a combination thereof in an amount of 8 weight percent to 20 weight percent, based on the total weight of the soap concentrate.
11. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil or hydrogenated castor oil fatty acid in an amount of 50 weight percent to 65 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, and a combination thereof in an amount of 10 weight percent to 20 weight percent, based on the total weight of the soap concentrate; and
a complexing agent in an amount of 6 weight percent to 12 weight percent, based on the total weight of the soap concentrate.
12. A process according to claim 1 wherein the feed components comprise:
hydrogenated castor oil or hydrogenated castor oil fatty acid in an amount of 50 weight percent to 65 weight percent, based on the total weight of the soap concentrate; and
at least one selected from the group consisting of lithium hydroxide, lithium hydroxide monohydrate, calcium hydroxide and a combination thereof in an amount of 10 weight percent to 20 weight percent, based on the total weight of the soap concentrate; and
a complexing agent in an amount of 6 weight percent to 12 weight percent, based on the total weight of the soap concentrate.