IP Library Granted Patent US 8,927,537
Granted Patent B2
US 8,927,537 · App. 12/340,246 · Granted Jan 6, 2015

Patches, formulations, and associated methods for transdermal delivery of alprazolam and other drugs

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Quick Facts
Patent No.
US 8,927,537
App. No.
12/340,246
Granted
Jan 6, 2015
Kind
B2
Abstract

The present invention is drawn to transdermal drug formulations, transdermal patches incorporating such formulations, as well as associated methods. The formulations can include about 0.3 wt % to about 5 wt % of a drug, such as alprazolam, about 4 wt % to about 30 wt % water, about 10 wt % to about 40 wt % glycerol, about 0.5 wt % to about 6 wt % oleyl alcohol. Other co-solvents and/or additives can be present to achieve a 100 wt % formulation.

Claims (48)

1. A formulation for transdermal delivery of a drug, comprising

from about 0.3 wt % to about 5 wt % of alprazolam,

from about 4 wt % to about 30 wt % water,

from about 10 wt % to about 40 wt % glycerol, and

from about 0.5 wt % to about 6 wt % oleyl alcohol,

wherein the alprazolam in the formulation has a degradation rate of less than 5% per year at 25° C.

2. A formulation as in claim 1 , further comprising from about 20 wt % to about 85 wt % of additional solvent.

3. A formulation as in claim 1 , wherein alprazolam comprises about 0.5 wt % to about 3 wt % of the formulation.

4. A formulation as in claim 1 , wherein alprazolam comprises about 0.8 wt % to about 1.8 wt % of the formulation.

5. A formulation as in claim 1 , wherein alprazolam comprises about 1.0 wt % to about 1.5 wt % of the formulation.

6. A formulation as in claim 1 , wherein water comprises about 5 wt % to about 25 wt % of the formulation.

7. A formulation as in claim 1 , wherein water comprises about 6 wt % to about 15 wt % of the formulation.

8. A formulation as in claim 1 , wherein glycerol comprises about 15 wt % to 37 wt % about of the formulation.

9. A formulation as in claim 1 , wherein glycerol comprises about 20 wt % to about 35 wt % of the formulation.

10. A formulation as in claim 1 , wherein the oleyl alcohol comprises about 1 wt % to about 5 wt % of the formulation.

11. A formulation as in claim 1 , wherein the oleyl alcohol comprises about 2 wt % to about 4 wt % of the formulation.

12. A formulation as in claim 2 , wherein the additional solvent includes propylene glycol.

13. A formulation as in claim 1 , wherein the formulation has a pH of 7.0 to 10.

14. A formulation as in claim 1 , wherein the formulation includes a compound selected from the group consisting of BHT and EDTA.

15. A formulation as in claim 1 , wherein the formulation includes a skin irritation reduction agent selected from the group consisting of corticosteroids and anti-inflammatory agents.

16. A formulation as in claim 1 , wherein the formulation has a viscosity of about 20,000 to centipoise to about 200,000 centipoise.

17. A formulation as in claim 1 , incorporated in a transdermal patch.

18. A transdermal patch for transdermal delivery of alprazolam, comprising:

a transdermal drug formulation incorporated into a transdermal patch, said transdermal drug formulation comprising from about 0.3 wt % to about 5 wt % alprazolam, from about 4 wt % to about 30 wt % water, from about 10 wt % to about 40 wt % glycerol, from about 0.5 wt % to about 6 wt % oleyl alcohol, and optionally from about 20 wt % to about 85 wt % of additional solvent, wherein the alprazolam in the formulation has a degradation rate of less than 5% per year at 25° C.

19. A transdermal patch as in claim 18 , wherein the patch has a formulation-skin contact area of from 2 cm 2 to 100 cm 2 .

20. A transdermal patch as in claim 18 , wherein the patch has a formulation-skin contact area of from 5 cm 2 to 60 cm 2 .

21. A patch as in claim 20 , wherein each square centimeter of the formulation-skin contact area generates a mean AUC of at least 20 ng·hr/ml when administered to at least 10 human adults for a 72 hour period of time.

22. A transdermal patch as in claim 20 , wherein each square centimeter of the formulation-skin contact area generates a mean AUC of at least 34 ng·hr/ml when administered to at least 10 human adults for a 72 hour period of time.

23. A transdermal patch as in claim 20 , wherein each square centimeter of the formulation-skin contact area generates a mean AUC of at least 50 ng·hr/ml when administered to at least 10 human adults for a 72 hour period of time.

24. A transdermal patch as in claim 20 , wherein the total quantity of alprazolam in said patch per cm 2 of the transdermal drug formulation-skin contact area is less than 2 mg/cm 2 .

25. A transdermal patch as in claim 18 , wherein the patch includes a microporous non-rate-limiting membrane.

26. A transdermal patch as in claim 18 , wherein the patch is configured to deliver alprazolam therapeutically effective rates for a period of at least 48 hours.

27. A formulation for transdermal delivery of alprazolam, comprising:

alprazolam,

about 6 wt % to about 15 wt % water,

about 20 wt % to about 35 wt % glycerol,

about 40% to about 70% propylene glycol, and

about 2 wt % to about 4 wt % oleyl alcohol

wherein the alprazolam in the formulation has a degradation rate of less than 5% per year at 25° C.

28. A formulation as in claim 27 incorporated into a transdermal patch.

29. A formulation as in claim 27 , said formulation having a pH of 7-10.

30. A formulation as in claim 27 , wherein the alprazolam is present at from about 1.0 wt % to about 1.5 wt %.

31. A transdermal patch for transdermal delivery of alprazolam, comprising:

a transdermal drug formulation incorporated in a transdermal patch, wherein the transdermal drug formulation comprises about 1.0 wt % to about 1.5 wt % alprazolam, about 6 wt % to about 15 wt % water, about 20 wt % to about 35 wt % glycerol, about 40% to about 70% propylene glycol, from about 2 wt % to about 4 wt % oleyl alcohol, and has a pH of 7-10; wherein each square centimeter of the contact area between said formulation and the skin is capable of generating a mean AUC of at least 50 ng.hr/ml when administered to at least 10 human adults for a 72 hour period of time and wherein the alprazolam in the formulation has a degradation rate of less than 5% per year at 25° C.

32. A method of treating anxiety disorder or panic disorder in a subject, comprising:

applying a transdermal drug formulation to a skin surface of a subject, said transdermal formulation comprising from about 0.3 wt % to about 5 wt % alprazolam, from about 4 wt % to about 30 wt % water, from about 10 wt % to about 40 wt % glycerol, and from about 0.5 wt % to about 6 wt % oleyl alcohol and optionally about 20 wt % to about 85 wt % of additional solvent; and

maintaining said transdermal drug formulation in contact with said skin surface for a period of at least 48 hours.

33. A method as in claim 32 , wherein the applying step is by applying the transdermal drug formulation to the skin surface by way of a transdermal patch which includes the transdermal drug formulation.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded May 17, 2023
From: PALADIN LABS INC.
To: NUVO RESEARCH INC.
Reel/Frame 063695/0543 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2016
From: NUVO RESEARCH INC.
To: CRESCITA THERAPEUTICS INC.
Reel/Frame 040485/0021 →
RELEASE OF SECURITY INTEREST Recorded Jan 8, 2015
From: PALADIN LABS INC.
To: NUVO RESEARCH INC.
Reel/Frame 034664/0991 →
GENERAL SECURITY AGREEMENT Recorded Aug 20, 2012
From: NUVO RESEARCH INC.
To: PALADIN LABS INC.
Reel/Frame 028816/0225 →
CONFIRMATION OF ASSIGNMENT Recorded Jul 10, 2012
From: NUVO RESEARCH AMERICA, INC.
To: NUVO RESEARCH INC.
Reel/Frame 028535/0690 →
CONFIRMATION OF ASSIGNMENT Recorded Jul 6, 2012
From: ZARS PHARMA, INC.
To: NUVO RESEARCH AMERICA, INC.
Reel/Frame 028509/0561 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 3, 2009
From: SHARMA, SANJAY; WARNER, KEVIN S.; ZHANG, JIE; YAN, GUANG
To: ZARS PHARMA, INC.
Reel/Frame 022335/0449 →