IP Library Granted Patent US 7,967,894
Granted Patent B1
US 7,967,894 · App. 12/348,615 · Granted Jun 28, 2011

System and method for improved mercury control

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Quick Facts
Patent No.
US 7,967,894
App. No.
12/348,615
Granted
Jun 28, 2011
Kind
B1
Abstract

A combustion system having improved mercury collection. The system includes a combustion chamber for burning a fuel containing mercury, whereby burning produces a flue gas stream containing mercury and a device for removing mercury from the flue gas stream. The device includes a thermopolymer substrate; and a mercury-receptor attached to the substrate. In one embodiment, the system may further include a collector downstream of the device for collecting the mercury attached to the thermopolymer. The inventions further include alternative methods of mercury removal and preparation of the polymer substrate.

Claims (49)

1. A method for providing mercury collection in a combustion system, said method comprising the steps of:

(a) burning a fuel containing mercury in a combustion chamber, whereby burning produces a flue gas stream containing mercury; and

(b) removing mercury from the flue gas stream by contacting the flue gas stream with a thermopolymer, wherein said thermopolymer contains substitutions to increase conductivity.

2. A method of mercury-removal from a fluid, said method comprising the step of: contacting the fluid containing mercury with a polymer having a mercury-receptor, wherein said mercury-receptor was attached to said substrate by heating said substrate, exposing said substrate to said mercury-receptor, and cooling said substrate.

3. The method of claim 2 , wherein the fluid is a flue gas.

4. The method of claim 3 , wherein the fluid is a fossil fuel combustion flue gas.

5. The method of claim 2 , wherein the fluid includes a vapor phase.

6. The method of claim 2 , wherein the fluid includes a liquid phase.

7. The method of claim 6 , wherein the liquid is water.

8. The method of claim 2 , wherein the step of contacting includes passing the fluid through a membrane.

9. The method of claim 2 , wherein the step of contacting includes injecting the polymer into the fluid.

10. The method of claim 9 , wherein the polymer is a particle.

11. The method of claim 2 , wherein the polymer is an aromatic polymer.

12. The method of claim 11 , wherein the aromatic polymer is a polyamide.

13. The method of claim 11 , wherein the aromatic polymer is a polysulfone.

14. The method of claim 2 , wherein the mercury-receptor is a halogen.

15. The method of claim 14 , wherein the halogen is selected from the group consisting of chlorine, bromine, and iodine.

16. The method of claim 2 , wherein the polymer having a mercury-receptor is created by reacting a halogenated monomer with another monomer.

17. The method of claim 2 , wherein the polymer having a mercury-receptor is created in situ by exposing the polymer to a gaseous mercury-receptor.

18. The method of claim 2 wherein the polymer having a mercury-receptor is created in situ by exposing the polymer to a mercury-receptor in solution.

19. The method of claim 2 , wherein said polymer contains substitutions to increase conductivity.

20. A method for providing mercury collection in a combustion system, said method comprising the steps of:

(a) burning a fuel containing mercury in a combustion chamber, whereby burning produces a flue gas stream containing mercury;

(b) removing mercury from the flue gas stream by contacting the flue gas stream with a device including: (i) a thermopolymer substrate; and (ii) a mercury-receptor attached to the substrate, wherein said mercury-receptor was attached to said substrate by heating said substrate, exposing said substrate to said mercury-receptor, and cooling said substrate; and

(c) collecting the mercury attached to the thermopolymer.

21. A method of removing mercury from a fluid, said method comprising the steps of:

(a) heating a polymer membrane;

(b) exposing the heated membrane to a mercury-receptor;

(c) cooling the exposed polymer membrane; and

(d) contacting the polymer with a mercury containing fluid.

22. The method of claim 21 , wherein the fluid is a gas.

23. The method of claim 22 , wherein the gas is a combustion flue gas.

24. The method of claim 21 , wherein the step of heating includes heating above the dew-point temperature of the membrane.

25. The method of claim 24 , wherein the heating occurs downstream of a combustion zone.

26. The method of claim 21 , wherein the step of exposing is achieved through a gas including a mercury-receptor.

27. The method of clam 26 , wherein the gas including a mercury receptor includes chlorine gas.

28. The method of claim 26 , wherein the gas including a mercury receptor includes a bromine gas.

29. The method of claim 21 , wherein the step of exposing is achieved through a liquid including a mercury-receptor.

30. The method of claim 21 , wherein the step of cooling includes cooling to below the dew-point temperature of the membrane.

31. The method of claim 30 , wherein the step of contacting includes passing the fluid through a membrane.

32. A method for providing mercury collection in a combustion system, said method comprising the steps of:

burning a fuel containing mercury in a combustion chamber, whereby burning produces a flue gas stream containing mercury;

injecting a supply of gaseous monomers downstream from the beginning of the combustion chamber; and

removing mercury from the flue gas stream by contacting the flue gas stream with a thermopolymer formed from the gaseous monomers.

33. A method of removing mercury from a flue gas, said method comprising the steps of:

heating a polymer substrate above the dew-point temperature of the substrate;

exposing the heated substrate to at least one of a gas including a mercury-receptor and a liquid including a mercury-receptor;

cooling the exposed polymer substrate to below the dew-point temperature of the substrate; and

contacting the polymer substrate with the flue gas.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Jul 29, 2013
From: NALCO MOBOTEC, LLC
To: NALCO COMPANY
Reel/Frame 030893/0130 →
CHANGE OF NAME Recorded Jul 10, 2013
From: NALCO MOBOTEC, INC.
To: NALCO MOBOTEC LLC
Reel/Frame 030775/0576 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 7, 2011
From: MOBOTEC USA, INC.
To: NALCO MOBOTEC, INC.
Reel/Frame 025908/0798 →