IP Library Granted Patent US 9,174,970
Granted Patent B2
US 9,174,970 · App. 12/357,710 · Granted Nov 3, 2015

5-fluoro pyrimidine derivatives

Inventors: Zoltan L. Benko (Indianapolis, IN); Timothy Boebel (Indianapolis, IN); Nneka T. Breaux (Indianapolis, IN); Kristy Bryan (Carmel, IN); George E. Davis (Carmel, IN); Jeffrey B. Epp (Noblesville, IN); Beth Lorsbach (Indianapolis, IN); Timothy P. Martin (Noblesville, IN); Kevin G. Meyer (Zionsville, IN); Bassam S. Nader (Fishers, IN); W. John Owen (Carmel, IN); Mark A. Pobanz (Zionsville, IN); James M. Ruiz (Westfield, IN); Frisby D. Smith (Davis, CA); Michael T. Sullenberger (Westfield, IN); Jeffery D. Webster (New Palestine, IN); Chenglin Yao (Westfield, IN); David H. Young (Carmel, IN)
Assignee: Dow AgroSciences LLC
C07D405/12A01N43/54C07D239/47
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Quick Facts
Patent No.
US 9,174,970
App. No.
12/357,710
Granted
Nov 3, 2015
Kind
B2
Abstract

This present disclosure is related to the field of 5-fluoro pyrimidines and their derivatives and to the use of these compounds as fungicides.

Claims (45)

1. A compound of Formula (I)

wherein R 1 is —N(R 3 )R 4 ;

R 2 is —OR 21 ;

R 3 is: H;

wherein m is 1;

R 4 is: H;

R 20 is independently halogen, cyano, nitro, amino, C 1 -C 6 alkoxyalkoxy, C 1 -C 6 alkyl, C 1 -C 6 haloalkyl, C 1 -C 6 hydroxyalkyl, C 2 -C 6 alkoxyalkyl, C 2 -C 6 haloalkoxyalkyl, C 2 -C 6 alkenyl, C 2 -C 6 haloalkenyl, C 3 -C 6 alkynyl, C 3 -C 6 haloalkynyl, hydroxyl, C 1 -C 6 alkoxy, C 1 -C 6 haloalkoxy, C 2 -C 6 alkenyloxy, C 2 -C 6 haloalkenyloxy, C 3 -C 6 alkynyloxy, C 3 -C 6 haloalkynyloxy, C 1 -C 6 alkylthio, C 1 -C 6 haloalkylthio, C 1 -C 6 alkylsulfonyl, C 1 -C 6 haloalkylsulfonyl, C 2 -C 6 alkenylthio, C 2 -C 6 haloalkenylthio, C 2 -C 6 haloalkenylsulfonyl, C 3 -C 6 alkynylthio, C 3 -C 6 alkynylsulfonyl, C 3 -C 6 haloalkynylsulfonyl, C 1 -C 6 alkylamino, C 2 -C 8 dialkylamino, C 3 -C 8 dialkylaminocarbonyl, C 2 -C 6 alkoxycarbonyl, C 2 -C 6 alkylcarbonyl, C 3 -C 6 trialkylsilyl, 2-[(E)-methoxyimino]-N-methyl-acetamidyl, phenyl, benzyl, benzyloxy, phenoxy,or a 5- or 6-membered heteroaromatic ring wherein each phenyl, benzyl, benzyloxy, phenoxy, or 5- or 6-membered heteroaromatic ring may be optionally substituted with 1-3 substitutents independently selected from R 31 ;

R 21 is:

—(CHR 22 ) m R 23 ;

R 22 is H;

R 23 is:

C 3 -C 6 alkyl; or

phenyl optionally substituted with 1-5 R 20 ;

R 31 is independently halogen, cyano, nitro, C 1 -C 6 alkyl, C 1 -C 6 haloalkyl, C 1 -C 6 hydroxyalkyl, C 2 -C 6 alkoxyalkyl, C 2 -C 6 haloalkoxyalkyl, C 2 -C 6 alkenyl, C 2 -C 6 haloalkenyl, C 3 -C 6 alkynyl, C 3 -C 6 haloalkynyl, hydroxyl, C 1 -C 6 alkoxy, C 1 -C 6 haloalkoxy, C 2 -C 6 alkenyloxy, C 2 -C 6 haloalkenyloxy, C 3 -C 6 alkynyloxy, C 3 -C 6 haloalkynyloxy, C 1 -C 6 alkylthio, C 1 -C 6 alkylsulfonyl, C 1 -C 6 haloalkylsulfonyl, C 2 -C 6 alkenylthio, C 2 -C 6 haloalkenylthio, C 2 -C 6 haloalkenylsulfonyl, C 3 -C 6 alkynylthio, C 3 -C 6 alkynylsulfonyl, C 3 -C 6 haloalkynylsulfonyl, C 1 -C 6 alkylamino, C 2 -C 8 dialkylamino, C 3 -C 8 dialkylaminocarbonyl, or C 3 -C 6 trialkylsilyl.

2. A compound of Formula (I)

wherein R 1 is —N(R 3 )R 4 ;

R 2 is —OR 21 ;

R 3 is H;

R 4 is H;

R 21 is (—CHR 22 ) m R 23 , M is 1;

R 22 is H;

R 23 is phenyl optionally substituted with 1-5 R 20 ;

R 20 is halogen, cyano, nitro, amino, C 1 -C 6 alkoxyalkoxy, C 1 -C 6 alkyl, C 1 -C 6 haloalkyl, C 1 -C 6 hydroxyalkyl, C 2 -C 6 alkoxyalkyl, C 2 -C 6 haloalkoxyalkyl, C 2 -C 6 alkenyl, hydroxyl, C 1 -C 6 alkoxy, C 1 -C 6 haloalkoxy, C 1 -C 6 alkylthio, C 1 -C 6 haloalkylthio, C 1 -C 6 alkylsulfonyl, C 1 -C 6 alkylamino, benzyloxy, or phenoxy, wherein each benzyloxy, phenoxy, may be optionally substituted with 1-3 substitutents independently selected from R 31 ; and

R 31 is halogen, C 1 -C 6 alkyl, or C 1 -C 6 alkoxy.

3. A compound of Formula (I)

wherein R 1 is —N(R 3 )R 4 ;

R 2 is —OR 21 ;

R 3 is H;

R 4 is H;

R 21 is (—CHR 22 ) m R 23 , M is 1;

R 22 is H; and

R 23 is phenyl, p-tolyl, 4-fluoro-phenyl, 4-methoxy-phenyl, 3-methoxy-phenyl, 3 fluoro-phenyl, 3-bromo-phenyl,2,4,6-trimethyl-phenyl, 1-ethyl-2-methoxy-phenyl, 3-benzonitrile, or 3-fluoro-4-methoxy-phenyl.

4. A composition for the control of a fungal pathogen including the compound of claim 1 and a phytologically acceptable carrier material.

5. The composition of claim 4 wherein the fungal pathogen is one Apple Scab ( Venturia inaequalis ), Speckled Leaf Blotch of Wheat ( Septoria tritici ), Leaf spot of sugarbeets ( Cercospora beticola ), Leaf Spot of peanut ( Cercospora arachidicola ), and Black Sigatoka ( Mycosphaerella fijiensis ).

6. A method for the control and prevention of fungal attack on a plant, the method including the steps of:

applying a fungicidally effective amount of at least one of the compounds of claim 1 to at least one of the plant, an area adjacent to the plant, soil adapted to support growth of the plant, a root of the plant, foliage of the plant, and a seed adapted to produce at least one of the plant and another plant.

7. A composition for the control of a fungal pathogen including the compound of claim 2 and a phytologically acceptable carrier material.

8. The composition of claim 7 wherein the fungal pathogen is one Apple Scab ( Venturia inaequalis ), Speckled Leaf Blotch of Wheat ( Septoria tritici ), Leaf spot of sugarbeets ( Cercospora beticola ), Leaf Spot of peanut ( Cercospora arachidicola ), and Black Sigatoka ( Mycosphaerella fijiensis ).

9. A method for the control and prevention of fungal attack on a plant, the method including the steps of:

applying a fungicidally effective amount of at least one of the compounds of claim 2 to at least one of the plant, an area adjacent to the plant, soil adapted to support growth of the plant, a root of the plant, foliage of the plant, and a seed adapted to produce at least one of the plant and another plant.

10. A composition for the control of a fungal pathogen including the compound of claim 3 and a phytologically acceptable carrier material.

11. The composition of claim 10 wherein the fungal pathogen is one Apple Scab ( Venturia inaequalis ), Speckled Leaf Blotch of Wheat ( Septoria tritici ), Leaf spot of sugarbeets ( Cercospora beticola ), Leaf Spot of peanut ( Cercospora arachidicola ), and Black Sigatoka ( Mycosphaerella fijiensis ).

12. A method for the control and prevention of fungal attack on a plant, the method including the steps of:

applying a fungicidally effective amount of at least one of the compounds of claim 3 to at least one of the plant, an area adjacent to the plant, soil adapted to support growth of the plant, a root of the plant, foliage of the plant, and a seed adapted to produce at least one of the plant and another plant.

13. The compound of claim 3 , wherein R 23 is p-tolyl.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Sep 6, 2023
From: DFJ ELEMENT PARTNERS, LLC (ON BEHALF OF DFJ ELEMENT, LP)
To: A-TURF, INC.; SURFACE AMERICA, INC.; ECORE INTERNATIONAL INC.; SPECTRASYSTEMS, INC.; DODGE DELAWARE INC.; DODGE REALTY PARTNERS, LP
Reel/Frame 064812/0674 →
PLEDGE AND SECURITY AGREEMENT Recorded Sep 8, 2016
From: ECORE INTERNATIONAL INC.; SURFACE AMERICA, INC.; A-TURF, INC.; SPECTRASYSTEMS, INC.; DODGE REALTY PARTNERS, LP; DODGE DELAWARE INC.
To: DFJ ELEMENT, L.P., AS AGENT
Reel/Frame 039955/0334 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 21, 2009
From: BENKO, ZOLTAN L.; BOEBEL, TIMOTHY; BREAUX, NNEKA T.; BRYAN, KRISTY; DAVIS, GEORGE E.; EPP, JEFFREY B.; LORSBACH, BETH; MARTIN, TIMOTHY P.; MEYER, KEVIN G.; OWEN, W. JOHN; POBANZ, MARK A.; NADER, BASSAM S.; RUIZ, JAMES M.; SMITH, FRISBY D.; SULLENBERGER, MICHAEL T.; WEBSTER, JEFFERY D.; YAO, CHENGLIN; YOUNG, DAVID H.
To: DOW AGROSCIENCES LLC
Reel/Frame 022572/0044 →
Continuity (3)
Provisional Application 61011799 · Jan 22, 2008
Provisional Application 61115297 · Nov 17, 2008
Related Publication 20090203647A1 · Aug 13, 2009