Reduction of graphene oxide to graphene in high boiling point solvents
View Patent ↗A method of creating graphene comprising the steps of dispersing graphene oxide into water to form a dispersion. Where the method further comprises adding a solvent to the dispersion to form a solution, and controlling a temperature of the solution to form graphene.
1. A method of creating graphene consisting of the steps of:
dispersing graphene oxide into water to form a dispersion;
adding a solvent to the dispersion to form a solution; and
controlling a temperature of the solution to form graphene.
2. The method of claim 1 wherein dispersing the graphene oxide into water comprises dispersing the graphene oxide into the water by sonication.
3. The method of claim 1 wherein the dispersion comprises a ratio of approximately one milligram of graphene oxide to approximately one milliliter of water.
4. The method of claim 1 wherein the solvent is a water miscible solvent.
5. The method of claim 4 wherein the water miscible solvent is at least one of n-methylpyrrolidone, ethylene glycol, glycerin, dimethylpyrrolidone, acetone, tetrahydrofuran, acetonitrile, dimethylformamide, an amine and an alcohol.
6. The method of claim 1 wherein adding solvent to the dispersion comprises adding an amount of solvent approximately equivalent to the amount of the dispersion.
7. The method of claim 1 wherein controlling the temperature of the solution comprises heating the solution to approximately 200° C. to form a reduction.
8. The method of claim 7 wherein controlling the temperature of the solution comprises the step of stirring the solution while heating the solution.
9. The method of claim 7 wherein controlling the temperature of the solution comprises the step of holding a temperature of the solution at approximately 200° C.
10. The method of claim 7 wherein controlling the temperature of the solution comprises holding a temperature of the solution once the water has evaporated from the solution.
11. The method of claim 7 wherein controlling the temperature of the solution comprises heating the solution in at least one of an autoclave and a high pressure chamber.
12. The method of claim 1 wherein the graphene oxide is dispersed in water by sonication, and the dispersion comprises a ratio of approximately two milligrams of graphene oxide to approximately one milliliter of water.
13. The method of claim 12 wherein the solvent is a water miscible solvent that is at least one of n-methylpyrrolidone, ethylene glycol, glycerin, dimethylpyrrolidone, acetone, tetrahydrofuran, acetonitrile, dimethylformamide, an amine and an alcohol.
14. The method of claim 12 wherein adding solvent to the dispersion comprises adding an amount of solvent approximately equivalent to one half the amount of dispersion.