IP Library Granted Patent US 7,699,988
Granted Patent B2
US 7,699,988 · App. 12/399,481 · Granted Apr 20, 2010

Enhanced water treatment for reclamation of waste fluids and increased efficiency treatment of potable waters

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Quick Facts
Patent No.
US 7,699,988
App. No.
12/399,481
Granted
Apr 20, 2010
Kind
B2
Abstract

Disclosed is a process for reclamation of waste fluids. A conditioning container is employed for receipt of waste material on a continuous flow for treatment within the container by immersible transducers producing ultrasonic acoustic waves in combination with a high level of injected ozone. The treated material exhibits superior separation properties for delivery into a centrifuge for enhanced solid waste removal. The invention discloses a cost efficient and environmentally friendly process and apparatus for cleaning and recycling of flowback, or frac water, which has been used to stimulate gas production from shale formations. The apparatus is mobile and containerized and suitable for installation at the well site.

Claims (11)

1. A mobile flowback water treatment system comprising: a backwash filter having an inlet that is fluidly connected to a source of flowback fluid, said backwash filter also having an outlet, the outlet of said backwash filter is fluidly connected to a first inlet of an ozone injector device, said ozone injector device having a second inlet fluidly connected to a source of ozone, said injector device having an outlet fluidly connected to an inlet of an ozone contact tank, said ozone tank having an outlet fluidly connected to a first inlet of an inline static mixer, said system also including a source of aluminum sulfate, said source of aluminum sulfate being fluidly connected to a second inlet of said inline static mixer, said in line static mixer having an outlet in fluid communication with an inlet of a main reactor tank, the inlet of said main reactor tank fluidly connected to an inlet manifold contained within said main reactor tank, said manifold configured to cause hydrodynamic cavitations within the main reactor tank, said main reactor further including ultrasonic transducers to create acoustic cavitations with said main reactor tank, said main reactor tank further including at least one electrically charged anode and at least one cathode within said main reaction tank configured to provide DC current to the flowback water within said tank.

2. The mobile flowback water treatment system of claim 1 wherein said main reactor tank has an outlet fluidly connected to at least one centrifuge to separate solids out of said flowback water suspended solids are removed from the flowback water at said at least one centrifuge.

3. The mobile flowback water treatment system of claim 2 wherein an outlet of said at least one centrifuge is fluidly connected to a plurality of the media tanks, said plurality of media tanks having a flowback fluid outlet, whereby the flowback fluid is polished and any remaining heavy metals as removed and any remaining ozone is converted to oxygen.

4. The mobile flowback water treatment system of claim 3 wherein the outlet of said plurality of media tanks is fluidly connected to a plurality of micron sized filters capable of filtering solids of one micron, said filters having a fluid outlet.

5. The mobile flowback water treatment system of claim 4 wherein the fluid outlet of said plurality of micron sized filters is fluidly connected to a plurality of reverse osmosis pumps, each pump increasing the fluid pressure of the flowback water, the fluid output from each pump is then introduced into a filtering chamber containing a reverse osmosis membrane thereby forcing the flowback water through a reverse osmosis membrane, said filtering chambers having a first and second outlet, the first outlet containing clean flowback water for subsequent storage and distribution and a second outlet containing concentrated waste to return to a reject water tank for reinjection or other suitable disposal.

6. The mobile flowback water treatment system of claim 1 wherein an ozone booster pump is connected between the outlet of said backwash filter and the first inlet of said ozone injector device.

7. The mobile flowback water treatment system of claim 1 wherein a feed pump moves said source of aluminum sulfate to said second inlet of said inline static mixer.

8. The mobile flowback treatment system of claim 1 wherein said main reactor tank is operated under a pressure greater than atmospheric pressure.

9. The mobile flowback treatment system of claim 1 wherein said source of ozone is an ozone generator which is in fluid communication with said injector.

10. The mobile flowback treatment system of claim 1 wherein said treatment system is mounted within a standard truck trailer that is capable of transport by truck, rail or ship.

11. The mobile flowback treatment system of claim 1 , said transducers include at least one pair of ultrasonic transducers operating at approximately 16 KHz and at least one pair of ultrasonic transducers operating at approximately 20 KHz.

Assignments (12)
CORRECTION BY DECLARATION ERRONEOUSLY FILED AGAINST REEL/FRAME:057538/0499 Recorded Oct 4, 2023
From: BRISBEN WATER SOLUTIONS LLC
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 065128/0340 →
CORRECTION BY DECLARATION ERRONEOUSLY FILED AGAINST REEL/FRAME:063722/0722 Recorded Oct 4, 2023
From: BRISBEN WATER SOLUTIONS LLC
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 065128/0393 →
RELEASE OF SECURITY INTEREST Recorded May 22, 2023
From: RKB HYDROTECH PROFESSIONAL, LLC
To: ECOZONIX, LLC
Reel/Frame 063722/0722 →
SECURITY INTEREST Recorded Sep 17, 2021
From: ECOZONIX, LLC
To: RKB HYDROTECH PROFESSIONAL, LLC
Reel/Frame 057538/0499 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 31, 2019
From: ECOSPHERE TECHNOLOGIES, INC
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 049326/0590 →
SECURITY INTEREST Recorded Mar 3, 2017
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 041459/0603 →
SECURITY INTEREST Recorded Nov 7, 2016
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 040234/0673 →
SECURITY INTEREST Recorded Sep 14, 2016
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 039724/0566 →
SECURITY INTEREST Recorded Jun 6, 2016
From: ECOSPHERE TECHNOLOGIES, INC.'
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 038818/0668 →
SECURITY INTEREST Recorded May 5, 2016
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 038465/0139 →
SECURITY INTEREST Recorded Mar 4, 2016
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLOUTIONS LLC
Reel/Frame 037893/0204 →
SECURITY INTEREST Recorded Jan 21, 2016
From: ECOSPHERE TECHNOLOGIES, INC.
To: BRISBEN WATER SOLUTIONS LLC
Reel/Frame 037543/0172 →